← Back to Patent Explorer
US5259147A Expired / Lapsed US ⏱️ 0.0 years remaining

Granular abrasive material

Assignee: Imerys Fused Minerals Laufenburg GmbH
•
Filing: 1993-02-18
•
Granted: 1993-11-09
•
Expires: 2013-02-18
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract A granular abrasive material is produced from a dispersion consisting of raw materials containing alumina, compounds containing silica and other additives. The dispersion is ground to a sinterable slip with a grain size of less than 1 micrometer. The slip is dried and may be pressed before being subjected to a multi-stage heating process to produce sintered corundum crystals.

Inventors

  • 👤 Wolfgang Falz
  • 👤 Gunter Bigorajski
  • 👤 Herbert Exner

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 06:28
CPC Classifications
C; C09; C09K; C09K3/00; C09K3/14; C09K3/1409; C09K3/1418; Y; Y10; Y10T; Y10T428/00; Y10T428/24; Y10T428/24355; Y10T428/24372; Y10T428/24413

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 219 words
A method for producing granular abrasive material including the steps of: forming a dispersion of solid materials containing alumina, compounds containing silica, and other additives selected from compounds of the metals; silicon, zirconium, titanium, chromium, iron, magnesium, zinc, cobalt or nickel, in water and/or an organic compound, said dispersion containing sufficient alumina to provide a content of at least fifty-five weight percent alpha-aluminum oxide in the produced granular abrasive materials; grinding said solid materials of said dispersion until said solid materials of said dispersion are reduced to particles of which substantially all have a particle size of less than 0.1 micrometer to produce a sinterable slip; drying the ground dispersion of said solid material; and subjecting said dried dispersion to at least a two stage heat treatment including a first stage wherein said dried dispersion is preheated to between 250° and 600° C. for the expulsion of chemically bound water and/or organic compounds, and a subsequent stage wherein said preheated dried dispersion is heated to between 1400° and 1700° C. to sinter it to a density of more than eighty-five percent of the theoretical density of corundum such as to produce said granular abrasive material comprising both alpha-aluminum oxide and a silicate material and wherein the diameters of the crystals of said alpha-aluminum oxide are less than one micrometer.
Claim 2
Independent Claim 219 words
A method for producing granular abrasive material including the steps of: forming a dispersion of solid materials containing alumina, compounds containing silica, and other additives selected from compounds of the metals; silicon, zirconium, titanium, chromium, iron, magnesium, zinc, cobalt or nickel, in water and/or an organic compound, said dispersion containing sufficient alumina to provide a content of at least fifty-five weight percent alpha-aluminum oxide in the produced granular abrasive materials; grinding said solid materials of said dispersion until said solid materials of said dispersion are reduced to particles of which substantially all have a particle size of less than 0.1 micrometer to produce a sinterable slip; drying the ground dispersion of said solid material; and subjecting said dried dispersion to at least a two stage heat treatment including a first stage wherein said dried dispersion is preheated to between 250° and 600° C. for the expulsion of chemically bound water and/or organic compounds, and a subsequent stage wherein said preheated dried dispersion is heated to between 1400° and 1700° C. to sinter it to a density of more than eighty-five percent of the theoretical density of corundum such as to produce said granular abrasive material comprising both alpha-aluminum oxide and a silicate material and wherein the diameters of the crystals of said alpha-aluminum oxide are less than one micrometer.
Claim 3
Dependent Claim 20 words
A method according to claim 1, wherein said sinterable slip is compacted in a press prior to said heat treatment.
Claim 4
Dependent Claim 25 words
A method according to claim 1, wherein said materials containing alumina are selected from the group consisting of calcined alumina, aluminium hydroxides, and mixtures thereof.
Claim 5
Dependent Claim 53 words
A method according to claim 1, wherein said heat treatment comprises three stages and includes a second stage intermediate said first stage and said subsequent stage, said second stage including heating said preheated slip to between 1100° and 1400° C. and maintaining this temperature for a period of from ten to thirty minutes.
Claim 6
Dependent Claim 26 words
A method according to claim 4, wherein in the finished granular abrasive material the proportion of said silicate phase is from 0.3 to 10% by weight.
Claim 7
Dependent Claim 34 words
A method according to claim 4, wherein said abrasive granular material includes further simple or complex metal oxides dissolved or dispersed in the corundum matrix in addition to said alpha-aluminium oxide and silicate phase.
Claim 8
Dependent Claim 20 words
A method according to claim 6, wherein the proportion of said metal oxides is from 0.2 to 45% by weight.
Claim 9
Dependent Claim 20 words
A method according to claim 5, wherein said silicate phase in said finished granular abrasive material is present as glass.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1996-11-08 1997-05-10 1997-11-09 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2000-11-08 2001-05-10 2001-11-09 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2004-11-08 2005-05-10 2005-11-09 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag