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US6037003A Expired / Lapsed US ⏱️ 0.0 years remaining

Chemical vapor deposition of aluminum oxide

Assignee: Harvard University
•
Filing: 1997-10-15
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Granted: 2000-03-14
•
Expires: 2017-10-15
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Abstract

Abstract An aluminum oxide film is deposited on a heated substrate by CVD from one or more alkylaluminum alkoxide compounds having composition R n Al 2 (OR') 6-n , wherein R and R' are alkyl groups and n is in the range of 1 to 5.

Inventors

  • 👤 Roy Gordon
  • 👤 Keith Kramer
  • 👤 Xinye Liu

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 01:35
CPC Classifications
C; C23; C23C; C23C16/00; C23C16/22; C23C16/30; C23C16/40; C23C16/403

Claims Analysis

Total Claims: 15
Claim 1
Independent Claim 70 words
A process for forming a material comprising aluminum oxide, comprising: providing a vapor generated from a non-pyrophoric liquid, said liquid comprised of one or more alkylaluminum alkoxide compounds having a composition R n Al 2 (OR') 6-n , where R and R' are alkyl groups and n is in the range of 1 to 5; and contacting the vapor with a heated surface to deposit an aluminum oxide containing material.
Claim 2
Dependent Claim 70 words
A process for forming a material comprising aluminum oxide, comprising: providing a vapor generated from a non-pyrophoric liquid, said liquid comprised of one or more alkylaluminum alkoxide compounds having a composition R n Al 2 (OR') 6-n , where R and R' are alkyl groups and n is in the range of 1 to 5; and contacting the vapor with a heated surface to deposit an aluminum oxide containing material.
Claim 3
Dependent Claim 58 words
A process for forming a material comprising aluminum oxide, comprising: providing a vapor comprised of one or more alkylaluminum alkoxide compounds having a composition R n Al 2 (OR') 6-n , where R and R' are alkyl groups and n is less than four; and contacting the vapor with a heated surface to deposit an aluminum oxide-containing material.
Claim 4
Dependent Claim 58 words
A process for forming a material comprising aluminum oxide, comprising: providing a vapor comprised of one or more alkylaluminum alkoxide compounds having a composition R n Al 2 (OR') 6-n , where R and R' are alkyl groups and n is less than four; and contacting the vapor with a heated surface to deposit an aluminum oxide-containing material.
Claim 5
Dependent Claim 11 words
The process of claim 1, wherein n is less than four.
Claim 6
Dependent Claim 12 words
The process of claim 1 or 2, wherein n is about three.
Claim 7
Dependent Claim 19 words
The process of claim 1 or 2, in which the vapor further includes a reactive oxygen-containing gas or vapor.
Claim 8
Dependent Claim 14 words
The process of claim 5, in which the reactive oxygen-containing gas is oxygen gas.
Claim 9
Dependent Claim 24 words
The process of claim 1 or 2, wherein the vapor comprises a predominant amount of an alkylaluminum alkoxide, wherein n is three or less.
Claim 10
Dependent Claim 17 words
The process of claim 1 or 2, wherein the vapor comprises a predominant amount of triethyldialuminum tri-sec-butoxide.
Claim 11
Dependent Claim 17 words
The process of claim 1 or 2, wherein the vapor comprises a predominant amount of triethyldialuminum tri-isopropoxide.
Claim 12
Dependent Claim 21 words
The process of claim 1 or 2, in which the substrate temperature is in the range from 500 to 700° C.
Claim 13
Dependent Claim 19 words
The process of claim 6, in which the substrate temperature is in the range from 300 to 500° C.
Claim 14
Dependent Claim 14 words
The process of claim 1, wherein the liquid is vaporized by thin film evaporation.
Claim 15
Dependent Claim 16 words
The process of claim 1, wherein the liquid is vaporized by nebulization into a carrier gas.

References Cited (Backward Citations)

US2805965A Cited
US2972555A Cited
DE3918932A1 Cited
US5098857A Cited
WO1997020963A1 Cited
WO1998002444A1 Cited
WO1998016667A1 Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 2003-03-14 2003-09-13 2004-03-14 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2007-03-14 2007-09-13 2008-03-14 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2011-03-14 2011-09-13 2012-03-14 $7700.00 Window Closed / Lapsed

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