US5116414A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Long-term control of root growth
Assignee: Battelle Memorial Institute Inc
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Filing: 1983-11-23
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Granted: 1992-05-26
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Expires: 2003-11-23
Abstract
Abstract A method and system for long-term control of root growth without killing the plants bearing those roots involves incorporating a 2,6-dinitroaniline in a polymer and disposing the polymer in an area in which root control is desired. This results in controlled release of the substituted aniline herbicide over a period of many years. Herbicides of this class have the property of preventing root elongation without translocating into other parts of the plant. The herbicide may be encapsulated in the polymer or mixed with it. The polymer-herbicide mixture may be formed into pellets, sheets, pipe gaskets, pipes for carrying water, or various other forms. The invention may be applied to other protection of buried hazardous wastes, protection of underground pipes, prevention of root intrusion beneath slabs, the dwarfing of trees or shrubs and other applications. The preferred herbicide is 4-difluoromethyl-N,N-dipropyl-2,6-dinitro-aniline, commonly known as trifluralin.
Inventors
- 👤 Frederick G. Burton
- 👤 Dominic A. Cataldo
- 👤 John F. Cline
- 👤 W. Eugene Skiens
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-04 15:21
CPC Classifications
A; A01; A01N; A01N33/00; A01N33/16; A01N33/18; A01N25/00; A01N25/34; A01N41/00; A01N41/02; A01N41/04; A01N41/06
Claims Analysis
Total Claims: 28
Claim 1
Independent Claim
167 words
A method for preventing roots of plants from intruding into a zone of soil below the surface of said soil, without killing said plants, said method comprising the following steps: (a) incorporating a herbicidal 2,6-dinitroaniline into a polymer to form a controlled release device, the release rate and the amount of said 2,6-dinitroaniline being sufficiently large to maintain for an extended period of time said zone at a concentration of said 2,6-dinitroaniline sufficiently high to prevent roots of said plants from intruding into said zone of soil but sufficiently low to prevent killing of the plants; (b) inserting at least one controlled release device into said zone of soil; (c) allowing said 2,6-dinitroaniline to release into the zone to maintain for an extended period of time the concentration of said 2,6-dinitroaniline in said zone sufficiently high to prevent roots of plants from intruding into said zone of soil, but sufficiently low to prevent killing the plants whose roots are prevented from intruding into said zone of soil.
Claim 2
Independent Claim
167 words
A method for preventing roots of plants from intruding into a zone of soil below the surface of said soil, without killing said plants, said method comprising the following steps: (a) incorporating a herbicidal 2,6-dinitroaniline into a polymer to form a controlled release device, the release rate and the amount of said 2,6-dinitroaniline being sufficiently large to maintain for an extended period of time said zone at a concentration of said 2,6-dinitroaniline sufficiently high to prevent roots of said plants from intruding into said zone of soil but sufficiently low to prevent killing of the plants; (b) inserting at least one controlled release device into said zone of soil; (c) allowing said 2,6-dinitroaniline to release into the zone to maintain for an extended period of time the concentration of said 2,6-dinitroaniline in said zone sufficiently high to prevent roots of plants from intruding into said zone of soil, but sufficiently low to prevent killing the plants whose roots are prevented from intruding into said zone of soil.
Claim 3
Dependent Claim
65 words
The method of claim 1 wherein the step of incorporating a herbicidal 2,6-dinitroaniline comprises: (a) mixing said 2,6-dinitroaniline with said polymer to form a 2,6-dinitroaniline polymer mixture; (b) molding said mixture to form a shaped controlled release device; (c) allowing said device to cool such that it maintains its shape, said 2,6-dinitroaniline being distributed throughout the polymer and releasing controllably when contacted with the soil.
Claim 4
Dependent Claim
68 words
The method of claim 1 wherein the step of incorporating a herbicidal 2,6-dinitroaniline comprises: (a) mixing a herbicidal 2,6-dinitroaniline with carbon black and said polymer to form a 2,6-dinitroaniline-polymer mixture; (b) molding said mixture to form a shaped controlled release device; (c) allowing said device to cool such that it maintains its shape, said 2,6-dinitroaniline being distributed throughout the polymer and releasing controllably when contacted with the soil.
Claim 5
Dependent Claim
66 words
The method of claim 1 wherein the step of incorporating a herbicidal 2,6-dinitroaniline comprises: (a) mixing a herbicidal 2,6-dinitroaniline with said polymer to form a 2,6-dinitroaniline polymer mixture; (b) extruding said mixture to form a shaped controlled release device; (c) allowing said device to cool such that it maintains its shape, said 2,6-dinitroaniline being distributed throughout the polymer and releasing controllably when contacted with the soil.
Claim 6
Dependent Claim
67 words
The method of claim 1 wherein the step of incorporating a herbicidal 2,6-dinitroaniline comprises: (a) mixing said 2,6-dinitroaniline with carbon black and said polymer to form a 2,6-dinitroaniline-polymer mixture; (b) extruding said mixture to form a shaped controlled release device; (c) allowing said device to cool such that it maintains its shape, said 2,6-dinitroaniline being distributed throughout the polymer and releasing controllably when contacted with the soil.
Claim 7
Dependent Claim
31 words
The method of claim 1 wherein the step of incorporating a herbicidal 2,6-dinitroaniline into a polymer comprises: placing said 2,6-dinitroaniline in a cavity of a shaped polymer; and, closing said cavity.
Claim 8
Dependent Claim
23 words
The method of claim 6 further comprising dissolving said 2,6-dinitroaniline in a solvent prior to the step of placing it in said cavity.
Claim 9
Independent Claim
78 words
The method of any of claims 1, 2, 3, 4, 5 or 6 wherein a plurality of said devices are inserted in said zone and said devices are spaced sufficiently close to each other to maintain the concentration of said 2,6-dinitroaniline in said zone above the minimum effective level so as to prevent the roots from intruding into said zone but sufficiently far apart to maintain the concentration in said zone sufficiently low to avoid killing the plants.
Claim 10
Independent Claim
18 words
The method of any of claims 1, 2, 3, 4, 5 or 6 wherein said 2,6-dinitroaniline is trifluralin.
Claim 11
Independent Claim
45 words
The method of any of claims 1, 2, 3, 4, 5, 6, 7, 8 or 9 wherein said polymer is selected from the group consisting of: polyurethane, poly (ethylene-vinyl acetate), silicone rubber, polyesters, vinyl acetate, butyl rubber, chlorobutyl rubbers, ethylene-propylene-diene monomer rubber, polypropylene and polyethylne.
Claim 12
Dependent Claim
13 words
The method of claim 1 wherein said polymer is a low density polyethylene.
Claim 13
Dependent Claim
20 words
The method of claim 1 wherein said polymer is selected from the group consisting of high density polythylene and polypropylene.
Claim 14
Dependent Claim
20 words
The method of claim 1 wherein said 2,6-dinitroaniline comprises from 10 to 50 parts per hundred weight of the polymer.
Claim 15
Dependent Claim
34 words
The method of claim 1 wherein said device comprises about 30 parts per hundred weight carbon black and 40 parts per hundred by weight of said 2,6-dinitroaniline based on the weight of the polymer.
Claim 16
Independent Claim
104 words
A method for preventing roots of plants from reaching a pipeline formed of a polymer installed beneath the surface of the soil, comprising the following step: incorporating into the polymer forming said pipeline a herbicidal 2,6-dinitroaniline, said 2,6 dinitroaniline diffusing out of said polymer at a sufficiently fast rate to maintain the soil adjacent to said pipeline at a sufficiently high concentration to prevent roots of plants from entering the pipeline but sufficiently slow rate to maintain the soil adjacent to said pipeline at a sufficiently low concentration of said 2,6-dinitroaniline to avoid filling the plants whose roots are prevented from entering the pipeline.
Claim 17
Independent Claim
104 words
A method for preventing roots of plants from reaching a pipeline formed of a polymer installed beneath the surface of the soil, comprising the following step: incorporating into the polymer forming said pipeline a herbicidal 2,6-dinitroaniline, said 2,6 dinitroaniline diffusing out of said polymer at a sufficiently fast rate to maintain the soil adjacent to said pipeline at a sufficiently high concentration to prevent roots of plants from entering the pipeline but sufficiently slow rate to maintain the soil adjacent to said pipeline at a sufficiently low concentration of said 2,6-dinitroaniline to avoid filling the plants whose roots are prevented from entering the pipeline.
Claim 18
Dependent Claim
10 words
The method of claim 5 wherein said 2,6-dinitroaniline is trifluralin.
Claim 19
Dependent Claim
30 words
The method of claim 15 wherein said polymer is selected from the group consisting of polyethylene, polypropylene, silicone rubber, butyl rubber, chlorobutyl rubber, natural rubber, ethylene-propylene-diene monomer rubber, and polyvinylchloride.
Claim 20
Dependent Claim
30 words
The method of claim 16 wherein said polymer is selected from the group consisting of polyethylene, polypropylene, silicone rubber, butyl rubber, chlorobutyl rubber, natural rubber, ethylene-propylene-diene monomer rubber, and polyvinylchloride.
Claim 21
Independent Claim
96 words
A method for protecting a pipeline installed beneath the surface of the soil from penetration of said pipeline by plant roots, said method comprising: placing at least one controlled release device beneath the surface of the soil, in or adjacent said pipeline, said device comprising: (a) a polymer; and (b) a herbicidal 2,6-dinitroaniline dispersed throughout said polymer, said 2,6-dinitroaniline diffusing out, for an extended period, of said polymer upon contact with the soil sufficiently fast of time so as to prevent roots of plants from penetrating the pipeline but sufficiently low to avoid killing said plants.
Claim 22
Independent Claim
96 words
A method for protecting a pipeline installed beneath the surface of the soil from penetration of said pipeline by plant roots, said method comprising: placing at least one controlled release device beneath the surface of the soil, in or adjacent said pipeline, said device comprising: (a) a polymer; and (b) a herbicidal 2,6-dinitroaniline dispersed throughout said polymer, said 2,6-dinitroaniline diffusing out, for an extended period, of said polymer upon contact with the soil sufficiently fast of time so as to prevent roots of plants from penetrating the pipeline but sufficiently low to avoid killing said plants.
Claim 23
Dependent Claim
21 words
The method of claim 19 wherein said pipeline comprises at least one joint and said device is positioned in said joint.
Claim 24
Dependent Claim
14 words
The method of claim 20 wherein said device forms a gasket for said joint.
Claim 25
Dependent Claim
16 words
The method of claim 19 wherein said device is positioned outside said pipeline and adjacent thereto.
Claim 26
Dependent Claim
19 words
The method of claim 19 wherein said device is in the form of sheets positioned adjacent to said pipeline.
Claim 27
Dependent Claim
14 words
The method of claim 23 wherein said device is in the form of pellets.
Claim 28
Dependent Claim
10 words
The method of claim 19 wherein said 2,6-dinitroaniline is trifluralin.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1995-05-26 | 1995-11-25 | 1996-05-26 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1999-05-26 | 1999-11-25 | 2000-05-26 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2003-05-26 | 2003-11-25 | 2004-05-26 | $7700.00 | Window Closed / Lapsed |