Patent US5453216A successfully refreshed from Google Patents.
US5453216A
Expired / Lapsed
US
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Delayed-release encapsulated warewashing composition and process of use
Assignee: Creative Products Resource Inc
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Filing: 1994-04-28
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Granted: 1995-09-26
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Expires: 2014-04-28
Abstract
Abstract A delayed-release composite particle is provided which comprises (a) a core particle comprising an inorganic detergent builder salt and an effective amount of at least one wash additive; and (b) a waxy coating encapsulating said core particle, which coating has a melting point of greater than about 65° C. and which chemically disintegrates in aqueous solution at a temperature of less than about 65° C. and a pH of above about 9.0.
Inventors
- 👤 George W. Kellett
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-29 11:06
CPC Classifications
C; C11; C11D; C11D3/00; C11D3/16; C11D3/20; C11D3/2075; C11D3/2079; C11D1/00; C11D1/66; C11D1/667; C11D1/72; C11D17/00; C11D17/0039
Claims Analysis
Total Claims: 29
Claim 1
Independent Claim
160 words
A delayed-release composite particle consisting essentially of: (a) a core particle comprising about 70-95 wt-% of an inorganic detergent builder salt and about 5-30 wt-% of a nonionic surfactant rinse aid; and (b) a waxy coating encapsulating said core particle, which coating comprises a major amount of not more than about 85 wt-% of a solid fatty acid or solid fatty acid blend and a minor amount of at least about 15 wt-% of a mixture of ethylene oxide esters of (C 16 -C 22 ) fatty acids having at least one ethylene oxide so that the coating has a melting point of greater than the operating temperature of the dishwashing machine and which chemically disintegrates in aqueous solution at a temperature of less than about 65° C. and at a pH of above about 9.0 wherein the core particle comprises about 75-99 wt-% of the composite particle and wherein the coating comprises about 1-25 wt-% of the composite particle.
Claim 2
Dependent Claim
160 words
A delayed-release composite particle consisting essentially of: (a) a core particle comprising about 70-95 wt-% of an inorganic detergent builder salt and about 5-30 wt-% of a nonionic surfactant rinse aid; and (b) a waxy coating encapsulating said core particle, which coating comprises a major amount of not more than about 85 wt-% of a solid fatty acid or solid fatty acid blend and a minor amount of at least about 15 wt-% of a mixture of ethylene oxide esters of (C 16 -C 22 ) fatty acids having at least one ethylene oxide so that the coating has a melting point of greater than the operating temperature of the dishwashing machine and which chemically disintegrates in aqueous solution at a temperature of less than about 65° C. and at a pH of above about 9.0 wherein the core particle comprises about 75-99 wt-% of the composite particle and wherein the coating comprises about 1-25 wt-% of the composite particle.
Claim 3
Dependent Claim
13 words
The composition of claim 1 wherein said particulate detergent further comprises an enzyme.
Claim 4
Independent Claim
219 words
A method of dishwashing comprising the steps of placing in an automatic dishwashing machine with soiled ware an effective amount of a composition comprising: (i) about 50-95% by weight of a particulate detergent capable of providing an alkaline washing solution having a pH greater than about 9.0 during a dishwashing cycle in said dishwashing machine; and (ii) about 5-50% by weight of composite particles consisting essentially of 77-99 wt-% of an inner core comprising a water soluble support matrix and a nonionic surfactant rinse aid, wherein said core is encapsulated by about 1-25 wt-% of a waxy coating comprising, a major amount of not more than about 85 wt-% of a solid fatty acid or solid fatty acid blend and a minor amount of at least about 15 wt-% of a mixture of ethylene oxide esters of (C 16 -C 22 ) fatty acids having at least one ethylene oxide so that the coating has a melting point greater than the operating temperature of said dishwashing machine, wherein said coating chemically disintegrates and is solubilized during said dishwashing cycle, thereby dissolving said core at a time later than the start of said dishwashing cycle, so that an effective amount of said rinse aid is delivered to the rinse cycle of said dishwashing machine; and (b) operating said dishwashing machine.
Claim 5
Independent Claim
219 words
A method of dishwashing comprising the steps of placing in an automatic dishwashing machine with soiled ware an effective amount of a composition comprising: (i) about 50-95% by weight of a particulate detergent capable of providing an alkaline washing solution having a pH greater than about 9.0 during a dishwashing cycle in said dishwashing machine; and (ii) about 5-50% by weight of composite particles consisting essentially of 77-99 wt-% of an inner core comprising a water soluble support matrix and a nonionic surfactant rinse aid, wherein said core is encapsulated by about 1-25 wt-% of a waxy coating comprising, a major amount of not more than about 85 wt-% of a solid fatty acid or solid fatty acid blend and a minor amount of at least about 15 wt-% of a mixture of ethylene oxide esters of (C 16 -C 22 ) fatty acids having at least one ethylene oxide so that the coating has a melting point greater than the operating temperature of said dishwashing machine, wherein said coating chemically disintegrates and is solubilized during said dishwashing cycle, thereby dissolving said core at a time later than the start of said dishwashing cycle, so that an effective amount of said rinse aid is delivered to the rinse cycle of said dishwashing machine; and (b) operating said dishwashing machine.
Claim 6
Dependent Claim
202 words
A composition suitable for use in a dishwashing machine, said composition comprising: (a) about 50-95% by weight of a particulate detergent capable of providing an alkaline washing solution having a pH greater than about 9.0 during a dishwashing cycle in said dishwashing machine; and (b) about 5-50% by weight of composite particles consisting essentially of about 77-99 wt-% of an inner core comprising a water soluble support matrix and a nonionic surfactant rinse aid, wherein said core is encapsulated by about 1-25 wt-% of a waxy coating comprising a major amount of not more than about 85 wt-% of a solid fatty acid or solid fatty acid blend and a minor amount of at least about 15 wt-% of a mixture of ethylene oxide esters of (C 16 -C 22 ) fatty acids having at least one ethylene oxide so that the coating has a melting point greater than the operating temperature of said dishwashing machine, wherein said coating chemically disintegrates and is solubilized during said dishwashing cycle, thereby dissolving said core at a time later than the start of said dishwashing cycle, so that an effective amount of said rinse aid is delivered to the rinse cycle of said dishwashing machine.
Claim 7
Dependent Claim
202 words
A composition suitable for use in a dishwashing machine, said composition comprising: (a) about 50-95% by weight of a particulate detergent capable of providing an alkaline washing solution having a pH greater than about 9.0 during a dishwashing cycle in said dishwashing machine; and (b) about 5-50% by weight of composite particles consisting essentially of about 77-99 wt-% of an inner core comprising a water soluble support matrix and a nonionic surfactant rinse aid, wherein said core is encapsulated by about 1-25 wt-% of a waxy coating comprising a major amount of not more than about 85 wt-% of a solid fatty acid or solid fatty acid blend and a minor amount of at least about 15 wt-% of a mixture of ethylene oxide esters of (C 16 -C 22 ) fatty acids having at least one ethylene oxide so that the coating has a melting point greater than the operating temperature of said dishwashing machine, wherein said coating chemically disintegrates and is solubilized during said dishwashing cycle, thereby dissolving said core at a time later than the start of said dishwashing cycle, so that an effective amount of said rinse aid is delivered to the rinse cycle of said dishwashing machine.
Claim 8
Dependent Claim
39 words
The composite particle of claim 1 wherein the mixture of ethylene oxide esters of (C 16 -C 22 )fatty acids comprises a mixture of the monoethylene oxide ester of stearic acid and a polyethylene oxide ester of stearic acid.
Claim 9
Dependent Claim
15 words
The composite particle of claim 1 wherein the inorganic detergent builder salt is sodium tripolyphosphate.
Claim 10
Dependent Claim
26 words
The composite particle of claim 1 wherein the nonionic surfactant rinse aid is a polyethylene oxide ether of a (C 8 -C 22 ) fatty alcohol.
Claim 11
Dependent Claim
15 words
The composite particle of claim 1 wherein the core particle further comprises about 5-10% polyvinylpyrrolidone.
Claim 12
Dependent Claim
105 words
A delayed-release composite particle comprising: (a) a core particle comprising about 85-97.5 wt-% of the composite particle, wherein said core particle comprises about 70-95% of a water-soluble support matrix and about 5-30% of at least one wash additive; and (b) a waxy coating encapsulating said core particle which comprises about 70-85% of a blend of (C 18 -C 36 ) fatty acids having a melting point range of about 70°-75° C. and about 15-30% of a mixture of the monoethylene oxide ester of a (C 16 -C 22 ) fatty acid and the polyethylene oxide ester of a (C 16 -C 22 ) fatty acid.
Claim 13
Dependent Claim
105 words
A delayed-release composite particle comprising: (a) a core particle comprising about 85-97.5 wt-% of the composite particle, wherein said core particle comprises about 70-95% of a water-soluble support matrix and about 5-30% of at least one wash additive; and (b) a waxy coating encapsulating said core particle which comprises about 70-85% of a blend of (C 18 -C 36 ) fatty acids having a melting point range of about 70°-75° C. and about 15-30% of a mixture of the monoethylene oxide ester of a (C 16 -C 22 ) fatty acid and the polyethylene oxide ester of a (C 16 -C 22 ) fatty acid.
Claim 14
Dependent Claim
16 words
The composite particle of claim 9 wherein the support matrix comprises an inorganic detergent builder salt.
Claim 15
Dependent Claim
16 words
The composite particle of claim 9 wherein the wash additive comprises a nonionic surfactant rinse aid.
Claim 16
Dependent Claim
29 words
The composite particle of claim 11 wherein the wash additive comprises the condensation product of about 35-40 moles of ethylene oxide with a (C 8 -C 22 ) alkanol.
Claim 17
Dependent Claim
15 words
The composite particle of claim 12 wherein the core particle comprises about 0.05-10% of polyvinylpyrrolidone.
Claim 18
Dependent Claim
12 words
The composition of claim 4 wherein said core further comprises a bleach.
Claim 19
Dependent Claim
14 words
The composition of claim 4 wherein said support matrix comprises an inorganic builder salt.
Claim 20
Dependent Claim
17 words
The composition claim 4 wherein said waxy coating has a melting point of above about 60° C.
Claim 21
Dependent Claim
14 words
The composition of claim 4 wherein said particulate detergent comprises an inorganic builder salt.
Claim 22
Dependent Claim
12 words
The composition of claim 15 wherein said support matrix comprises sodium tripolyphosphate.
Claim 23
Dependent Claim
22 words
The composition of claim 4 wherein said coating comprises a plurality of fatty acids having a melting point of about 60°-65° C.
Claim 24
Dependent Claim
17 words
The composition of claim 4 wherein said fatty acids have a carbon chain length of about 18-36,
Claim 25
Dependent Claim
17 words
The composition of claim 4 wherein said coating further comprises a plurality of ethylene glycol stearate esters.
Claim 26
Dependent Claim
17 words
The composition of claim 4 wherein said coating has a melting point greater than about 65° C.
Claim 27
Dependent Claim
16 words
The composition of claim 22 wherein said melting is about 70° C. to about 75° C.
Claim 28
Dependent Claim
18 words
The composition of claim 4 wherein said rinse aid comprises an ethylene oxide ether of a fatty alcohol,
Claim 29
Dependent Claim
11 words
The composition of claim 24 wherein said core further comprises polyvinylpyrrolidone.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1998-09-25 | 1999-03-27 | 1999-09-26 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 2002-09-25 | 2003-03-27 | 2003-09-26 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2006-09-25 | 2007-03-27 | 2007-09-26 | $7700.00 | Window Closed / Lapsed |