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US5620526A Expired / Lapsed US ⏱️ 0.0 years remaining

In-situ cleaning of plasma treatment chamber

Assignee: Fujitsu VLSI Ltd
•
Filing: 1994-07-22
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Granted: 1997-04-15
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Expires: 2014-07-22
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Abstract

Abstract A cleaning of a plasma chamber is done by a NF 3 plasma treatment (typically under 1 to 1.5 Torr). The etching rate of an oxide layer can be improved by inserting, between the NF 3 plasma treatments, a low pressure (lower than 10 -1 Torr) plasma treatment preferably in a plasma of oxygen, water vapor, silane, fluorine, a hydrate compound, nitrogen trifluoride, or a mixture of nitrogen trifluoride with at least one of hydrogen fluoride, fluorine, water vapor and hydride compounds.

Inventors

  • 👤 Hirofumi Watatani
  • 👤 Masahiko Doki
  • 👤 Shoji Okuda
  • 👤 Junya Nakahira
  • 👤 Hideaki Kikuchi

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-03 11:54
CPC Classifications
C; C09; C09K; C09K13/00; C09K13/04; C09K13/08; C23; C23C; C23C16/00; C23C16/44; C23C16/4401; C23C16/4405

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 140 words
A process for in-situ cleaning of a plasma treatment chamber, said process comprising the steps of: conducting a first plasma treatment in a plasma treatment chamber with nitrogen trifluoride plasma at a first pressure, so as to remove an oxide layer previously deposited inside the plasma treatment chamber; conducting a second plasma treatment in said plasma treatment chamber at a second pressure lower than said first pressure, said second plasma treating being conducted in a plasma of a gas selected from a group consisting of oxygen, water vapor, silane, fluorine, nitrogen trifluoride, or a mixture of nitrogen trifluoride with at least one of hydrogen fluoride, fluorine, and water vapor; and a third plasma treatment in said plasma treatment chamber with nitrogen trifluoride plasma at a third pressure higher than said second pressure, so as to further remove said oxide layer.
Claim 2
Dependent Claim 140 words
A process for in-situ cleaning of a plasma treatment chamber, said process comprising the steps of: conducting a first plasma treatment in a plasma treatment chamber with nitrogen trifluoride plasma at a first pressure, so as to remove an oxide layer previously deposited inside the plasma treatment chamber; conducting a second plasma treatment in said plasma treatment chamber at a second pressure lower than said first pressure, said second plasma treating being conducted in a plasma of a gas selected from a group consisting of oxygen, water vapor, silane, fluorine, nitrogen trifluoride, or a mixture of nitrogen trifluoride with at least one of hydrogen fluoride, fluorine, and water vapor; and a third plasma treatment in said plasma treatment chamber with nitrogen trifluoride plasma at a third pressure higher than said second pressure, so as to further remove said oxide layer.
Claim 3
Dependent Claim 16 words
A process according to claim 1, wherein said second pressure is lower than 10 -1 Torr.
Claim 4
Dependent Claim 16 words
A process according to claim 1, wherein said second pressure is lower than 10 -3 Torr.
Claim 5
Dependent Claim 17 words
A process according to claim 1, wherein said second plasma treatment is conducted in an oxygen plasma.
Claim 6
Dependent Claim 19 words
A process according to claim 1, wherein said second plasma treatment is conducted in a plasma of nitrogen trifluoride.
Claim 7
Dependent Claim 18 words
A process according to claim 1, wherein said second plasma treatment is conducted in a plasma of silane.
Claim 8
Dependent Claim 26 words
A process according to claim 1, wherein said first and/or third plasma treatments are conducted in a plasma of a mixture of nitrogen trifluoride and fluorine.
Claim 9
Dependent Claim 34 words
A process according to claim 1, wherein said third plasma treatment is conducted under the same conditions as those of said first plasma treatment and said first and second plasma treatments are cyclically repeated.
Claim 10
Dependent Claim 15 words
A process according to claim 1, wherein said plasma chamber is a microwave plasma chamber.
Claim 11
Dependent Claim 19 words
A process according to claim 1, wherein said first pressure is in a range of 1 to 1.5 Torr.

References Cited (Backward Citations)

US4811684A Cited
US4960488A Cited
JPS63267430A Cited
US5207836A Cited
US5211796A Cited
JPH04214873A Cited
US5356478A Cited
US5286297A Cited
US5326723A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 2000-04-14 2000-10-14 2001-04-15 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2004-04-14 2004-10-14 2005-04-15 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2008-04-14 2008-10-14 2009-04-15 $7700.00 Window Closed / Lapsed

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