Patent US3971733A successfully refreshed from Google Patents.
US3971733A
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Water-wettable wax composition and process for producing the same
Assignee: Honeywell International Inc
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Filing: 1974-12-17
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Granted: 1976-07-27
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Expires: 1994-12-17
Abstract
Abstract A water-wettable wax composition comprising a particulate hydrocarbon wax and an emulsifier which is (a) a hydrophilic oil-in-water emulsifier having an HLB of from about 10 to about 20, or (b) mixtures of said hydrophilic oil-in-water emulsifier with a lipophilic emulsifier, wherein there is sufficient hydrophilic emulsifier present to render the overall mixture hydrophilic, said particulate hydrocarbon wax having a particle size of about 1 to 5 microns, the emulsifier being uniformly dispersed in the wax particles.. This wax composition forms a homogeneous water suspension suitable for imparting lubricity.
Inventors
- 👤 Edwin Francis Hawkins
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-27 15:11
CPC Classifications
D; D06; D06M; D06M13/00; D06M13/02; C; C08; C08K; C08K3/00; C08K3/34; D06M11/00; D06M11/77; D06M11/79
Claims Analysis
Total Claims: 16
Claim 1
Independent Claim
158 words
A textile lubricating water-wettable wax composition consisting essentially of a particulate hydrocarbon wax having a chain length of from about 30 to 55 carbon atoms, a melting point ranging from about 65°C. to about 105°C., and a penetration ranging from about 1 to about 6; about 1 to 10 percent based on the weight of said hydrocarbon wax of a conditioning agent selected from the group consisting of a finely-ground calcium silicate, magnesium silicate, and precipitated ultra-fine silica, and an emulsifier selected from the group consisting of: a. a hydrophilic oil-in-water emulsifier having an HLB of from about 10 to about 20, and b. mixtures of said hydrophilic oil-in-water emulsifier with a lipophilic emulsifier, wherein there is sufficient hydrophilic emulsifier present to render the overall mixture hydrophilic; said particulate hydrocarbon wax having a particle size of 1 to 5 microns, the ratio of total emulsifier to said particulate hydrocarbon wax being about 3 to 20 percent by weight.
Claim 2
Dependent Claim
158 words
A textile lubricating water-wettable wax composition consisting essentially of a particulate hydrocarbon wax having a chain length of from about 30 to 55 carbon atoms, a melting point ranging from about 65°C. to about 105°C., and a penetration ranging from about 1 to about 6; about 1 to 10 percent based on the weight of said hydrocarbon wax of a conditioning agent selected from the group consisting of a finely-ground calcium silicate, magnesium silicate, and precipitated ultra-fine silica, and an emulsifier selected from the group consisting of: a. a hydrophilic oil-in-water emulsifier having an HLB of from about 10 to about 20, and b. mixtures of said hydrophilic oil-in-water emulsifier with a lipophilic emulsifier, wherein there is sufficient hydrophilic emulsifier present to render the overall mixture hydrophilic; said particulate hydrocarbon wax having a particle size of 1 to 5 microns, the ratio of total emulsifier to said particulate hydrocarbon wax being about 3 to 20 percent by weight.
Claim 3
Dependent Claim
12 words
The composition of claim 1 wherein the conditioning agent is ultra-fine silica.
Claim 4
Dependent Claim
24 words
The composition of claim 1, wherein the hydrophilic oil-in-water emulsifier is selected from the group consisting of sodium lauryl sulfate and sodium N-methyl-N-oleoyl taurate.
Claim 5
Dependent Claim
21 words
The composition of claim 1 wherein the lipophilic emulsifier is selected from the group consisting of partial esters of fatty acids.
Claim 6
Dependent Claim
26 words
The composition of claim 1 additionally comprising up to 5 percent based on the weight of the hydrocarbon wax of a sodium lignin sulfonate dispersing agent.
Claim 7
Dependent Claim
167 words
A textile lubricating water-wettable wax composition consisting essentially of a particualte hydrocarbon wax having a chain length of from about 30 to 55 carbon atoms, a melting point ranging from about 65°C. to about 105°C., and a penetration ranging from about 1 to about 6; about 1 to 10 percent based on the weight of said hydrocarbon wax of ultra-fine silica; and an emulsifier selected from the group consisting of: a. a hydrophilic oil-in-water emulsifier selected from the group consisting of sodium lauryl sulfate and sodium N-methyl-N-oleoyl taurate, said emulsifier having an HLB of from about 10 to about 20, and b. mixtures of said hydrophilic oil-in-water emulsifier with a lipophilic emulsifier selected from the group consisting of partial esters of fatty acids, wherein there is sufficient hydrophilic emulsifier present to render the overall mixture hydrophilic; said particulate hydrocarbon wax having a particle size of 1 to 5 microns, the ratio of total emulsifier to said particulate hydrocarbon wax being about 3 to 20 percent by weight.
Claim 8
Dependent Claim
167 words
A textile lubricating water-wettable wax composition consisting essentially of a particualte hydrocarbon wax having a chain length of from about 30 to 55 carbon atoms, a melting point ranging from about 65°C. to about 105°C., and a penetration ranging from about 1 to about 6; about 1 to 10 percent based on the weight of said hydrocarbon wax of ultra-fine silica; and an emulsifier selected from the group consisting of: a. a hydrophilic oil-in-water emulsifier selected from the group consisting of sodium lauryl sulfate and sodium N-methyl-N-oleoyl taurate, said emulsifier having an HLB of from about 10 to about 20, and b. mixtures of said hydrophilic oil-in-water emulsifier with a lipophilic emulsifier selected from the group consisting of partial esters of fatty acids, wherein there is sufficient hydrophilic emulsifier present to render the overall mixture hydrophilic; said particulate hydrocarbon wax having a particle size of 1 to 5 microns, the ratio of total emulsifier to said particulate hydrocarbon wax being about 3 to 20 percent by weight.
Claim 9
Dependent Claim
29 words
The composition of claim 6 wherein said composition additionally contains up to 5 percent based on the weight of the hydrocarbon wax of a sodium lignin sulfonate dispersing agent.
Claim 10
Independent Claim
153 words
A method of preparing a textile lubricating water-wettable wax composition comprising: a. mixing at substantially ambient temperature a particulate hydrocarbon wax having a chain length of from about 30 to 55 carbon atoms, a melting point ranging from about 65°C. to about 105°C., and a penetration ranging from about 1 to about 6, with 1 to 10 percent by weight based on the weight of the hydrocarbon wax of a conditioning agent selected from the group consisting of finely ground calcium silicate, magnesium silicate and precipitated ultra-fine silica, and an emulsifier selected from the group consisting of: a hydrophilic oil-in-water emulsifier having an HLB of from about 10 to about 20, and mixtures of said hydrophilic oil-in-water emulsifier with a lipophilic emulsifier, wherein there is sufficient hydrophilic emulsifier present to render the overall mixture hydrophilic; the ratio of total emulsifier to said particulate hydrocarbon wax being about 3 to 20 percent by weight;
Claim 11
Independent Claim
153 words
A method of preparing a textile lubricating water-wettable wax composition comprising: a. mixing at substantially ambient temperature a particulate hydrocarbon wax having a chain length of from about 30 to 55 carbon atoms, a melting point ranging from about 65°C. to about 105°C., and a penetration ranging from about 1 to about 6, with 1 to 10 percent by weight based on the weight of the hydrocarbon wax of a conditioning agent selected from the group consisting of finely ground calcium silicate, magnesium silicate and precipitated ultra-fine silica, and an emulsifier selected from the group consisting of: a hydrophilic oil-in-water emulsifier having an HLB of from about 10 to about 20, and mixtures of said hydrophilic oil-in-water emulsifier with a lipophilic emulsifier, wherein there is sufficient hydrophilic emulsifier present to render the overall mixture hydrophilic; the ratio of total emulsifier to said particulate hydrocarbon wax being about 3 to 20 percent by weight;
Claim 12
Dependent Claim
36 words
b. grinding the mixture from step (a) in a jet mill to thereby form a particulate product having a particle size of about 1 to 5 microns, the emulsifier being uniformly dispersed in said wax particles.
Claim 13
Dependent Claim
36 words
b. grinding the mixture from step (a) in a jet mill to thereby form a particulate product having a particle size of about 1 to 5 microns, the emulsifier being uniformly dispersed in said wax particles.
Claim 14
Dependent Claim
31 words
The method of claim 8 wherein the hydrophilic oil-in-water emulsifier is selected from the group consisting of sodium lauryl sulfate and sodium N-methyl-N-oleoyl taurate and the conditioning agent is ultra-fine silica.
Claim 15
Dependent Claim
28 words
The method of claim 8 wherein the lipophilic emulsifier is selected from the group consisting of partial esters of fatty acids and the conditioning agent is ultra-fine silica.
Claim 16
Dependent Claim
40 words
The method of claim 8 wherein in step (a) up to 5 percent based on the weight of the hydrocarbon wax of a sodium lignin sulfonate dispersing agent is incorporated into the mixture and the conditioning agent is ultra-fine silica.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1979-07-27 | 1980-01-26 | 1980-07-27 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1983-07-27 | 1984-01-26 | 1984-07-27 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1987-07-27 | 1988-01-26 | 1988-07-27 | $7700.00 | Window Closed / Lapsed |