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US5162739A Expired / Lapsed US ⏱️ 0.0 years remaining

Balanced multi-tuned high-power broadband coil for nmr

Assignee: Doty Scientific Inc
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Filing: 1991-04-05
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Granted: 1992-11-10
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Expires: 2011-04-05
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Abstract

Abstract A double-tuned NMR sample excitation coil has a first end connected through a first balancing inductor to ground and a second end connected through a second balancing inductor to a low-frequency (LF) capacitor tuning and matching network. Two two balancing inductors have inductance less than 50% but greater than 10% that of the excitation coil. Each balancing coil is tuned by a capacitor network to an independent resonant frequency when disconnected from the sample coil that is less than 95% but greater than 60% of the final high frequency (HF) resonance. Moreover, both such independent resonant frequencies are equal within 10%. Broadband operation is possible under a variety of temperatures and the circuit works with high-speed sample spinners.

Inventors

  • 👤 F. David Doty

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 05:47
CPC Classifications
G; G01; G01R; G01R33/00; G01R33/20; G01R33/28; G01R33/32; G01R33/36; G01R33/3628; G01R33/3635

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 233 words
A balanced, multi-tuned, broad and circuit for high-field solids NMR probes requiring high-frequency port carrying a signal of a high frequency and a low-frequency port carrying a low frequency, said multi-tuned circuit comprising: a multi-turn sample excitation coil with a first lead at a first end and a second lead at a second end; a first balancing inductor connected with low first-lead inductance between said first end of said excitation coil and ground, said first end of said excitation coil also coupled to said high-frequency port via a fist high frequency high voltage variable capacitor network; a low-frequency high-voltage tuning and matching capacitor network coupled to said low-frequency port; a second balancing inductor and second high frequency high voltage variable capacitor network connected with low second-lead inductance between said second end of said excitation coil and said low-frequency high-voltage tuning and matching capacitor network; said first and second balancing inductors each having inductance less than 50% but greater than 10% of that of said excitation coil; said second balancing inductor further comprising a solenoid with fewer than five turns and having inductance less than 60 nH; each of said balancing coils tuned to substantially equal values of capacitive reactance at the desired high frequency by said first and second high frequency high voltage variable capacitor networks; said excitation coil further characterized in having its self-resonant frequency greater than 110% of said high frequency.
Claim 2
Dependent Claim 233 words
A balanced, multi-tuned, broad and circuit for high-field solids NMR probes requiring high-frequency port carrying a signal of a high frequency and a low-frequency port carrying a low frequency, said multi-tuned circuit comprising: a multi-turn sample excitation coil with a first lead at a first end and a second lead at a second end; a first balancing inductor connected with low first-lead inductance between said first end of said excitation coil and ground, said first end of said excitation coil also coupled to said high-frequency port via a fist high frequency high voltage variable capacitor network; a low-frequency high-voltage tuning and matching capacitor network coupled to said low-frequency port; a second balancing inductor and second high frequency high voltage variable capacitor network connected with low second-lead inductance between said second end of said excitation coil and said low-frequency high-voltage tuning and matching capacitor network; said first and second balancing inductors each having inductance less than 50% but greater than 10% of that of said excitation coil; said second balancing inductor further comprising a solenoid with fewer than five turns and having inductance less than 60 nH; each of said balancing coils tuned to substantially equal values of capacitive reactance at the desired high frequency by said first and second high frequency high voltage variable capacitor networks; said excitation coil further characterized in having its self-resonant frequency greater than 110% of said high frequency.
Claim 3
Dependent Claim 26 words
The multi-tuned circuit of claim 1 wherein said second balancing inductor is further characterized in having a length-to-diameter ratio greater than 0.2 and less than 2.0.
Claim 4
Dependent Claim 35 words
The multi-tuned circuit of claim 1 wherein each of said first and second balancing inductors is turned to resonate, when disconnected from the excitation coil, at a frequency less than 95% of the high frequency.
Claim 5
Dependent Claim 22 words
The multi-tuned circuit of claim 1 wherein said low-frequency high-voltage tuning and matching capacitor network comprises at least one high-pressure-gas-filled variable capacitor.
Claim 6
Dependent Claim 30 words
The multi-tuned circuit of claim 1 wherein said first balancing inductor is further characterized as comprising a coaxial line having a length approximately one fourth of the high frequency wavelength.
Claim 7
Dependent Claim 17 words
The multi-tuned circuit of claim 1 further comprising a series high-frequency trap coupled to the low-frequency port.
Claim 8
Dependent Claim 26 words
The multi-tuned circuit of claim 1 wherein each of said first and second balancing inductors has inductance less than 25% of that of said excitation coil.
Claim 9
Dependent Claim 28 words
The multi-tuned circuit of claim 2 further characterized in that the length-to-diameter ratio of said second balancing inductor is about 0.7 and the number of turns is two.
Claim 10
Dependent Claim 25 words
The multi-tuned circuit of claim 1 wherein said second balancing inductor has a number of turns no fewer than two and no greater than four.
Claim 11
Dependent Claim 19 words
The multi-tuned circuit of claim 1 wherein said second balancing inductor has an inductance of less than 25 nH.

References Cited (Backward Citations)

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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1995-11-10 1996-05-11 1996-11-10 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1999-11-10 2000-05-11 2000-11-10 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2003-11-10 2004-05-11 2004-11-10 $7700.00 Window Closed / Lapsed

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