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US3985846A Expired / Lapsed US ⏱️ 0.0 years remaining

Ceramic firing process

Assignee: WR Grace and Co
•
Filing: 1975-04-16
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Granted: 1976-10-12
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Expires: 1995-04-16
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Abstract

Abstract This invention relates to an improvement in the process of preparing porous ceramic articles which are formed by blending a composition containing a polyolefin, a ceramic filler and a plasticizer; shaping the blend; extracting the plasticizer and firing the article to remove the polyolefin. The improvement comprises soaking the extracted article in a water solution of a surfactant prior to firing which results in a substantial reduction in the number of cracked pieces when firing many pieces simultaneously.

Inventors

  • 👤 Christian Bent Lundsager
  • 👤 Robert Matthews Murch

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-03 20:33
CPC Classifications
B; B01; B01D; B01D53/00; B01D53/34; B01J; B01J37/00; B01J37/0009; B01J37/0018; C; C04; C04B; C04B26/00; C04B26/02; C04B26/04; C04B26/045; C04B38/00; C04B38/06; C04B38/0615

Claims Analysis

Total Claims: 3
Claim 1
Independent Claim 91 words
In a process for preparing porous ceramic structures with good resistance to cracking during firing wherein a composition consisting essentially of a polyolefin, a ceramic filler and a plasticizer is homogeneously blended, said composition is shaped to form a plastic structure, whereupon said plasticizer is extracted with an appropriate solvent and said polyolefin is subsequently removed by heating to form a porous ceramic structure, the improvement which consists of soaking said extracted ceramic structure in an aqueous solution of 1/2% synthetic surfactant for 8 to 16 hours prior to said heating.
Claim 2
Dependent Claim 91 words
In a process for preparing porous ceramic structures with good resistance to cracking during firing wherein a composition consisting essentially of a polyolefin, a ceramic filler and a plasticizer is homogeneously blended, said composition is shaped to form a plastic structure, whereupon said plasticizer is extracted with an appropriate solvent and said polyolefin is subsequently removed by heating to form a porous ceramic structure, the improvement which consists of soaking said extracted ceramic structure in an aqueous solution of 1/2% synthetic surfactant for 8 to 16 hours prior to said heating.
Claim 3
Dependent Claim 25 words
The process of claim 1 further characterized in that said firing of the ceramic structures takes place in a kiln operated at reducing atmosphere conditions.

References Cited (Backward Citations)

US3261894A Cited
US3755204A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-10-12 1980-04-12 1980-10-12 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-10-12 1984-04-12 1984-10-12 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-10-12 1988-04-12 1988-10-12 $7700.00 Window Closed / Lapsed

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