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US5099788A Expired / Lapsed US ⏱️ 0.0 years remaining

Method and apparatus for forming a diamond film

Assignee: Soken Inc
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Filing: 1990-07-03
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Granted: 1992-03-31
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Expires: 2010-07-03
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Abstract

Abstract A method and apparatus for forming a diamond film, has a casing in which vacuum is maintained at a predetermined value. A substrate is disposed within the casing so that the diamond film is formed thereon. A gas plasma generator for generating a gas plasma near the substrate from a plasma source gas and a carbon source gas by an arc discharge is provided within the casing. A detector detects a factor which is related to a change in a surface temperature of the diamond film, and an electronic controller controls in response to the detected factor the surface temperature of the diamond film so as to maintain such temperature near a predetermined optimal value for forming the diamond film. As the surface temperature is maintained near the optimal value by a feedback control, high purity diamond film is obtained irrespective of the thickness or the forming time thereof.

Inventors

  • 👤 Nobuei Ito
  • 👤 Minoru Yamamoto
  • 👤 Satoshi Nakamura
  • 👤 Tadashi Hattori

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 13:57
CPC Classifications
C; C23; C23C; C23C16/00; C23C16/22; C23C16/26; C23C16/27; C23C16/276; C23C16/44; C23C16/50; C23C16/513; C23C16/52

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 202 words
An apparatus for forming a diamond film comprising: a casing in which pressure is maintained to a predetermined value; supporting means for supporting within said casing a substrate on which said diamond film is to be formed; gas supplying means for supplying at least carbon source gas and plasma source gas into said casing; plasma generating means for generating gas plasma near said substrate from said carbon source gas and plasma source gas; temperature detecting means for detecting a temperature of a forming surface of said diamond film and for producing a detecting signal indicative of a detected forming temperature of said diamond film, while said diamond film is being formed; control signal producing means, electrically connected to said temperature detecting means so as to receive said detecting signal, for determining a control signal for maintaining said forming surface temperature near a predetermined optimal temperature of said diamond film in response to said detecting signal, and for producing said control signal; and temperature adjusting means, electrically connected to said control signal producing means, for adjusting said forming temperature based on said control signal so that said forming surface temperature is maintained near said optimal temperature while said diamond film is being formed.
Claim 2
Independent Claim 202 words
An apparatus for forming a diamond film comprising: a casing in which pressure is maintained to a predetermined value; supporting means for supporting within said casing a substrate on which said diamond film is to be formed; gas supplying means for supplying at least carbon source gas and plasma source gas into said casing; plasma generating means for generating gas plasma near said substrate from said carbon source gas and plasma source gas; temperature detecting means for detecting a temperature of a forming surface of said diamond film and for producing a detecting signal indicative of a detected forming temperature of said diamond film, while said diamond film is being formed; control signal producing means, electrically connected to said temperature detecting means so as to receive said detecting signal, for determining a control signal for maintaining said forming surface temperature near a predetermined optimal temperature of said diamond film in response to said detecting signal, and for producing said control signal; and temperature adjusting means, electrically connected to said control signal producing means, for adjusting said forming temperature based on said control signal so that said forming surface temperature is maintained near said optimal temperature while said diamond film is being formed.
Claim 3
Dependent Claim 30 words
An apparatus as claimed in claim 1, wherein said temperature detecting means is provided outside said casing and optically detects said forming surface temperature through a window of said casing.
Claim 4
Dependent Claim 30 words
An apparatus as claimed in claim 1, wherein said temperature detecting means includes a photo sensitive element which detects a luminous brightness of said forming surface of said diamond film.
Claim 5
Dependent Claim 35 words
An apparatus as claimed in claim 1, wherein said control signal producing means produces said control signal only when a difference between said detected forming surface temperature and said optimal temperature exceeds a predetermined value.
Claim 6
Dependent Claim 27 words
An apparatus as claimed in claim 1, wherein said temperature adjusting means adjusts said forming surface temperature within in a range between 800° C. and 1000° C.
Claim 7
Independent Claim 224 words
An apparatus for forming a diamond film comprising: a casing in which pressure is maintained to a predetermined value; supporting means for supporting within said casing a substrate on which said diamond film is to be formed; gas supplying means for supplying at least carbon source gas and plasma source gas into said casing; plasma generating means for generating gas plasma near said substrate from said carbon source gas and plasma source gas; temperature detecting means for detecting a temperature of a forming surface of said diamond film and for producing a detecting signal indicative of a detected forming temperature of said diamond film, while said diamond film is being formed; control signal producing means, electrically connected to said temperature detecting means so as to receive said detecting signal, for determining a control signal for maintaining said forming surface temperature near a predetermined optimal temperature of said diamond film on the basis of a difference between said detected forming surface temperature and said predetermined optimal temperature, and for producing said control signal; and temperature adjusting means, electrically connected to said control signal producing means so as to receive said control signal, for adjusting a position of said supporting means in response to said control signal so that said forming surface temperature is maintained near said optimal temperature while said diamond film is being formed.
Claim 8
Independent Claim 224 words
An apparatus for forming a diamond film comprising: a casing in which pressure is maintained to a predetermined value; supporting means for supporting within said casing a substrate on which said diamond film is to be formed; gas supplying means for supplying at least carbon source gas and plasma source gas into said casing; plasma generating means for generating gas plasma near said substrate from said carbon source gas and plasma source gas; temperature detecting means for detecting a temperature of a forming surface of said diamond film and for producing a detecting signal indicative of a detected forming temperature of said diamond film, while said diamond film is being formed; control signal producing means, electrically connected to said temperature detecting means so as to receive said detecting signal, for determining a control signal for maintaining said forming surface temperature near a predetermined optimal temperature of said diamond film on the basis of a difference between said detected forming surface temperature and said predetermined optimal temperature, and for producing said control signal; and temperature adjusting means, electrically connected to said control signal producing means so as to receive said control signal, for adjusting a position of said supporting means in response to said control signal so that said forming surface temperature is maintained near said optimal temperature while said diamond film is being formed.
Claim 9
Dependent Claim 35 words
An apparatus as claimed in claim 6, wherein said control signal producing means produces said control signal only when a difference between said detected forming surface temperature and said optimal temperature exceeds a predetermined value.
Claim 10
Dependent Claim 50 words
An apparatus as claimed in claim 6, wherein said temperature adjusting means adjusts said position of said supporting means in a way that a distance between said substrate and said gas plasma generating means increases when said forming surface temperature is higher than said optimal temperature by a predetermined value.

References Cited (Backward Citations)

US3980042A Cited
US4767608A Cited
US4851254A Cited
US4981671A Cited
US4883560A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1995-03-31 1995-09-30 1996-03-31 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1999-03-31 1999-09-30 2000-03-31 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2003-03-31 2003-09-30 2004-03-31 $7700.00 Window Closed / Lapsed

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