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US4082601A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for fabricating Li(NbTa)O3 films onto lithium tantalate single crystals

Assignee: Individual
•
Filing: 1976-01-26
•
Granted: 1978-04-04
•
Expires: 1996-01-26
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Abstract

Abstract The inventive process produces a Li(NbTa)O 3 single-domain, single-crystalline film on a lithium tantalate single-crystal. The film is grown on the lithium tantalate, single-crystal by hydrothermal synthesis wherein the alkaline solution is heated to a temperature which is lower than the Curie point temperature of lithium tantalate. The mother material is a mixture of tantalum and lithium salts. The resulting film may guide several modes of light, and possibly modulate them.

Inventors

  • 👤 Andre Maurice Regreny
  • 👤 Michel Xavier Passaret
  • 👤 Loic Andre Rivoallan

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 05:08
CPC Classifications
G; G02; G02B; G02B6/00; G02B6/10; G02B6/12; G02B6/13; G02B6/132; G02B2006/12035; G02B2006/1204; Y; Y10; Y10S; Y10S117/00; Y10S117/918

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 72 words
A process of manufacturing single crystal Li(NbTa)O 3 films on lithium tantalate single-crystals, wherein said film is grown in a pressure of about 1200 bars on the said lithium tantalate single-crystal by hydrothermal synthesis wherein the alkaline solution is heated to a temperature in the order of approximately 370° C. which is lower than the Curie point of lithium tantalate single-crystal, the mother material being a mixture of tantalum and niobium salts.
Claim 2
Dependent Claim 72 words
A process of manufacturing single crystal Li(NbTa)O 3 films on lithium tantalate single-crystals, wherein said film is grown in a pressure of about 1200 bars on the said lithium tantalate single-crystal by hydrothermal synthesis wherein the alkaline solution is heated to a temperature in the order of approximately 370° C. which is lower than the Curie point of lithium tantalate single-crystal, the mother material being a mixture of tantalum and niobium salts.
Claim 3
Dependent Claim 15 words
A process of manufacture according to claim 1, wherein the alkaline is a lithia solution.
Claim 4
Dependent Claim 25 words
A process of manufacture according to claim 1 wherein tantalum salt is lithium tantalate and niobium salt is niobium pentoxide Nb 2 O 5 .
Claim 5
Dependent Claim 23 words
A process of manufacture according to claim 1 wherein tantalum salt is tantalum pentoxide and niobium salt is lithium niobate LiNbO 3 .
Claim 6
Dependent Claim 20 words
A process of manufacture according to claim 1 wherein both the tantalum and niobium salts are oxides of those elements.
Claim 7
Dependent Claim 26 words
A process of manufacture according to claim 1 wherein the film thickness is determined as a function of the temperature and time duration of the reaction.
Claim 8
Dependent Claim 29 words
A process of manufacture according to claim 1 wherein a refractive index of the film is predetermined as a function of the niobium/tantalum ratio in the initial mother material.

References Cited (Backward Citations)

US2954300A Cited
US3440025A Cited
US3428438A Cited
US3533755A Cited
US3634044A Cited
JPS4721219U Cited
US4001076A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1981-04-03 1981-10-03 1982-04-04 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1985-04-03 1985-10-03 1986-04-04 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1989-04-03 1989-10-03 1990-04-04 $7700.00 Window Closed / Lapsed

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