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US5211801A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for manufacturing single-crystal silicon carbide

Assignee: Infineon Technologies AG
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Filing: 1991-07-15
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Granted: 1993-05-18
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Expires: 2011-07-15
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Abstract

Abstract Single crystals of silicon carbide (SiC) can be manufactured by subliming and partially decomposing a base material of crystalline silicon carbide powder and by growing the single crystals from seed crystals. According to the present invention, an excess of silicon is added to the silicon carbide base material. Using this technique, high purity, single-crystal silicon carbide is obtained.

Inventors

  • 👤 Rene Stein

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-03 17:53
CPC Classifications
C; C30; C30B; C30B23/00; C30B29/00; C30B29/10; C30B29/36

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 81 words
A method for the growth of single-crystal silicon carbide in a reaction vessel having a protective atmosphere and a small temperature gradient in the direction of growth, comprising: adding excess silicon to a crystalline silicon carbide powder; subliming and partially decomposing the crystalline silicon carbide powder; and growing, on a seed crystal, single crystals of silicon carbide from the sublimed and partially decomposed crystalline silicon carbide powder; wherein said excess silicon is in an amount of from about 0.1% to 5%.
Claim 2
Independent Claim 81 words
A method for the growth of single-crystal silicon carbide in a reaction vessel having a protective atmosphere and a small temperature gradient in the direction of growth, comprising: adding excess silicon to a crystalline silicon carbide powder; subliming and partially decomposing the crystalline silicon carbide powder; and growing, on a seed crystal, single crystals of silicon carbide from the sublimed and partially decomposed crystalline silicon carbide powder; wherein said excess silicon is in an amount of from about 0.1% to 5%.
Claim 3
Dependent Claim 25 words
The method for the manufacture of single-crystal silicon carbide as recited in claim 1, wherein the crystalline silicon carbide powder is manufactured from highly-purified silicon.
Claim 4
Dependent Claim 39 words
The method for the manufacture of single-crystal silicon carbide as recited in claim 1, wherein the crystalline silicon carbide powder is industrial silicon carbide and the method further comprises purifying the industrial silicon carbide before adding the excess silicon.
Claim 5
Dependent Claim 25 words
The method for the manufacture of single-crystal silicon carbide as recited in claim 1, wherein the excess silicon is added in a finely dispersed form.
Claim 6
Dependent Claim 28 words
The method for the manufacture of single-crystal silicon carbide as recited in claim 1 wherein the crystalline silicon carbide powder has a molar Si:C ratio greater than 1.
Claim 7
Dependent Claim 28 words
The method for the manufacture of single-crystal silicon carbide as recited in claim 1, wherein said excess silicon is in an amount of from about 1% to 2%.

References Cited (Backward Citations)

US2854364A Cited
US3359077A Cited
US4147572A Cited
US4298423A Cited
US4623425A Cited
US4756895A Cited
JPH02128913A Cited
JPH02128912A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1996-05-17 1996-11-16 1997-05-18 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2000-05-17 2000-11-16 2001-05-18 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2004-05-17 2004-11-16 2005-05-18 $7700.00 Window Closed / Lapsed

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