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US5098662A Expired / Lapsed US ⏱️ 0.0 years remaining

Modular solvent extractor/concentrator apparatus

Assignee: Corning Inc
•
Filing: 1990-08-10
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Granted: 1992-03-24
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Expires: 2010-08-10
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Abstract

Abstract The invention relates generally to laboratory glassware apparatus and particularly to laboratory apparatus and kits thereof. The disclosed apparatus is used to extract and/or concentrate specific substances for analytical purposes from sample liquids by passing a predetermined solvent through the sample. The invention includes a modular sample container body for holding a sample to be processed. The container body has a variety of disconnect joints for receiving a variety of disconnectable attachments that are used in the extraction and/or concentration process of the specific substance. The invention also includes a universal modular container body having a variety of disconnect joints that may be used with solvents having a density lesser or greater than the density of the sample liquid being processed.

Inventors

  • 👤 Bruce A. Killough

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 03:01
CPC Classifications
B; B01; B01D; B01D11/00; B01D11/02; B01D11/0215; B01D11/0219; B01L; B01L3/00; B01L3/56; B01L3/569; G; G01; G01N; G01N1/00; G01N1/28; G01N1/34; G01N1/40; G01N1/4055; G01N2001/4061

Claims Analysis

Total Claims: 31
Claim 1
Independent Claim 157 words
A kit for forming a modular solvent extractor apparatus comprising: a) a container body for holding a sample to be treated with a solvent to render an extraction therefrom, the container body having a mouth, at least one solvent vapor port, and at least one solvent extract port; b) an extract connecting tube having a disconnect joint at each end thereof; c) a hollow vapor connecting arm having a disconnect joint at one or both ends thereof, a solvent extract inlet port being located at a preselected position along the vapor arm and having a disconnect joint to accommodate one of the disconnect joints of the extract connecting tube; d) a disconnect joint at the solvent vapor port to accommodate one of the disconnect joints of the vapor connecting arm; and e) a disconnect joint the at least one solvent extract port to accommodate one of the disconnect joints of at least one the extract connecting tube.
Claim 2
Dependent Claim 157 words
A kit for forming a modular solvent extractor apparatus comprising: a) a container body for holding a sample to be treated with a solvent to render an extraction therefrom, the container body having a mouth, at least one solvent vapor port, and at least one solvent extract port; b) an extract connecting tube having a disconnect joint at each end thereof; c) a hollow vapor connecting arm having a disconnect joint at one or both ends thereof, a solvent extract inlet port being located at a preselected position along the vapor arm and having a disconnect joint to accommodate one of the disconnect joints of the extract connecting tube; d) a disconnect joint at the solvent vapor port to accommodate one of the disconnect joints of the vapor connecting arm; and e) a disconnect joint the at least one solvent extract port to accommodate one of the disconnect joints of at least one the extract connecting tube.
Claim 3
Dependent Claim 30 words
The extractor kit of claim 1 wherein at least one of the disconnect joints comprises a socket joint accommodating a ball joint thereby forming a ball and socket joint arrangement.
Claim 4
Dependent Claim 224 words
A kit for forming a modular solvent extractor apparatus comprising: a) a container body for holding a sample to be treated with solvent to render an extraction therefrom, the container body having a mouth, at least one solvent vapor port, and at least one solvent extract port; b) an extract connecting tube having a disconnect joint at each end thereof; c) a hollow vapor connecting arm having a disconnect joint at one or both ends thereof, a solvent extract inlet port having a disconnect joint to accommodate one of the disconnect joints of the extract connecting tube, and the solvent extract inlet port being located at a preselected position along the vapor arm; d) a disconnect joint at the solvent vapor port to accommodate at least one of the disconnect joints of the vapor connecting arm; e) a disconnect joint at the solvent extract port to accommodate one of the disconnect joints of the extract connecting tube there by allowing the container body to be connected to the vapor arm by the extract connecting tube; and f) a removable tubular insert for placement within the container body, the insert having a passage extending axially therethrough, an adjoining through passage extending generally perpendicularly from the axially extending passage, and the insert being shaped and sized to be accommodated by the mouth of the container body.
Claim 5
Dependent Claim 224 words
A kit for forming a modular solvent extractor apparatus comprising: a) a container body for holding a sample to be treated with solvent to render an extraction therefrom, the container body having a mouth, at least one solvent vapor port, and at least one solvent extract port; b) an extract connecting tube having a disconnect joint at each end thereof; c) a hollow vapor connecting arm having a disconnect joint at one or both ends thereof, a solvent extract inlet port having a disconnect joint to accommodate one of the disconnect joints of the extract connecting tube, and the solvent extract inlet port being located at a preselected position along the vapor arm; d) a disconnect joint at the solvent vapor port to accommodate at least one of the disconnect joints of the vapor connecting arm; e) a disconnect joint at the solvent extract port to accommodate one of the disconnect joints of the extract connecting tube there by allowing the container body to be connected to the vapor arm by the extract connecting tube; and f) a removable tubular insert for placement within the container body, the insert having a passage extending axially therethrough, an adjoining through passage extending generally perpendicularly from the axially extending passage, and the insert being shaped and sized to be accommodated by the mouth of the container body.
Claim 6
Dependent Claim 30 words
The extractor kit of claim 3 wherein at least one of the disconnect joints comprises a socket joint accommodating a ball joint thereby forming a ball and socket joint arrangement.
Claim 7
Dependent Claim 165 words
A kit for forming a modular combination solvent extractor/concentrator comprising: a) a container body for holding a sample to be treated with solvent to render an extraction therefrom, the container body having a mouth, at least one solvent vapor port, and at least one solvent extract port; b) an extract connecting tube having a disconnect joint at each end thereof and a stopcock located at a predetermined position along the extract connecting tube; c) a hollow vapor connecting arm having a disconnect joint at one or both ends thereof, a solvent extract inlet port being located at a preselected position along the vapor arm and having a disconnect joint to accommodate one of the disconnect joints of the extract connecting tube; d) a disconnect joint at the solvent vapor inlet port to accommodate one of the disconnect joints of the vapor connecting arm; and e) a disconnect joint at the solvent extract port to accommodate one of the disconnect joints of the extract connecting tube.
Claim 8
Dependent Claim 165 words
A kit for forming a modular combination solvent extractor/concentrator comprising: a) a container body for holding a sample to be treated with solvent to render an extraction therefrom, the container body having a mouth, at least one solvent vapor port, and at least one solvent extract port; b) an extract connecting tube having a disconnect joint at each end thereof and a stopcock located at a predetermined position along the extract connecting tube; c) a hollow vapor connecting arm having a disconnect joint at one or both ends thereof, a solvent extract inlet port being located at a preselected position along the vapor arm and having a disconnect joint to accommodate one of the disconnect joints of the extract connecting tube; d) a disconnect joint at the solvent vapor inlet port to accommodate one of the disconnect joints of the vapor connecting arm; and e) a disconnect joint at the solvent extract port to accommodate one of the disconnect joints of the extract connecting tube.
Claim 9
Dependent Claim 30 words
The extractor/concentrator kit of claim 5 wherein at least one of the disconnect joints comprises a socket joint accommodating a ball joint thereby forming a ball and socket joint arrangement.
Claim 10
Dependent Claim 17 words
The extractor/concentrator kit of claim 5 wherein the vapor connecting arm comprises a Snyder distillation column therein.
Claim 11
Dependent Claim 234 words
A kit for forming a modular combination solvent extractor/concentrator comprising: a) a container body for holding a sample to be treated with solvent to render an extraction therefrom, the container body having a mouth, at least one solvent vapor port, and at least one solvent extract port; b) an extract connecting tube having a disconnect joint at each end thereof and a stopcock located at a predetermined position along the extract connecting tube; c) a hollow vapor connecting arm having a disconnect joint at one or more ends thereof, a solvent extract inlet port being located at a preselected position along the vapor arm and having a disconnect joint to accommodate one of the disconnect joints of the extract connecting tube, and the extract inlet port; d) a disconnect joint at the solvent vapor port to accommodate one of the disconnect joints of the vapor connecting arm; e) a disconnect joint at the solvent extract port to accommodate one of the disconnect joints of the extract connecting tube thereby allowing the container body to be connected to the vapor arm by the extract connecting tube; and f) a removable tubular insert for placement within the container body, the insert having a passage extending axially therethrough, an adjoining through passage extending generally perpendicularly from the axially extending passage, and the insert being shaped and sized to be accommodated by the mouth of the container body.
Claim 12
Dependent Claim 234 words
A kit for forming a modular combination solvent extractor/concentrator comprising: a) a container body for holding a sample to be treated with solvent to render an extraction therefrom, the container body having a mouth, at least one solvent vapor port, and at least one solvent extract port; b) an extract connecting tube having a disconnect joint at each end thereof and a stopcock located at a predetermined position along the extract connecting tube; c) a hollow vapor connecting arm having a disconnect joint at one or more ends thereof, a solvent extract inlet port being located at a preselected position along the vapor arm and having a disconnect joint to accommodate one of the disconnect joints of the extract connecting tube, and the extract inlet port; d) a disconnect joint at the solvent vapor port to accommodate one of the disconnect joints of the vapor connecting arm; e) a disconnect joint at the solvent extract port to accommodate one of the disconnect joints of the extract connecting tube thereby allowing the container body to be connected to the vapor arm by the extract connecting tube; and f) a removable tubular insert for placement within the container body, the insert having a passage extending axially therethrough, an adjoining through passage extending generally perpendicularly from the axially extending passage, and the insert being shaped and sized to be accommodated by the mouth of the container body.
Claim 13
Dependent Claim 30 words
The extractor/concentrator kit of claim 8 wherein at least one of the disconnect joints comprises a socket joint accommodating a ball joint thereby forming a ball and socket joint arrangement.
Claim 14
Dependent Claim 17 words
The extractor/concentrator kit of claim 8 wherein the vapor connecting arm comprises a Snyder distillation column therein.
Claim 15
Dependent Claim 150 words
A modular solvent extractor apparatus comprising: a) a container body for holding a sample to be treated with a solvent to render an extraction therefrom, the container body having a mouth, at least one solvent vapor port having a disconnect joint, and at least one solvent extract port being located at a preselected position upon the container body having a disconnect joint; b) an extract connecting tube having a disconnect joint at each end thereof, one of the disconnect joints being accommodated by the joint on the solvent extract port; c) a hollow vapor connecting arm having a disconnect joint at both ends thereof, one of the disconnect joints accommodating the joint means at the solvent vapor port; and d) a solvent extract inlet port being located at a preselected position along the vapor arm and having a disconnect joint accommodating the remaining disconnect joint of the extract connecting tube.
Claim 16
Dependent Claim 150 words
A modular solvent extractor apparatus comprising: a) a container body for holding a sample to be treated with a solvent to render an extraction therefrom, the container body having a mouth, at least one solvent vapor port having a disconnect joint, and at least one solvent extract port being located at a preselected position upon the container body having a disconnect joint; b) an extract connecting tube having a disconnect joint at each end thereof, one of the disconnect joints being accommodated by the joint on the solvent extract port; c) a hollow vapor connecting arm having a disconnect joint at both ends thereof, one of the disconnect joints accommodating the joint means at the solvent vapor port; and d) a solvent extract inlet port being located at a preselected position along the vapor arm and having a disconnect joint accommodating the remaining disconnect joint of the extract connecting tube.
Claim 17
Dependent Claim 29 words
The apparatus of claim 11 wherein at least one of the disconnect joints comprises a socket joint accommodating a ball joint thereby forming a ball and socket joint arrangement.
Claim 18
Dependent Claim 27 words
The apparatus of claim 11 further comprising the sample containing body having at least one solvent extract port having a disconnect joint accommodating a disconnect joint plug.
Claim 19
Dependent Claim 86 words
The modular solvent extractor apparatus of claim 11 further comprising: a) a Kuderna-Danish flask having a first disconnect joint and a second disconnect joint, the first disconnect joint being connectable to one of the disconnect joints located at one of the ends of the vapor connecting arm; and b) a concentrator tube having a disconnect joint which is connectable to the second disconnect joint of the Kuderna-Danish flask; and c) a condensor having a disconnect joint which is connectable to the mouth of the container body.
Claim 20
Dependent Claim 178 words
A modular combination solvent extractor/concentrator apparatus comprising: a) a container body for holding a sample to be treated with a solvent to render an extraction therefrom, the container body having a mouth, at least one solvent vapor port having a disconnect joint, and at least one solvent extract port being located at a preselected position upon the container body having a disconnect joint; b) an extract connecting tube having a stopcock located at a preselected position along the extract connecting tube and a disconnect joint at each end of the extract connecting tube, one of the disconnect joints being accommodated by the disconnect joint on the solvent extract port; c) a hollow vapor connecting arm having a disconnect joint at both ends, one of the disconnect joints accommodating the disconnect joint at the solvent vapor port; d) a Snyder distillation column within the vapor connecting arm; and e) a solvent extract inlet port being located at a preselected position along the vapor arm and having a disconnect joint accommodating the remaining disconnect joint of the extract connecting tube.
Claim 21
Dependent Claim 178 words
A modular combination solvent extractor/concentrator apparatus comprising: a) a container body for holding a sample to be treated with a solvent to render an extraction therefrom, the container body having a mouth, at least one solvent vapor port having a disconnect joint, and at least one solvent extract port being located at a preselected position upon the container body having a disconnect joint; b) an extract connecting tube having a stopcock located at a preselected position along the extract connecting tube and a disconnect joint at each end of the extract connecting tube, one of the disconnect joints being accommodated by the disconnect joint on the solvent extract port; c) a hollow vapor connecting arm having a disconnect joint at both ends, one of the disconnect joints accommodating the disconnect joint at the solvent vapor port; d) a Snyder distillation column within the vapor connecting arm; and e) a solvent extract inlet port being located at a preselected position along the vapor arm and having a disconnect joint accommodating the remaining disconnect joint of the extract connecting tube.
Claim 22
Dependent Claim 87 words
The modular combination solvent extractor/concentration apparatus of claim 15 further comprising: a) a Kuderna-Danish flask having a first disconnect joint and a second disconnect joint, the first disconnect joint being connectable to one of the disconnect joints located at one of the ends of the vapor connecting arm; and b) a concentrator tube having a disconnect joint which is connectable to the second disconnect joint of the Kuderna-Danish flask; and c) a condenser having a disconnect joint which is connectable to the mouth of the container body.
Claim 23
Dependent Claim 29 words
The apparatus of claim 15 wherein at least one of the disconnect joints comprises a socket joint accommodating a ball joint thereby forming a ball and socket joint arrangement.
Claim 24
Dependent Claim 27 words
The apparatus of claim 15, further comprising the sample containing body having at least one solvent extract port having a disconnect joint accommodating a disconnect joint plug.
Claim 25
Dependent Claim 69 words
An apparatus as claimed in claim 15, comprising a removable tubular insert for placement within the container body, the insert having a passage extending axially therethrough for introducing solvent at a level below the middle portion of the container body, an adjoining through passage extending generally perpendicularly from the axially extending passage, and the insert being shaped and sized to be accommodated by the mouth of the container body.
Claim 26
Dependent Claim 142 words
A container body for holding a sample to be treated with solvent to render an extraction therefrom comprising: a) an upper portion, a middle portion, and a lower portion; b) a mouth extending from the upper portion; c) a vapor port located within the upper portion; d) an upper extract port located with the middle portion; e) a lower extract port located within the lower portion; f) each of the ports having a disconnect joint to accommodate disconnectable attachments; and g) a removable tubular insert for placement within the container body, the insert having a passage extending axially therethrough for introducing solvent at a level below the middle portion of the container body, an adjoining through passage extending generally perpendicularly from the axially extending passage, and the insert being shaped and sized to be accommodated by the mouth of the container body.
Claim 27
Dependent Claim 142 words
A container body for holding a sample to be treated with solvent to render an extraction therefrom comprising: a) an upper portion, a middle portion, and a lower portion; b) a mouth extending from the upper portion; c) a vapor port located within the upper portion; d) an upper extract port located with the middle portion; e) a lower extract port located within the lower portion; f) each of the ports having a disconnect joint to accommodate disconnectable attachments; and g) a removable tubular insert for placement within the container body, the insert having a passage extending axially therethrough for introducing solvent at a level below the middle portion of the container body, an adjoining through passage extending generally perpendicularly from the axially extending passage, and the insert being shaped and sized to be accommodated by the mouth of the container body.
Claim 28
Dependent Claim 32 words
A container body as claimed in claim 20 wherein at least one of the disconnect joints comprises a socket joint accommodating a ball joint thereby forming a ball and socket joint arrangement.
Claim 29
Dependent Claim 132 words
A container body for holding a sample to be treated with solvent to render an extraction therefrom comprising: a) an upper portion, a middle portion, and a lower portion; b) a mouth extending from the upper portion; c) a vapor port located within the upper portion; d) a solvent extract port located with the middle portion; e) each of the ports having a disconnect joint to accommodate disconnectable attachments; and f) a removable tubular insert for placement within the container body, the insert having a passage extending axially therethrough for introducing solvent at a level below the middle portion of the container body, an adjoining through passage extending generally perpendicularly from the axially extending passage, and the insert being shaped and sized to be accommodated by the mouth of the container body.
Claim 30
Dependent Claim 132 words
A container body for holding a sample to be treated with solvent to render an extraction therefrom comprising: a) an upper portion, a middle portion, and a lower portion; b) a mouth extending from the upper portion; c) a vapor port located within the upper portion; d) a solvent extract port located with the middle portion; e) each of the ports having a disconnect joint to accommodate disconnectable attachments; and f) a removable tubular insert for placement within the container body, the insert having a passage extending axially therethrough for introducing solvent at a level below the middle portion of the container body, an adjoining through passage extending generally perpendicularly from the axially extending passage, and the insert being shaped and sized to be accommodated by the mouth of the container body.
Claim 31
Dependent Claim 32 words
A container body as claimed in claim 22 wherein at least one of the disconnect joints comprises a socket joint accommodating a ball joint thereby forming a ball and socket joint arrangement.

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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1995-03-24 1995-09-23 1996-03-24 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1999-03-24 1999-09-23 2000-03-24 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2003-03-24 2003-09-23 2004-03-24 $7700.00 Window Closed / Lapsed

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