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Ordered iron aluminide alloys having an improved room-temperature ductility and method thereof

Assignee: Lockheed Martin Energy Systems Inc
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Filing: 1990-07-02
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Granted: 1992-01-28
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Expires: 2010-07-02
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Abstract

Abstract A process is disclosed for improving the room temperature ductility and strength of iron aluminide intermetallic alloys. The process involves thermomechanically working an iron aluminide alloy by means which produce an elongated grain structure. The worked alloy is then heated at a temperature in the range of about 650 DEG C. to about 800 DEG C. to produce a B2-type crystal structure. The alloy is rapidly cooled in a moisture free atmosphere to retain the B2-type crystal structure at room temperature, thus providing an alloy having improved room temperature ductility and strength.

Inventors

  • 👤 Vinod K. Sikka

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 20:21
CPC Classifications
C; C22; C22C; C22C38/00; C22C38/06; C21; C21D; C21D8/00

Claims Analysis

Total Claims: 15
Claim 1
Independent Claim 94 words
A method for improving the room temperature ductility and high temperature strength of iron aluminide intermetallic alloys comprising: a) thermomechanically working said alloys by means which produce an elongated grain structure, the elongated grains making up said elongated grain structure being oriented generally in the primary working direction; b) heating said alloys at a temperature and for a period of time sufficient to produce a B2-type crystal structure; and c) rapidly cooling said alloys in a moisture free medium, retaining said B2-type crystal structure to provide alloys having improved room temperature ductility and strength.
Claim 2
Independent Claim 94 words
A method for improving the room temperature ductility and high temperature strength of iron aluminide intermetallic alloys comprising: a) thermomechanically working said alloys by means which produce an elongated grain structure, the elongated grains making up said elongated grain structure being oriented generally in the primary working direction; b) heating said alloys at a temperature and for a period of time sufficient to produce a B2-type crystal structure; and c) rapidly cooling said alloys in a moisture free medium, retaining said B2-type crystal structure to provide alloys having improved room temperature ductility and strength.
Claim 3
Dependent Claim 21 words
The method of claim 1 wherein said iron aluminide intermetallic alloy comprises an alloy based on the composition Fe 3 Al.
Claim 4
Dependent Claim 26 words
The method of claim 2 wherein greater than 95% of said elongated grains in said elongated grain structure have an aspect ratio greater than about 20.
Claim 5
Dependent Claim 25 words
The method of claim 2 wherein said iron aluminide intermetallic alloy is heated at a temperature in the range of 650° C. to 800° C.
Claim 6
Dependent Claim 30 words
The method of claim 2 wherein said iron aluminide intermetallic alloy is held at said temperature for a period of time in the range of 15 minutes to 2 hours.
Claim 7
Independent Claim 121 words
A method for improving the room temperature ductility and strength of an iron aluminide intermetallic alloy consisting essentially of 25 to 31 at. % aluminum, minor alloying constituents and iron comprising: a) thermomechanically working said alloy by means which produce an elongated grain structure, the elongated grains making up said elongated grain structure being oriented generally in the primary working direction and greater than 95% of said elongated grains having an aspect ratio greater than about 20; b) heating said alloys at a temperature and for a period of time sufficient to produce a B2-type crystal structure; and c) quenching said alloys in a moisture-free medium, retaining said B2-type crystal structure to provide alloys having improved room temperature ductility and strength.
Claim 8
Independent Claim 121 words
A method for improving the room temperature ductility and strength of an iron aluminide intermetallic alloy consisting essentially of 25 to 31 at. % aluminum, minor alloying constituents and iron comprising: a) thermomechanically working said alloy by means which produce an elongated grain structure, the elongated grains making up said elongated grain structure being oriented generally in the primary working direction and greater than 95% of said elongated grains having an aspect ratio greater than about 20; b) heating said alloys at a temperature and for a period of time sufficient to produce a B2-type crystal structure; and c) quenching said alloys in a moisture-free medium, retaining said B2-type crystal structure to provide alloys having improved room temperature ductility and strength.
Claim 9
Dependent Claim 34 words
The method of claim 6 wherein said alloy is heated in the temperature range of 650° C. to 800° C. for a period of time in the range of 15 minutes to 2 hours.
Claim 10
Dependent Claim 34 words
The method of claim 6 wherein said alloy is heated in the temperature range of 700° C. to 750° C. for a period of time in the range of 15 minutes to 2 hours.
Claim 11
Dependent Claim 166 words
A new method for improving the room temperature ductility and strength of an iron aluminide intermetallic alloy comprising: a) thermomechanically working an alloy consisting essentially of 25 to 31 at. % aluminum, up to a total of about 12 at. % of an element or combination of elements selected from the class consisting of Cr, Zr, Nb, Mo, B, C, and mixtures thereof, and the balance iron, by means which produce an elongated grain structure, the elongated grains making up said elongated grain structure being oriented generally in the primary working direction, greater than 95% of said elongated grains having an aspect ratio greater than about 20; b) heating said alloys at a temperature in the range of 650° C. to 800° C. for a period of time in the range of 15 minutes to 2 hours to produce a B2-type crystal structure; and c) quenching said alloys in oil to retain said B2-type crystal structure to provide alloys having improved room temperature ductility and strength.
Claim 12
Dependent Claim 166 words
A new method for improving the room temperature ductility and strength of an iron aluminide intermetallic alloy comprising: a) thermomechanically working an alloy consisting essentially of 25 to 31 at. % aluminum, up to a total of about 12 at. % of an element or combination of elements selected from the class consisting of Cr, Zr, Nb, Mo, B, C, and mixtures thereof, and the balance iron, by means which produce an elongated grain structure, the elongated grains making up said elongated grain structure being oriented generally in the primary working direction, greater than 95% of said elongated grains having an aspect ratio greater than about 20; b) heating said alloys at a temperature in the range of 650° C. to 800° C. for a period of time in the range of 15 minutes to 2 hours to produce a B2-type crystal structure; and c) quenching said alloys in oil to retain said B2-type crystal structure to provide alloys having improved room temperature ductility and strength.
Claim 13
Dependent Claim 21 words
The method of claim 9 wherein said thermomechanical working is achieved by any one of extrusion, drawing, rolling and mixtures thereof.
Claim 14
Dependent Claim 110 words
An improved ordered iron aluminide intermetallic alloy product having improved room temperature ductility and strength made by the process comprising: a) thermomechanically working said alloy by means which produce an elongated grain structure, the elongated grains in said elongated grain structure being oriented generally in the primary working direction and greater than 95% of said elongated grains having an aspect ratio greater than about 20; b) heating said alloys at a temperature and for a period of time sufficient to produce a B2-type crystal structure; and c) rapidly cooling said alloys in a moisture-free medium, retaining said B2-type crystal structure to provide alloys having improved room temperature ductility and strength.
Claim 15
Dependent Claim 110 words
An improved ordered iron aluminide intermetallic alloy product having improved room temperature ductility and strength made by the process comprising: a) thermomechanically working said alloy by means which produce an elongated grain structure, the elongated grains in said elongated grain structure being oriented generally in the primary working direction and greater than 95% of said elongated grains having an aspect ratio greater than about 20; b) heating said alloys at a temperature and for a period of time sufficient to produce a B2-type crystal structure; and c) rapidly cooling said alloys in a moisture-free medium, retaining said B2-type crystal structure to provide alloys having improved room temperature ductility and strength.

References Cited (Backward Citations)

US2768915A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1995-01-27 1995-07-29 1996-01-28 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1999-01-27 1999-07-29 2000-01-28 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2003-01-27 2003-07-29 2004-01-28 $7700.00 Window Closed / Lapsed

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