Patent US5084141A successfully refreshed from Google Patents.
US5084141A
Expired / Lapsed
US
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Process of destructive distillation of organic material
Assignee: Individual
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Filing: 1988-11-11
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Granted: 1992-01-28
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Expires: 2008-11-11
Abstract
Abstract The organic material (such as waste tire compound) is pyrolyzed by pre-heating the organic material (without pyrolysis) in a preheat zone 9 by a hot gas stream; feeding pre-heated material directly to a microwave discharge zone 10 by means of conveyor 8; pyrolyzing the pre-heated material in the microwave discharge zone to produce solid fission products containing elemental carbon and gaseous by-products; and recycling at least some of the latter to the hot gas stream which is supplied to the pre-heating zone.
Inventors
- 👤 Kenneth M. Holland
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-07 11:01
CPC Classifications
C; C08; C08J; C08J11/00; C08J11/04; C08J11/10; C08J11/12; B; B01; B01J; B01J19/00; B01J19/08; B01J19/12; B01J19/122; B01J19/126; C10; C10B; C10B19/00; C10B53/00; C10B53/07; B01J2219/00; B01J2219/08; B01J2219/12; B01J2219/1203; B01J2219/1206; B01J2219/1209; B01J2219/1221; B01J2219/1224; B01J2219/1227; C08J2321/00; Y; Y02; Y02P; Y02P20/00; Y02P20/141; Y02P20/143; Y02P20/145; Y02W; Y02W30/00; Y02W30/50; Y02W30/62
Claims Analysis
Total Claims: 15
Claim 1
Independent Claim
196 words
A process of destructive distillation of waste organic material containing a substantial proportion of carbon-carbon bonds, which comprises: (a) pre-heating said waste organic material at superatmospheric pressure and a temperature of at least about 250° C. in a pre-heating zone, substantially without pyrolysis of said organic material to elemental carbon, by means of a hot gas stream; (b) feeding said pre-heated material by movable feed means directly from said pre-heating zone to a microwave discharge zone, with the stream of hot gas flowing in a direction opposite to the preheated material, said microwave discharge zone having an atmosphere comprising a substantially oxygen-free gas at superatmospheric pressure; (c) pyrolyzing said pre-heated material in said zone by means of a microwave discharge in the low gigahertz frequency range for about 15 to 60 minutes, to cause fission of substantially all the carbon-carbon bonds in said organic material, in addition to fission of more polar chemical bonds, to produce solid fission products of elemental carbon, and gaseous by-products; (d) collecting said solid fission products downstream of said microwave discharge zone; and (e) recycling at least part of said gaseous by-products to said hot gas stream to effect said pre-heating.
Claim 2
Dependent Claim
196 words
A process of destructive distillation of waste organic material containing a substantial proportion of carbon-carbon bonds, which comprises: (a) pre-heating said waste organic material at superatmospheric pressure and a temperature of at least about 250° C. in a pre-heating zone, substantially without pyrolysis of said organic material to elemental carbon, by means of a hot gas stream; (b) feeding said pre-heated material by movable feed means directly from said pre-heating zone to a microwave discharge zone, with the stream of hot gas flowing in a direction opposite to the preheated material, said microwave discharge zone having an atmosphere comprising a substantially oxygen-free gas at superatmospheric pressure; (c) pyrolyzing said pre-heated material in said zone by means of a microwave discharge in the low gigahertz frequency range for about 15 to 60 minutes, to cause fission of substantially all the carbon-carbon bonds in said organic material, in addition to fission of more polar chemical bonds, to produce solid fission products of elemental carbon, and gaseous by-products; (d) collecting said solid fission products downstream of said microwave discharge zone; and (e) recycling at least part of said gaseous by-products to said hot gas stream to effect said pre-heating.
Claim 3
Dependent Claim
41 words
A process according to claim 1, wherein the feed means is used to forward said organic material through the pre-heating zone, to feed said pre-heated material to said microwave discharge zone, and to forward said material through said microwave discharge zone.
Claim 4
Dependent Claim
56 words
A process according to claim 1, wherein a first purge lock is provided for the supply of organic material to said pre-heating zone and a second purge lock is provided for removal of said material from said microwave discharge zone, said purge locks operating to substantially prevent inflow of oxygen-containing gas into each of said zones.
Claim 5
Dependent Claim
18 words
A process according to claim 1, wherein said hot gas stream further comprises separately supplied hydrocarbon or nitrogen.
Claim 6
Dependent Claim
36 words
A process according to claim 1, wherein liquid by-products from the microwave discharge zone are burnt and the resultant thermal energy is used to provide a minor part of the total energy put into the process.
Claim 7
Dependent Claim
26 words
A process according to claim 1, in which said organic material is predominantly selected from the group consisting of hydrocarbon materials, carbohydrate materials and mixtures thereof.
Claim 8
Dependent Claim
14 words
A process according to claim 1, wherein said organic material comprises a rubber compound.
Claim 9
Dependent Claim
13 words
A process according to claim 7, wherein said rubber compound contains carbon filler.
Claim 10
Dependent Claim
20 words
A process according to claim 1, wherein the temperature of the preheating zone varies from about 300° to 500° C.
Claim 11
Dependent Claim
17 words
A process according to claim 1, wherein the microwave discharge zone is separated from the preheating zone.
Claim 12
Dependent Claim
16 words
A process according to claim 1, wherein the separation is accomplished by using a microwave shield.
Claim 13
Dependent Claim
14 words
A process according to claim 1, wherein the microwave discharge is about 2.4 gigahertz.
Claim 14
Dependent Claim
33 words
A process according to claim 1, wherein said organic material comprises waste materials selected from the group consisting of natural or synthetic rubber compounds, agricultural waste material, animal waste materials and mixtures thereof.
Claim 15
Dependent Claim
35 words
A process according to claim 1, wherein the hot gas stream comprising the recycled part of the gaseous byproducts is passed countercurrently through the microwave discharge zone prior to passing countercurrently through the pre-heating zone.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1995-01-27 | 1995-07-29 | 1996-01-28 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1999-01-27 | 1999-07-29 | 2000-01-28 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2003-01-27 | 2003-07-29 | 2004-01-28 | $7700.00 | Window Closed / Lapsed |