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US5178689A Expired / Lapsed US ⏱️ 0.0 years remaining

Fe-based soft magnetic alloy, method of treating same and dust core made therefrom

Assignee: Toshiba Corp
•
Filing: 1991-06-05
•
Granted: 1993-01-12
•
Expires: 2011-06-05
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Abstract

Abstract Fe-based soft magnetic alloy having excellent soft magnetic characteristics with high saturated magnetic flux density, characterized in that it has fine crystal grains dispersed in an amorphous phase and is expressed by the general formula: Fe.sub.100-a-b-c Cu.sub.a M.sub.b Y.sub.c where: "M" is at least one or more selected from elements of groups IVa, Va, VIa of the periodic table, Mn, Co, Ni, Al, and the Platinum group, "Y" is at least one or more selected from Si, B, P, or C and 3<a≦8 (atomic %) 0.1<b≦8 3.1≦a+b≦12 15≦c≦28. Also described is a dust core made from an alloy powder having fine crystal grains dispersed in an amorphous phase and expressed by the formula Fe.sub.100-a-b-c-d-e Cu.sub.a M'.sub.b M".sub.c Si.sub.d B.sub.e where: "M'" is at least one element selected from the groups consisting of Group IVa, Va, VIa of the periodic table; "M"" is at least one element from the group consisting of Mn, Co, Ni, Al, and the Platinum group; and wherein "a", "b", "c", "d" and "e", expressed in atomic %, are as follows: 3<b≦8 0.1<b≦8 0≦c≦15 8≦d≦22 3≦e≦15 15≦d+e≦28. A method of treating the alloy to separate the fine crystal grains is also described which comprises heat treating said alloy for from one minute to ten hours at a temperature of from 50° C. below the crystallization temperature to 120° C. above the crystallization temperature.

Inventors

  • 👤 Masami Okamura
  • 👤 Takao Sawa

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-10 01:11
CPC Classifications
H; H01; H01F; H01F1/00; H01F1/01; H01F1/03; H01F1/12; H01F1/14; H01F1/147; H01F1/153; H01F1/15308; C; C22; C22C; C22C45/00; C22C45/02

Claims Analysis

Total Claims: 32
Claim 1
Independent Claim 94 words
An Fe-based soft magnetic alloy having fine crystal grains dispersed in an amorphous phase and as described in the following formula: Fe.sub.100-a-b-c Cu.sub.a M.sub.b Y.sub.c ; where "M" is at least one element selected from the group consisting of Ti, Zr, Hf, V, Nb, Ta, Cr, Mo, W of the periodic table, Mn, Co, Ni, Al and the Platinum group; "Y" is at least one element selected form the group consisting of Si, B, P, and C; and wherein "a", "b", and "c", expressed in atomic % are as follows: 3<a≦8 0.1<b≦8 3.1≦a+b≦12 15≦c≦28.
Claim 2
Dependent Claim 94 words
An Fe-based soft magnetic alloy having fine crystal grains dispersed in an amorphous phase and as described in the following formula: Fe.sub.100-a-b-c Cu.sub.a M.sub.b Y.sub.c ; where "M" is at least one element selected from the group consisting of Ti, Zr, Hf, V, Nb, Ta, Cr, Mo, W of the periodic table, Mn, Co, Ni, Al and the Platinum group; "Y" is at least one element selected form the group consisting of Si, B, P, and C; and wherein "a", "b", and "c", expressed in atomic % are as follows: 3<a≦8 0.1<b≦8 3.1≦a+b≦12 15≦c≦28.
Claim 3
Dependent Claim 26 words
An Fe-based soft magnetic alloy according to claim 1 wherein the area ratio of the fine crystal grains present in the alloy is at least 30%.
Claim 4
Dependent Claim 31 words
An Fe-based soft magnetic alloy according to claim 1 wherein of least 80% of fine crystal grains present in the alloy are in the range of 50 Å to 300 Å.
Claim 5
Dependent Claim 32 words
An Fe-based soft magnetic alloy according to claim 2 wherein at least 80% of the fine crystal grains present in the alloy are in the range of 50 Å to 300 Å.
Claim 6
Dependent Claim 24 words
An Fe-based soft magnetic alloy according to claim 1 wherein the amount of Cu is more than 3 and less than 5 atomic %.
Claim 7
Dependent Claim 20 words
An Fe-based soft magnetic alloy according to claim 1 wherein the amount of "M" is 1 to 7 atomic %.
Claim 8
Dependent Claim 20 words
An Fe-based soft magnetic alloy according to claim 1 wherein the amount of "M" is 1.5 to 5 atomic %.
Claim 9
Dependent Claim 20 words
An Fe-based soft magnetic alloy according to claim 1 wherein the amount of "Y" is 18 to 26 atomic %.
Claim 10
Dependent Claim 24 words
An Fe-based soft magnetic alloy according to claim 1 wherein the ratio of (Si and C) to (P and B) is more than 1.
Claim 11
Dependent Claim 98 words
A dust core consisting essentially of an alloy powder having fine crystal grains dispersed in an amorphous phase and as described in the following formula Fe.sub.100-a-b-c-d-e Cu.sub.a M'.sub.b M".sub.c Si.sub.d B.sub.e where: "M'" is at least one element selected from the group consisting of Ti, Zr, Hf, V, Nb, Ta, Cr, Mo, W of the periodic table; "M"" is at least one element selected from the group consisting of Mn, Co, Ni, Al, and the Platinum group; and wherein "a", "b", "c", "d" and "e", expressed in atomic %, are as follows: 3<a≦8 0.1<b≦8 0≦c≦15 8≦d≦22 3≦e≦15 15≦d+e≦28.
Claim 12
Dependent Claim 98 words
A dust core consisting essentially of an alloy powder having fine crystal grains dispersed in an amorphous phase and as described in the following formula Fe.sub.100-a-b-c-d-e Cu.sub.a M'.sub.b M".sub.c Si.sub.d B.sub.e where: "M'" is at least one element selected from the group consisting of Ti, Zr, Hf, V, Nb, Ta, Cr, Mo, W of the periodic table; "M"" is at least one element selected from the group consisting of Mn, Co, Ni, Al, and the Platinum group; and wherein "a", "b", "c", "d" and "e", expressed in atomic %, are as follows: 3<a≦8 0.1<b≦8 0≦c≦15 8≦d≦22 3≦e≦15 15≦d+e≦28.
Claim 13
Dependent Claim 24 words
A dust core according to claim 10 wherein the area ratio of the fine crystal grains present in the alloy is at least 30%.
Claim 14
Dependent Claim 22 words
A dust core according to claim 10 wherein at least 80% of the fine crystal grains are 50 Å to 300 Å.
Claim 15
Dependent Claim 22 words
A dust core according to claim 11 wherein at least 80% of the fine crystal grains are 50 Å to 300 Å.
Claim 16
Dependent Claim 21 words
A dust core according to claim 10 wherein the amount Cu is more than 3 and less than 5 atomic %.
Claim 17
Dependent Claim 18 words
A dust core according to claim 10 wherein the amount of M' is 1 to 7 atomic %.
Claim 18
Dependent Claim 18 words
A dust core according to claim 10 wherein the amount of M' is 1.5 to 5 atomic %.
Claim 19
Dependent Claim 17 words
A dust core according to claim 10 wherein amount of M" is less than 10 atomic %.
Claim 20
Dependent Claim 21 words
A dust core according to claim 10 wherein the amount of Cu, M' and M" is 3.1 to 25 atomic %.
Claim 21
Dependent Claim 18 words
A dust core according to claim 10 wherein the amount of Si is 10 to 22 atomic %.
Claim 22
Dependent Claim 18 words
A dust core according to claim 10 wherein the amount of Si is 12 to 18 atomic %.
Claim 23
Dependent Claim 18 words
A dust core according to claim 10 wherein the amount of B is 5 to 10 atomic %.
Claim 24
Dependent Claim 24 words
A dust core according to claim 10 wherein the particle size of the alloy powder is in the range of 1 to 100 μm.
Claim 25
Dependent Claim 18 words
An Fe-based soft magnetic alloy according to claim 1, wherein "a" is greater than or equal to 3.5.
Claim 26
Dependent Claim 18 words
An fe-based soft magnetic alloy according to claim 1, wherein "a" is greater than or equal to 4.0.
Claim 27
Dependent Claim 16 words
A dust core according to claim 10, wherein "a" is greater than or equal to 3.5.
Claim 28
Dependent Claim 16 words
A dust core according to claim 10, wherein "a" is greater than or equal to 4.0.
Claim 29
Dependent Claim 28 words
An Fe-based soft magnetic alloy according to claim 1, wherein the alloy has a core loss of between 290 and 330 mW/cc or between 210 and 250 mW/cc.
Claim 30
Dependent Claim 26 words
A dust core according to claim 10 wherein the alloy has a core loss of between 290 and 330 mW/cc or between 210 and 250 mW/cc
Claim 31
Dependent Claim 16 words
An Fe-based soft magnetic alloy according to claim 1, wherein the alloy does not contain Nb.
Claim 32
Dependent Claim 14 words
A dust core according to claim 1, wherein the alloy does not contain Nb.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1996-01-12 1996-07-13 1997-01-12 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2000-01-12 2000-07-13 2001-01-12 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2004-01-12 2004-07-13 2005-01-12 $7700.00 Window Closed / Lapsed

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