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US5080962A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for making silica optical devices and devices produced thereby

Assignee: GRYPHON VENTURES II LP
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Filing: 1989-04-05
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Granted: 1992-01-14
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Expires: 2009-04-05
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Abstract

Abstract An optical device made by treating, such as by a laser beam, a preselected portion of a silica gel monolithic body to obtain a density for the treated portion different from the density of the body.

Inventors

  • 👤 Larry L. Hench

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-31 10:08
CPC Classifications
C; C03; C03C; C03C1/00; C03C1/006; C03C23/00; C03C23/0005; C03C23/0025; G; G02; G02B; G02B6/00; G02B6/10; G02B6/12; G02B6/13; Y; Y10; Y10T; Y10T428/00; Y10T428/24; Y10T428/24942; Y10T428/24992

Claims Analysis

Total Claims: 26
Claim 1
Independent Claim 72 words
A method of making an optically transparent optical device comprising hydrolyzing a silica precursor to form a silica sol, gelling said sol to form an optically transparent monolithic body and heating a first preselected portion of the body to increase its density, while a second preselected portion is maintained cooler than the body, to obtain a density for the heated portion greater than the density of the unheated portion of the body.
Claim 2
Independent Claim 72 words
A method of making an optically transparent optical device comprising hydrolyzing a silica precursor to form a silica sol, gelling said sol to form an optically transparent monolithic body and heating a first preselected portion of the body to increase its density, while a second preselected portion is maintained cooler than the body, to obtain a density for the heated portion greater than the density of the unheated portion of the body.
Claim 3
Dependent Claim 18 words
The method of claim 1 wherein the second preselected portion is held in contact with a cooling medium.
Claim 4
Dependent Claim 16 words
The method of claim 1 wherein the first preselected portion is exposed to a laser beam.
Claim 5
Dependent Claim 15 words
The method of claim 1 wherein the first preselected portion is exposed to radiant energy.
Claim 6
Independent Claim 109 words
A method of making an optical device comprising making a silica monolithic body and treating a preselected portion of the body to obtain a density for the treated portion different from the density of the body wherein the body is heated to partially densify while maintaining a surface region of the body in contact with a cooling medium to create a thermal layer on said surface region, masking preselected areas of said thermal layer, etching away the thermal layer in the unmasked areas to expose areas of the partially densified body and heat treating the exposed areas of the partially densified body to increase the density of these areas.
Claim 7
Independent Claim 109 words
A method of making an optical device comprising making a silica monolithic body and treating a preselected portion of the body to obtain a density for the treated portion different from the density of the body wherein the body is heated to partially densify while maintaining a surface region of the body in contact with a cooling medium to create a thermal layer on said surface region, masking preselected areas of said thermal layer, etching away the thermal layer in the unmasked areas to expose areas of the partially densified body and heat treating the exposed areas of the partially densified body to increase the density of these areas.
Claim 8
Dependent Claim 10 words
An optical device made by the process of claim 5.
Claim 9
Dependent Claim 46 words
An optical device comprising a substrate of a silica gel monolith, a surface region of the substrate having a density lower than the main body of the substrate and another preselected region of the substrate having a density greater than the main body of the substrate.
Claim 10
Dependent Claim 46 words
An optical device comprising a substrate of a silica gel monolith, a surface region of the substrate having a density lower than the main body of the substrate and another preselected region of the substrate having a density greater than the main body of the substrate.
Claim 11
Dependent Claim 40 words
An optical device as in claim 7 wherein one face is covered by a thermal layer of lower density silica gel with portions of higher density than that of the main body of the substrate exposed through said thermal layer.
Claim 12
Dependent Claim 25 words
An optical device as in claim 8 wherein optical devices are mounted on said thermal layer and connected conductively to said portions of higher density.
Claim 13
Dependent Claim 31 words
An optical device as in claim 7 wherein conducting pathways of higher density than that of the main body of the substrate extend through said substrate parallel to said one face.
Claim 14
Dependent Claim 21 words
An optical device as in claim 10 wherein the conducting pathways also extend with a component normal to said one face.
Claim 15
Dependent Claim 21 words
An optical device as in claim 7 wherein the substrate contains regions of higher density in notional layers within the substrate.
Claim 16
Independent Claim 61 words
A method of making an optical device comprising hydrolyzing a SiO 2 precursor to form an SiO 2 sol, gelling said sol to form a substrate, treating one face of said substrate to densify preselected regions, hydrolyzing a silica precursor to form a SiO 2 gel layer on said treated face, and densifying preselected regions of said SiO 2 gel layer.
Claim 17
Independent Claim 61 words
A method of making an optical device comprising hydrolyzing a SiO 2 precursor to form an SiO 2 sol, gelling said sol to form a substrate, treating one face of said substrate to densify preselected regions, hydrolyzing a silica precursor to form a SiO 2 gel layer on said treated face, and densifying preselected regions of said SiO 2 gel layer.
Claim 18
Dependent Claim 28 words
The method of claim 13 wherein at least one of said preselected regions of said layer is conductively connected to one of said preselected regions of said substrate.
Claim 19
Dependent Claim 49 words
The method of claim 14 wherein a second SiO 2 layer is formed on the first mentioned layer and preselected regions of said second layer are densified and at least one of said densified regions is conductively connected to one of, said preselected regions of said first mentioned layer.
Claim 20
Dependent Claim 10 words
An optical device made by the process of claim 13.
Claim 21
Independent Claim 49 words
A method of making an optical device comprising hydrolyzing a SiO 2 precursor for form a SiO 2 sol, gelling said sol to form a substrate and treating one face of said substrate with an array of laser beams with preselected spacing to create preselected regions of increased density.
Claim 22
Independent Claim 49 words
A method of making an optical device comprising hydrolyzing a SiO 2 precursor for form a SiO 2 sol, gelling said sol to form a substrate and treating one face of said substrate with an array of laser beams with preselected spacing to create preselected regions of increased density.
Claim 23
Dependent Claim 24 words
A method of claim 17 wherein the array is a linear array that traverses the substrate face from one side to the opposite side.
Claim 24
Dependent Claim 40 words
The method of claim 18 wherein the face of the substrate is further treated by a linear array of laser beams that traverses the substrate in a direction at an angle to the traverse of the first mentioned linear array.
Claim 25
Dependent Claim 19 words
The method of claim 17 wherein the linear array is controlled to create interconnected preselected regions of increased density.
Claim 26
Dependent Claim 10 words
An optical device made by the process of claim 17.

References Cited (Backward Citations)

US3526603A Cited
US3878034A Cited
US4122240A Cited
US4169000A Cited
US4140548A Cited
US4286024A Cited
US4443493A Cited
US4432956A Cited
JPS6081031A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1995-01-13 1995-07-15 1996-01-14 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1999-01-13 1999-07-15 2000-01-14 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2003-01-13 2003-07-15 2004-01-14 $7700.00 Window Closed / Lapsed

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