US5413759A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Plasma sterilizer and method
Assignee: DePuy Orthopaedics Inc
•
Filing: 1993-06-07
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Granted: 1995-05-09
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Expires: 2013-06-07
Abstract
Abstract A method for plasma sterilization includes exposing an article to be sterilized to a plasma generated from a gas mixture. The gas mixture being either (a) argon, helium, nitrogen, or mixtures thereof, and oxygen and hydrogen; (b) argon, helium, nitrogen or mixtures thereof, and hydrogen; or (c) argon, helium, nitrogen or mixtures thereof, and oxygen. The exposure of the article to the plasma is carried out at a pressure of from 0.1 to 10 torr and a chamber temperature of less than 63° C. for a time period sufficient to effect sterilization. Contaminated articles can be pretreated in a plasma generated from oxygen and optionally argon, helium and/or nitrogen at the same conditions for up to 5 minutes to remove protein. The apparatus for plasma sterilization of articles includes a plasma generator and a sterilizing chamber. The plasma generator includes a plurality of generator tubes positioned in one or more electromagnetic field zones defined by one or more waveguides. The outlet of the generator tube preferably has a restriction for maintaining the gas pressure in the plasma generating chamber at from 0.3 to 10 torr.
Inventors
- 👤 Bryant A. Campbell
- 👤 Kern A. Moulton
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-02 10:28
CPC Classifications
A; A61; A61L; A61L2/00; A61L2/02; A61L2/14; H; H05; H05H; H05H1/00; H05H1/24; H05H1/46; Y; Y10; Y10S; Y10S422/00; Y10S422/906
Claims Analysis
Total Claims: 10
Claim 1
Independent Claim
88 words
A method for plasma sterilization comprising generating a plasma in a plasma generating chamber, passing said plasma from said plasma generating chamber via a restriction means and a plasma distribution means to a sterilizing chamber, effecting sterilization in said sterilizing chamber by exposing to the plasma in said sterilizing chamber for a time period sufficient to effect sterilization, wherein said restriction means and said plasma distribution means provide an indirect passageway which prevents direct impingement of nascent plasma generated in said plasma generating chamber into said sterilizing chamber.
Claim 2
Independent Claim
88 words
A method for plasma sterilization comprising generating a plasma in a plasma generating chamber, passing said plasma from said plasma generating chamber via a restriction means and a plasma distribution means to a sterilizing chamber, effecting sterilization in said sterilizing chamber by exposing to the plasma in said sterilizing chamber for a time period sufficient to effect sterilization, wherein said restriction means and said plasma distribution means provide an indirect passageway which prevents direct impingement of nascent plasma generated in said plasma generating chamber into said sterilizing chamber.
Claim 3
Dependent Claim
30 words
The method of claim 1 wherein the plasma is generated from a gas mixture containing from 1 to 10 (v/v) % oxygen and from 3 to 7 (v/v) % hydrogen.
Claim 4
Dependent Claim
34 words
The method of claim 1 wherein an article is contained within said sterilizing chamber and the article is enclosed in a porous container, and the container is surrounded by the plasma during the treatment.
Claim 5
Dependent Claim
49 words
A method for plasma sterilization as in claim 1, wherein: said plasma is generated from a mixture of gases comprising a first component consisting of oxygen or hydrogen or a mixture there of and a second component consisting of one or more of argon, helium, nitrogen or mixtures thereof.
Claim 6
Dependent Claim
27 words
The method of claim 4 wherein the mixture consists of about 5 (v/v) % hydrogen and about 95 (v/v) % argon, helium, nitrogen or a mixture thereof.
Claim 7
Dependent Claim
41 words
A method for plasma sterilization as in claim 1, wherein: said plasma is generated from a mixture of gases consisting of from 10 to 40 (v/v) % oxygen; and from 60 to 90 (v/v) % argon, helium, nitrogen, or mixtures thereof.
Claim 8
Dependent Claim
12 words
The method of claim 6 wherein the mixture of gases is air.
Claim 9
Independent Claim
78 words
A method for plasma sterilization comprising: generating a plasma in a plasma generating chamber; and flowing said plasma from said plasma generating chamber via a restriction means and a plasma distribution means into another chamber and maintaining the flow for a time period sufficient to effect sterilization therein, wherein said restriction means and said plasma distribution means provide an indirect passageway which prevents direct impingement of nascent plasma generated in said plasma generating chamber onto said another chamber.
Claim 10
Independent Claim
78 words
A method for plasma sterilization comprising: generating a plasma in a plasma generating chamber; and flowing said plasma from said plasma generating chamber via a restriction means and a plasma distribution means into another chamber and maintaining the flow for a time period sufficient to effect sterilization therein, wherein said restriction means and said plasma distribution means provide an indirect passageway which prevents direct impingement of nascent plasma generated in said plasma generating chamber onto said another chamber.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1998-05-08 | 1998-11-07 | 1999-05-09 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 2002-05-08 | 2002-11-07 | 2003-05-09 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2006-05-08 | 2006-11-07 | 2007-05-09 | $7700.00 | Window Closed / Lapsed |