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US5344480A Expired / Lapsed US ⏱️ 0.0 years remaining

Pressurizing with and recovering helium

Assignee: Praxair Technology Inc
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Filing: 1993-04-21
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Granted: 1994-09-06
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Expires: 2013-04-21
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Abstract

Abstract A process and system for pressurizing a vessel for integrity testing with gas comprising helium, recovering the gas comprising helium, and purifying the gas comprising helium for reuse. The process for purifying the gas stream comprising helium comprises drying the gas stream; separating the dried gas stream in a membrane separator stage into a helium-enriched permeate product stream and a helium-depleted raffinate stream; recovering helium in the raffinate stream in a membrane stripper stage thereby producing a purge stream; and purging water from the dryer with the purge stream.

Inventors

  • 👤 Thomas R. Schulte
  • 👤 Carl J. Heim
  • 👤 Vladimir T. Gorjaczkowski
  • 👤 Salvatore Giglia

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-07 00:45
CPC Classifications
G; G01; G01M; G01M3/00; G01M3/02; G01M3/04; G01M3/20; G01M3/202; B; B01; B01D; B01D53/00; B01D53/22; B01D53/225; B01D53/226; B01D53/229; C; C01; C01B; C01B23/00

Claims Analysis

Total Claims: 15
Claim 1
Independent Claim 75 words
A process for purifying a gas stream comprising helium and air constituents, said process comprising: (a) drying the gas stream in a fluid stream dryer; (b) separating the dried gas stream in a membrane separator stage into a helium-enriched permeate product stream and a helium-depleted raffinate stream; (c) recovering helium in said raffinate stream in a membrane stripper stage thereby producing a purge stream; and (d) purging water from said dryer with said purge stream.
Claim 2
Dependent Claim 75 words
A process for purifying a gas stream comprising helium and air constituents, said process comprising: (a) drying the gas stream in a fluid stream dryer; (b) separating the dried gas stream in a membrane separator stage into a helium-enriched permeate product stream and a helium-depleted raffinate stream; (c) recovering helium in said raffinate stream in a membrane stripper stage thereby producing a purge stream; and (d) purging water from said dryer with said purge stream.
Claim 3
Dependent Claim 20 words
The process as in claim 1 further comprising compressing said gas stream comprising helium prior to drying said gas stream.
Claim 4
Dependent Claim 58 words
The process as in claim 2 wherein said recovering helium from the raffinate stream in said membrane stripper stage comprises producing a permeate stream as a purge stream, and said process further comprises adding the purge stream after it has purged water from said dryer into the stream of gas comprising helium prior to compressing said gas stream.
Claim 5
Dependent Claim 52 words
The process as in claim 2 wherein said recovering helium from the raffinate stream in said membrane stripper stage comprises producing a raffinate stream as a purge stream, producing a helium-enriched permeate stream, and adding the helium-enriched permeate stream into the stream of gas comprising helium prior to compressing said gas stream.
Claim 6
Dependent Claim 34 words
The process as in claim 1 wherein said dryer comprises a membrane dryer and the purge stream sweeps the permeate side of the membrane dryer to maintain permeation of moisture from the gas stream.
Claim 7
Dependent Claim 42 words
The process as in claim 1 wherein said dryer comprises at least two switchable adsorbent beds, one of said beds serving to dry the gas stream, while the other of said beds is regenerated or desorbed of water by the purge stream.
Claim 8
Dependent Claim 34 words
The process as in claim 1 for purifying gas comprising helium and air constituents, said gas entering or contained in a tank for supplying gas comprising helium to a vessel for integrity testing thereof.
Claim 9
Dependent Claim 146 words
A helium purification system for purifying a gas stream comprising helium and air constituents including water, said system comprising: (a) a fluid stream dryer having: a port for receiving a moisture-rich stream; a port for discharging a moisture-depleted stream; a port for receiving a moisture-depleted purge stream for purging moisture from said dryer; and a port for discharging a moisture-enriched purge stream; and (b) a membrane separator having: an inlet for receiving a gas stream comprising helium, said inlet communicating with said dryer port for discharging said moisture-depleted stream; a permeate outlet for discharging a helium-enriched permeate stream; and a raffinate outlet for discharging a helium-depleted raffinate stream; and (c) a membrane stripper having: an inlet communicating with the raffinate outlet of said membrane separator; and an outlet for discharging a purge stream, said outlet communicating with said dryer port for receiving said moisture-depleted purge stream.
Claim 10
Dependent Claim 146 words
A helium purification system for purifying a gas stream comprising helium and air constituents including water, said system comprising: (a) a fluid stream dryer having: a port for receiving a moisture-rich stream; a port for discharging a moisture-depleted stream; a port for receiving a moisture-depleted purge stream for purging moisture from said dryer; and a port for discharging a moisture-enriched purge stream; and (b) a membrane separator having: an inlet for receiving a gas stream comprising helium, said inlet communicating with said dryer port for discharging said moisture-depleted stream; a permeate outlet for discharging a helium-enriched permeate stream; and a raffinate outlet for discharging a helium-depleted raffinate stream; and (c) a membrane stripper having: an inlet communicating with the raffinate outlet of said membrane separator; and an outlet for discharging a purge stream, said outlet communicating with said dryer port for receiving said moisture-depleted purge stream.
Claim 11
Dependent Claim 41 words
The system as in claim 8 further comprising compressing means, said compressing means having an inlet for receiving said gas stream comprising helium and air constituents including water and an outlet communicating with said dryer port for receiving said moisture-rich stream.
Claim 12
Dependent Claim 49 words
The system as in claim 9 wherein said dryer port for discharging said moisture-enriched purge stream communicates with said compressing means inlet, said membrane stripper outlet for discharging said purge stream comprises a permeate outlet, and said membrane stripper further comprises a raffinate outlet communicating externally of said system.
Claim 13
Dependent Claim 49 words
The system as in claim 9 wherein said dryer port for discharging said moisture-enriched purge stream communicates externally of said system, said membrane stripper outlet for discharging said purge stream comprises a raffinate outlet, and said membrane stripper further comprises a permeate outlet communicating with said compressing means inlet.
Claim 14
Dependent Claim 54 words
The system as in claim 9 wherein said dryer comprises a membrane dryer and said port for receiving said moisture-depleted purge stream and said port for discharging said moisture-enriched purge stream comprise means for sweeping the permeate side of the membrane dryer to maintain a rate of permeation of moisture from the moisture-rich stream.
Claim 15
Dependent Claim 51 words
The system as in claim 9 wherein said dryer comprises at least two switchable adsorbent beds, one of said beds serving to dry the moisture-rich stream during its adsorbing period, while the other of said beds is regenerated or desorbed of water during its desorbing period by said moisture-depleted purge stream.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1997-09-05 1998-03-07 1998-09-06 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2001-09-05 2002-03-07 2002-09-06 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2005-09-05 2006-03-07 2006-09-06 $7700.00 Window Closed / Lapsed

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