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US5310583A Expired / Lapsed US ⏱️ 0.0 years remaining

Vapor phase deposition of hydrogen silsesquioxane resin in the presence of nitrous oxide

Assignee: Dow Silicones Corp
•
Filing: 1992-11-02
•
Granted: 1994-05-10
•
Expires: 2012-11-02
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Abstract

Abstract Silicon and oxygen containing coatings are deposited by the chemical vapor deposition of hydrogen silsesquioxane in an environment comprising nitrous oxide.

Inventors

  • 👤 Marie N. Eckstein
  • 👤 David S. Ballance

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-04 14:38
CPC Classifications
C; C23; C23C; C23C16/00; C23C16/22; C23C16/30; C23C16/40; C23C16/401

Claims Analysis

Total Claims: 14
Claim 1
Independent Claim 44 words
A method of depositing a coating containing silicon and oxygen on a substrate comprising: introducing a gas comprising hydrogen silsesquioxane into a deposition chamber containing the substrate and a reactive environment comprising nitrous oxide; and inducing reaction of the gas to form the coating.
Claim 2
Independent Claim 44 words
A method of depositing a coating containing silicon and oxygen on a substrate comprising: introducing a gas comprising hydrogen silsesquioxane into a deposition chamber containing the substrate and a reactive environment comprising nitrous oxide; and inducing reaction of the gas to form the coating.
Claim 3
Dependent Claim 30 words
The method of claim 1 wherein the hydrogen silsesquioxane comprises a sample in which greater than about 75 % of the species have a molecular weight less than about 2000.
Claim 4
Dependent Claim 30 words
The method of claim 1 wherein the hydrogen silsesquioxane comprises a sample in which greater than about 75 % of the species have a molecular weight less than about 1200.
Claim 5
Dependent Claim 32 words
The method of claim 1 wherein the hydrogen silsesquioxane comprises a sample in which greater than about 75 % of the species have a molecular weight between about 400 and about 1000.
Claim 6
Dependent Claim 15 words
The method of claim 1 wherein the hydrogen silsesquioxane is diluted in a carrier gas.
Claim 7
Dependent Claim 46 words
The method of claim 1 wherein the hydrogen silsesquioxane is induced to react by a means selected from the group consisting of chemical vapor deposition, low pressure chemical vapor deposition, subatmospheric chemical vapor deposition, plasma enhanced chemical vapor deposition, electron cyclotron resonance, and jet vapor deposition.
Claim 8
Dependent Claim 19 words
The method of claim 1 wherein the hydrogen silsesquioxane is induced to react by exposure to an elevated temperature.
Claim 9
Dependent Claim 18 words
The method of claim 7 in which the temperature is in the range of about 100 °-1OOO° C.
Claim 10
Dependent Claim 19 words
The method of claim 1 wherein the hydrogen silsesquioxane resin is induced to react by exposure to a plasma.
Claim 11
Dependent Claim 16 words
The method of claim 9 in which the plasma comprises radio frequency energy or microwave energy.
Claim 12
Dependent Claim 32 words
The method of claim 1 wherein the deposition chamber is maintained at a pressure of less than about (5) torr and a temperature in the range of about (100° to 1200)° C.
Claim 13
Dependent Claim 32 words
The method of claim 1 wherein the deposition chamber is maintained at a pressure of less than about 1 atmosphere and a temperature in the range of about (100° to 1200)° C.
Claim 14
Dependent Claim 12 words
The method of claim 1 wherein the substrate comprises an electronic device.

References Cited (Backward Citations)

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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1997-05-09 1997-11-08 1998-05-10 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2001-05-09 2001-11-08 2002-05-10 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2005-05-09 2005-11-08 2006-05-10 $7700.00 Window Closed / Lapsed

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