Patent US7029632B1 successfully refreshed from Google Patents.
US7029632B1
Expired / Lapsed
US
⏱️ 0.0 years remaining
Radiation-heated fluidized-bed reactor
Assignee: Wacker Chemie AG
•
Filing: 2000-10-02
•
Granted: 2006-04-18
•
Expires: 2020-10-02
Abstract
Abstract A radiation-heated fluidized-bed reactor and a process for producing high-purity polycrystalline silicon by using this reactor are provided. In this reactor, a heater device ( 14 ) is a radiation source for thermal radiation which is arranged outside the inner reactor tube and as a cylinder around the heater zone, without being in direct contact with the inner reactor tube. The inner reactor tube is designed in such a manner that it uses thermal radiation to heat the silicon particles in the heating zone to a temperature which is such that the reaction temperature is established in the reaction zone.
Inventors
- 👤 Dieter Weidhaus
- 👤 Alexander Hayduk
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 20:08
CPC Classifications
B; B01; B01J; B01J8/00; B01J8/18; B01J8/1836; B01J8/1818; C; C01; C01B; C01B33/00; C01B33/02; C01B33/021; C01B33/027; B01J2208/00; B01J2208/00008; B01J2208/00017; B01J2208/00106; B01J2208/00115; B01J2208/00132; B01J2208/00433; B01J2208/00477; B01J2208/00495
Claims Analysis
Total Claims: 10
Claim 1
Independent Claim
348 words
A fluidized-bed reactor ( 1 ) comprising: a) a pressure-supporting enclosure ( 2 ); b) an inner reactor tube ( 3 ) within said enclosure ( 2 ) and made from a material which exhibits high transmission for thermal radiation; c) an inlet ( 4 ) at a top of said enclosure ( 2 ) for silicon particles ( 5 ); d) an inlet device ( 6 ) for supplying a reaction gas ( 7 ) which contains a silicon compound in gas or vapor form, the inlet device ( 6 ) being of tubular design and dividing the fluidized bed into zones consisting of a heating zone ( 17 ) and a separate reaction zone ( 18 ) situated above the heating zone, wherein the inlet device is positioned so that the reaction gas supplied by the inlet device does not enter the heating zone; e) a gas-distribution device ( 8 ) at a bottom of said enclosure ( 2 ) for feeding a fluidizing gas ( 9 ) into the heating zone; f) an outlet ( 10 ) at the top of said enclosure ( 2 ) for reaction gas which has not fully reacted, fluidizing gas and products of reaction ( 11 ) which are in gas or vapor form and collect above a fluidized-bed surface ( 19 ); g) an outlet ( 12 ) at the bottom of said enclosure ( 2 ) for a product ( 13 ); h) a heater device ( 14 ); i) an energy supply ( 15 ) for the heater device ( 14 ); and wherein the heater device ( 14 ) is a radiation source for thermal radiation which is arranged outside the inner reactor tube and as a cylinder around the heating zone ( 17 ), without being in direct contact with the inner reactor tube, and is designed in such a manner that it uses thermal radiation to heat the silicon particles in the heating zone to a temperature which is such that the reaction temperature is established in the reaction zone ( 18 ).
Claim 2
Dependent Claim
348 words
A fluidized-bed reactor ( 1 ) comprising: a) a pressure-supporting enclosure ( 2 ); b) an inner reactor tube ( 3 ) within said enclosure ( 2 ) and made from a material which exhibits high transmission for thermal radiation; c) an inlet ( 4 ) at a top of said enclosure ( 2 ) for silicon particles ( 5 ); d) an inlet device ( 6 ) for supplying a reaction gas ( 7 ) which contains a silicon compound in gas or vapor form, the inlet device ( 6 ) being of tubular design and dividing the fluidized bed into zones consisting of a heating zone ( 17 ) and a separate reaction zone ( 18 ) situated above the heating zone, wherein the inlet device is positioned so that the reaction gas supplied by the inlet device does not enter the heating zone; e) a gas-distribution device ( 8 ) at a bottom of said enclosure ( 2 ) for feeding a fluidizing gas ( 9 ) into the heating zone; f) an outlet ( 10 ) at the top of said enclosure ( 2 ) for reaction gas which has not fully reacted, fluidizing gas and products of reaction ( 11 ) which are in gas or vapor form and collect above a fluidized-bed surface ( 19 ); g) an outlet ( 12 ) at the bottom of said enclosure ( 2 ) for a product ( 13 ); h) a heater device ( 14 ); i) an energy supply ( 15 ) for the heater device ( 14 ); and wherein the heater device ( 14 ) is a radiation source for thermal radiation which is arranged outside the inner reactor tube and as a cylinder around the heating zone ( 17 ), without being in direct contact with the inner reactor tube, and is designed in such a manner that it uses thermal radiation to heat the silicon particles in the heating zone to a temperature which is such that the reaction temperature is established in the reaction zone ( 18 ).
Claim 3
Dependent Claim
35 words
The fluidized-bed reactor as claimed in claim 1 , wherein a space between said inner reactor tube ( 3 ) and said pressure-supporting enclosure ( 2 ) is provided with thermal insulation ( 16 ).
Claim 4
Dependent Claim
31 words
The fluidized-bed reactor as claimed in claim 1 , wherein the heater device is formed over a large area around the entire heating zone and thus forms a cylindrical radiation source.
Claim 5
Dependent Claim
26 words
The fluidized-bed reactor as claimed in claim 1 , wherein the heater device emits thermal radiation with a wavelength of from 0.4 μm to 900 μm.
Claim 6
Dependent Claim
26 words
The fluidized-bed reactor as claimed in claim 4 , wherein the heater device emits thermal radiation with a wavelength of from 0.4 μm to 300 μm.
Claim 7
Dependent Claim
51 words
The fluidized-bed reactor as claimed in claim 1 , wherein the heater device is selected from the group consisting of a heater element made from doped silicon, a heater element made from graphite, a heater element made from silicon carbide, a quartz tube radiator, a ceramic radiator and a wire radiator.
Claim 8
Dependent Claim
39 words
The fluidized-bed reactor as claimed in claim 1 , wherein all components of the reactor which come into contact with product are selected from the group consisting of an inert material and a component coated with an inert material.
Claim 9
Dependent Claim
355 words
A fluidized-bed reactor ( 1 ) comprising: (a) a pressure supporting enclosure ( 2 ); (b) an inner reactor tube ( 3 ) within said enclosure ( 2 ) and made from a material which exhibits high transmission for thermal radiation; (c) an inlet ( 4 ) at a top of said enclosure ( 2 ) for silicon particles ( 5 ) (d) an inlet device ( 6 ) for supplying a reaction gas ( 7 ) which contains a silicon compound in gas or vapor form, the inlet device ( 6 ) being of tubular design and dividing the fluidized bed into a heating zone ( 17 ) and a reaction zone ( 18 ) situated above the heating zone; (e) a gas-distribution device ( 8 ) at a bottom of said enclosure ( 2 ) for feeding a fluidizing gas ( 9 ) into the heating zone; (f) an outlet ( 10 ) at the top of said enclosure ( 2 ) for reaction gas which has not fully reacted, fluidizing gas and products of reaction ( 11 ) which are in gas or vapor form and collect above a fluidized-bed surface ( 19 ); (g) an outlet ( 12 ) at the bottom of said enclosure ( 2 ) for a product ( 13 ); (h) a heater device ( 14 ); (i) an energy supply ( 15 ) for the heater device ( 14 ); and wherein the heater device ( 14 ) is a radiation source for thermal radiation which is arranged outside the inner reactor tube and as a cylinder around the heating zone ( 17 ), without being in direct contact with the inner reactor tube, and is designed in such a manner that it uses thermal radiation to heat the silicon particles in the heating zone to a temperature which is such that the reaction temperature is established in the reaction zone ( 18 ) and wherein the heater device is a tube with meandering slots made from graphite with a SiC surface coating which is arranged in the reactor, standing on or hanging from electrode terminals.
Claim 10
Dependent Claim
355 words
A fluidized-bed reactor ( 1 ) comprising: (a) a pressure supporting enclosure ( 2 ); (b) an inner reactor tube ( 3 ) within said enclosure ( 2 ) and made from a material which exhibits high transmission for thermal radiation; (c) an inlet ( 4 ) at a top of said enclosure ( 2 ) for silicon particles ( 5 ) (d) an inlet device ( 6 ) for supplying a reaction gas ( 7 ) which contains a silicon compound in gas or vapor form, the inlet device ( 6 ) being of tubular design and dividing the fluidized bed into a heating zone ( 17 ) and a reaction zone ( 18 ) situated above the heating zone; (e) a gas-distribution device ( 8 ) at a bottom of said enclosure ( 2 ) for feeding a fluidizing gas ( 9 ) into the heating zone; (f) an outlet ( 10 ) at the top of said enclosure ( 2 ) for reaction gas which has not fully reacted, fluidizing gas and products of reaction ( 11 ) which are in gas or vapor form and collect above a fluidized-bed surface ( 19 ); (g) an outlet ( 12 ) at the bottom of said enclosure ( 2 ) for a product ( 13 ); (h) a heater device ( 14 ); (i) an energy supply ( 15 ) for the heater device ( 14 ); and wherein the heater device ( 14 ) is a radiation source for thermal radiation which is arranged outside the inner reactor tube and as a cylinder around the heating zone ( 17 ), without being in direct contact with the inner reactor tube, and is designed in such a manner that it uses thermal radiation to heat the silicon particles in the heating zone to a temperature which is such that the reaction temperature is established in the reaction zone ( 18 ) and wherein the heater device is a tube with meandering slots made from graphite with a SiC surface coating which is arranged in the reactor, standing on or hanging from electrode terminals.
References Cited (Backward Citations)
DE3638931A1
Cited
US4786477A
Cited
JPH01208311A
Cited
US4967486A
Cited
US5382412A
Cited
DE4327308A1
Cited
WO1996041036A2
Cited
US5810934A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 2009-04-17 | 2009-10-17 | 2010-04-18 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 2013-04-17 | 2013-10-17 | 2014-04-18 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2017-04-17 | 2017-10-17 | 2018-04-18 | $7700.00 | Window Closed / Lapsed |