Abstract The present invention enables the diamond coating of stationary elongate objects, such as twist drills, with a continuous uniform film without any motion of the twist drill due to the unexpected superb "throwing power" of a reactor disclosed herein. The CVD diamond reactor includes a vacuum chamber, inlet for feed hydrogen/hydrocarbon mixtures, and an outlet, in conventional fashion. The improvement for coating with CVD diamond the entire outer surface of at least a portion of a plurality of stationary elongate objects comprises disposed within said reactor, an elongate metal tube having a plurality of apertures for holding elongate objects disposed radially inwardly and having a cooling pipe in thermal contact with and disposed about the outside of said metal tube; and a filament running within said tube along its lengthwise extent and being in electrical connection with the source of voltage for heating said filament to a temperature adequate to initiate hydrocarbon disassociation, the portions of said elongate object within said tube surrounding said filament being heated thereby.
In a method for coating the CVD diamond elongate objects wherein a flow of hydrogen/hydrocarbon mixture is passed into a vacuum chamber of a diamond reactor held under CVD diamond-forming conditions wherein the mixture is at least partially disassociated for diamond deposition/growth on said substrate, the improvement for coating the entire outside surface of at least a portion of a plurality of stationary elongate objects which comprises passing said feed hydrogen/hydrocarbon mixture through an elongate metal tube disposed within said reactor which tube has a plurality of apertures which hold elongate objects disposed radially inwardly and which has a cooling pipe in thermal contact with and disposed about the outside of said tube, heating to a temperature adequate to initiate hydrocarbon disassociation said mixture with a filament which runs within said tube along the lengthwise extent and which is in electrical connection with the source of voltage for its heating, said heated filament also heating said elongate objects, and passing cooling fluid through said cooling pipe at a temperature and flow rate to maintain the elongate objects at a CVD diamond-forming temperature.
Claim 2
Dependent Claim
182 words
In a method for coating the CVD diamond elongate objects wherein a flow of hydrogen/hydrocarbon mixture is passed into a vacuum chamber of a diamond reactor held under CVD diamond-forming conditions wherein the mixture is at least partially disassociated for diamond deposition/growth on said substrate, the improvement for coating the entire outside surface of at least a portion of a plurality of stationary elongate objects which comprises passing said feed hydrogen/hydrocarbon mixture through an elongate metal tube disposed within said reactor which tube has a plurality of apertures which hold elongate objects disposed radially inwardly and which has a cooling pipe in thermal contact with and disposed about the outside of said tube, heating to a temperature adequate to initiate hydrocarbon disassociation said mixture with a filament which runs within said tube along the lengthwise extent and which is in electrical connection with the source of voltage for its heating, said heated filament also heating said elongate objects, and passing cooling fluid through said cooling pipe at a temperature and flow rate to maintain the elongate objects at a CVD diamond-forming temperature.
Claim 3
Dependent Claim
18 words
The method of claim 1 wherein said elongate objects that are coated with CVD diamond comprise twist drills.
Claim 4
Dependent Claim
27 words
The method of claim 1 wherein the ratio of hydrogen to hydrocarbon in said mixture passed into said vacuum chamber ranges from between about 1:10 and 1:1,000.
Claim 5
Dependent Claim
21 words
The method of claim 1 wherein said elongate objects are maintained at a temperature of between about 500° and 1100° C.
Claim 6
Dependent Claim
14 words
The method of claim 1 wherein a bias voltage is applied to said cylinder.