US5279783A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for manufacture of polyamide monofilament suture
Assignee: UNITED SATES SURGICAL Corp
•
Filing: 1992-01-30
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Granted: 1994-01-18
•
Expires: 2012-01-30
Abstract
Abstract A process for manufacturing polyamide monofilament suture includes the steps of extruding a polyamide resin, stretching the solidified monofilament and annealing the stretched monofilament so that it shrinks to within about 80 to about 97 percent of the length of the monofilament prior to annealing. The polyamide monofilament sutures so produced exhibit reduced energy compared to conventional polyamide monofilament sutures.
Inventors
- 👤 Cheng-Kung Liu
- 👤 John C. Brewer
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-03 08:33
CPC Classifications
A; A61; A61L; A61L17/00; A61L17/04; A61L17/14; D; D01; D01F; D01F6/00; D01F6/58; D01F6/60
Claims Analysis
Total Claims: 16
Claim 1
Independent Claim
176 words
A process for manufacturing a polyamide monofilament suture exhibiting reduced energy and/or increased knot security which comprises the operations of extruding a polyamide resin at an extrusion temperature of from about 215° to about 275° C. to provide a monofilament, stretching the solidified monofilament at a temperature of from about 40° to about 98° C. in liquid medium or at from about 50° to about 185° C. in gaseous medium at a stretch ratio of from about 3:1 to about 5:1 to provide a stretched monofilament and annealing the stretched monofilament at a temperature of from about 100° to about 180° C. to provide the finished suture, the annealing resulting in shrinkage of the stretched monofilament for a recovery to within about 80 to about 97 percent of the length of the monofilament prior to annealing, the finished suture exhibiting reduced energy and/or increased knot security compared with the energy and/or knot strength of a suture of equivalent size obtained by a process which omits or deviates significantly from one or more of the foregoing operations.
Claim 2
Dependent Claim
176 words
A process for manufacturing a polyamide monofilament suture exhibiting reduced energy and/or increased knot security which comprises the operations of extruding a polyamide resin at an extrusion temperature of from about 215° to about 275° C. to provide a monofilament, stretching the solidified monofilament at a temperature of from about 40° to about 98° C. in liquid medium or at from about 50° to about 185° C. in gaseous medium at a stretch ratio of from about 3:1 to about 5:1 to provide a stretched monofilament and annealing the stretched monofilament at a temperature of from about 100° to about 180° C. to provide the finished suture, the annealing resulting in shrinkage of the stretched monofilament for a recovery to within about 80 to about 97 percent of the length of the monofilament prior to annealing, the finished suture exhibiting reduced energy and/or increased knot security compared with the energy and/or knot strength of a suture of equivalent size obtained by a process which omits or deviates significantly from one or more of the foregoing operations.
Claim 3
Dependent Claim
79 words
The process of claim 1 wherein extruding is carried out at from about 220° to about 250° C., stretching is carried out at from about 60° to about 98° C. in liquid medium or at from about 100° to about 170° C. in gaseous medium at a stretch ratio of from about 3.5:1 to about 4.5:1 and annealing is carried out at from about 120° to about 180° C. with recovery to within about 85 to about 95 percent.
Claim 4
Dependent Claim
34 words
The process of claim 1 wherein the polyamide possesses a number average molecular weight of at least about 15,000 and a melt flow index in g/10 min of from about 3 to about 8.
Claim 5
Dependent Claim
23 words
The process of claim 1 wherein the polyamide possesses a melt flow index in g/10 min of from about 4 to about 6.
Claim 6
Dependent Claim
15 words
The process of claim 1 wherein the polyamide is a polycaprolactam or a polyhexamethylene adipamide.
Claim 7
Dependent Claim
41 words
The process of claim 1 wherein the polyamide is a polycaprolactam or a polyhexamethylene adipamide possessing a number average molecular weight of at least about 15,000 and a melt flow index in g/10 min of from about 3 to about 8.
Claim 8
Dependent Claim
29 words
The process of claim 1 wherein the polyamide is a polycaprolactam or polyhexamethylene adipamide possessing a melt flow index in g/10 min of from about 4 to about 6.
Claim 9
Dependent Claim
36 words
The process of claim 1 wherein for suture sizes of 3/0 and larger, the stretching operation is accomplished by passing the solidified monofilament through water at a temperature of from about 60° to about 98° C.
Claim 10
Dependent Claim
36 words
The process of claim 1 wherein for suture sizes of 3/0 and larger, the stretching operation is accomplished by passing the solidified monofilament through water at a temperature of from about 80° to about 95° C.
Claim 11
Dependent Claim
36 words
The process of claim 1 wherein for suture sizes of 4/0 and smaller, the stretching operation is accomplished by passing the solidified monofilament through air at a temperature of from about 100° to about 185° C.
Claim 12
Dependent Claim
36 words
The process of claim 1 wherein for suture sizes of 4/0 and smaller, the stretching operation is accomplished by passing the solidified monofilament through air at a temperature of from about 150° to about 170° C.
Claim 13
Dependent Claim
52 words
The process of claim 1 wherein the annealing operation is carried out at a temperature of from about 140° to about 180° C., the annealing resulting in shrinkage of the stretched monofilament for a recovery to within about 85 to about 97 percent of the length of the monofilament prior to annealing.
Claim 14
Dependent Claim
52 words
The process of claim 1 wherein the annealing operation is carried out at a temperature of from about 140° to about 170° C., the annealing resulting in shrinkage of the stretched monofilament for a recovery to within about 93 to about 100 percent of the length of the monofilament prior to annealing.
Claim 15
Dependent Claim
112 words
The process of claim 1 wherein the polyamide is a polycaprolactam or a polyhexamethylene adipamide, the extruding operation is carried out at a temperature of from about 215° to about 275° C., the stretching operation is carried out at a temperature of from about 60° to about 98° C. in water or at from about 100° to about 185° C. in air and a stretch ratio of from about 3.5:1 to about 5:1 and the annealing operation is carried out at a temperature of from about 120° to about 180° C. to provide a recovery to within about 85 to about 97 percent of the length of the monofilament prior to annealing.
Claim 16
Dependent Claim
110 words
The process of claim 1 wherein the polyamide is a polycaprolactam or a polyhexamethylene adipamide, the extruding operation is carried out at a temperature of from about 220° to about 250° C., the stretching operation is carried out at a temperature of from about 80° to about 95° in water or from about 150° to about 170° C. in air and a stretch ratio of from about 3.5:1 to about 4.5:1 and the annealing operation is carried out at a temperature of from about 140° to about 170° C. to provide a recovery to within about 93 to about 95 percent of the length of the monofilament prior to annealing.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1997-01-17 | 1997-07-19 | 1998-01-18 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 2001-01-17 | 2001-07-19 | 2002-01-18 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2005-01-17 | 2005-07-19 | 2006-01-18 | $7700.00 | Window Closed / Lapsed |