Patent US4416410A successfully refreshed from Google Patents.
Patent US4046619A successfully refreshed from Google Patents.
US4046619A
Expired / Lapsed
US
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Method of treating the surface of a glass member
Assignee: National Aeronautics and Space Administration
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Filing: 1976-05-03
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Granted: 1977-09-06
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Expires: 1996-05-03
Abstract
Abstract A method of treating a surface of a glass member intended to abut a transparent element for disrupting the light interference fringes formed therebetween. The method involves the steps of grinding the surface to form irregularities thereon; bathing the surface with an aqueous solution containing between substantially 41.3 percent and 45.7 percent by volume of sulfuric acid and between substantially 54.3 percent and 58.7 percent by volume of hydrofluoric acid for a time sufficient to polish the irregularities until the glass member is about 90 percent light transmissive; and washing the glass member with a liquid having a temperature substantially lower than the temperature of the aqueous solution for preventing further reaction between the aqueous solution and the surface.
Inventors
- 👤 Stephen H. Rice
- 👤 Rodney S. Spencer
- 👤 Charles M. Fleetwood, Jr.
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-01 21:25
CPC Classifications
C; C03; C03C; C03C15/00; G; G02; G02B; G02B1/00; G02B1/10; G02B1/12
Claims Analysis
Total Claims: 10
Claim 1
Independent Claim
173 words
A method of treating a glass member intended to abut a transparent element for disrupting the light interference fringes formed therebetween, comprising the steps of: grinding the surface of the glass member intended to abut the transparent element with a grinding powder of substantially 22.5 microns to form a multiplicity of alternating peaks and valleys, said peaks and valleys permitting nondetectable light interference fringes to form within said valleys when said transparent element contacts said peaks; bathing said surface with an aqueous solution having a temperature range of between substantially 70° and 75° F. and containing between substantially 41.3% and 45.7% by volume of sulfuric acid and between substantially 54.3% and 58.7% by volume of hydrofluoric acid for a time period of between substantially 105 and 135 seconds for polishing said peaks and valleys until said glass member is about 90% light transmissive; and washing said glass member with a liquid having a temperature range of between substantially 45° and 55° F. for preventing further reaction between said aqueous solution and said surface.
Claim 2
Independent Claim
173 words
A method of treating a glass member intended to abut a transparent element for disrupting the light interference fringes formed therebetween, comprising the steps of: grinding the surface of the glass member intended to abut the transparent element with a grinding powder of substantially 22.5 microns to form a multiplicity of alternating peaks and valleys, said peaks and valleys permitting nondetectable light interference fringes to form within said valleys when said transparent element contacts said peaks; bathing said surface with an aqueous solution having a temperature range of between substantially 70° and 75° F. and containing between substantially 41.3% and 45.7% by volume of sulfuric acid and between substantially 54.3% and 58.7% by volume of hydrofluoric acid for a time period of between substantially 105 and 135 seconds for polishing said peaks and valleys until said glass member is about 90% light transmissive; and washing said glass member with a liquid having a temperature range of between substantially 45° and 55° F. for preventing further reaction between said aqueous solution and said surface.
Claim 3
Dependent Claim
24 words
The method of claim 1 wherein said aqueous solution contains substantially 43.4% by volume of sulfuric acid and 56.6% by volume of hydrofluoric acid.
Claim 4
Dependent Claim
20 words
The method of claim 1 wherein the step of bathing involves the submerging of said surface into said aqueous solution.
Claim 5
Dependent Claim
18 words
The method of claim 3 further including the step of rotating said glass member within said aqueous solution.
Claim 6
Dependent Claim
19 words
The method of claim 4 wherein said glass member is rotated between substantially 30 and 50 revolutions per minute.
Claim 7
Dependent Claim
17 words
The method of claim 4 wherein said glass member is rotated at substantially 40 revolutions per minute.
Claim 8
Dependent Claim
26 words
The method of claim 1 wherein the step of bathing said surface in said aqueous solution is maintained for a time period of substantially 2 minutes.
Claim 9
Dependent Claim
29 words
The method of claim 1 further including the final step, of removing excess fluoride formed by the reaction of said aqueous solution with said glass member on said surface.
Claim 10
Dependent Claim
38 words
The method of claim 8 wherein the step of removing includes: scraping said surface with a brush to loosen said excess fluoride; washing said surface with water to remove said excess fluoride and; drying said surface with acetone.
References Cited (Backward Citations)
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1980-09-05 | 1981-03-07 | 1981-09-06 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1984-09-05 | 1985-03-07 | 1985-09-06 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1988-09-05 | 1989-03-07 | 1989-09-06 | $7700.00 | Window Closed / Lapsed |