Patent US5065775A successfully refreshed from Google Patents.
US5065775A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Tobacco processing
Assignee: RJ Reynolds Tobacco Co
•
Filing: 1990-02-23
•
Granted: 1991-11-19
•
Expires: 2010-02-23
Abstract
Abstract Denicotinized tobacco cut filler is provided by (i) providing an aqueous denicotinized tobacco extract, (ii) providing tobacco cut filler which has been extracted with an aqueous liquid, (iii) contacting the aqueous extract with the extracted cut filler, (iv) deliquoring the mixture of aqueous extract and extracted cut filler such that a certain level of the tobacco extract remains in contact with the extracted cut filler, and (v) drying the deliquored cut filler to provide a processed cut filler. Greater than 90 percent of the nicotine present in tobacco cut filler can be removed therefrom using such process steps.
Inventors
- 👤 Barry S. Fagg
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 15:52
CPC Classifications
A; A24; A24B; A24B15/00; A24B15/18; A24B15/24; A24B15/26
Claims Analysis
Total Claims: 44
Claim 1
Independent Claim
219 words
A process for altering the character of tobacco material, the process comprising the steps of: (a) providing extracted tobacco material by extracting tobacco material using a liquid extraction solvent and separating tobacco material not extracted by the solvent from the solvent and tobacco extract extracted by the solvent; (b) providing a tobacco extract by extracting tobacco material using a liquid extraction solvent, thereby providing a tobacco extract within the extraction solvent; (c) contacting the tobacco extract provided in step (b) within liquid extraction solvent with the extracted tobacco material provided in step (a) thereby providing a mixture of solvent, tobacco extract and extracted tobacco material; the mixture (i) including a weight of tobacco extractables greater than that weight of tobacco extract separated from the tobacco material in step (a), and (ii) including about 5 to about 40 percent extractables, based on the total weight of the solvent and tobacco extractables within the mixture; (d) separating the extracted tobacco material from a portion of the solvent and tobacco extract, thereby providing a mixture of solvent, tobacco extract and extracted tobacco material; the mixture thereby having a solvent content ranging from about 60 to about 90 weight percent, based on the total weight thereof; and (e) separating at least a portion of the solvent from the mixture provided in step (d).
Claim 2
Dependent Claim
219 words
A process for altering the character of tobacco material, the process comprising the steps of: (a) providing extracted tobacco material by extracting tobacco material using a liquid extraction solvent and separating tobacco material not extracted by the solvent from the solvent and tobacco extract extracted by the solvent; (b) providing a tobacco extract by extracting tobacco material using a liquid extraction solvent, thereby providing a tobacco extract within the extraction solvent; (c) contacting the tobacco extract provided in step (b) within liquid extraction solvent with the extracted tobacco material provided in step (a) thereby providing a mixture of solvent, tobacco extract and extracted tobacco material; the mixture (i) including a weight of tobacco extractables greater than that weight of tobacco extract separated from the tobacco material in step (a), and (ii) including about 5 to about 40 percent extractables, based on the total weight of the solvent and tobacco extractables within the mixture; (d) separating the extracted tobacco material from a portion of the solvent and tobacco extract, thereby providing a mixture of solvent, tobacco extract and extracted tobacco material; the mixture thereby having a solvent content ranging from about 60 to about 90 weight percent, based on the total weight thereof; and (e) separating at least a portion of the solvent from the mixture provided in step (d).
Claim 3
Dependent Claim
18 words
The process of claim 1 further including altering the chemical composition of the extract provided in step (b).
Claim 4
Dependent Claim
19 words
The process of claim 1 whereby at least one additive is incorporated into the extract provided in step (b).
Claim 5
Dependent Claim
21 words
The process of claim 3 whereby the solvent is a liquid having an aqueous character, and the selected substance includes nicotine.
Claim 6
Dependent Claim
21 words
The process of claim 3 whereby at least one selected substance is removed from the tobacco extract provided in step (b).
Claim 7
Dependent Claim
21 words
The process of claim 5 whereby the solvent is a liquid having an aqueous character, and the selected substance includes nicotine.
Claim 8
Dependent Claim
24 words
The process of claim 1, 2, 3 or 5 further including altering the chemical composition of the extracted tobacco material provided in step (a).
Claim 9
Dependent Claim
40 words
The process of claim 7 whereby the amount of tobacco extractables within the mixture provided in step (c) ranges from about 10 to about 30 percent, based on the total weight of the solvent and tobacco extractables within the mixture.
Claim 10
Dependent Claim
40 words
The process of claim 7 whereby the amount of tobacco extractables within the mixture provided in step (c) ranges from about 15 to about 25 percent, based on the total weight of the solvent and tobacco extractables within the mixture.
Claim 11
Dependent Claim
33 words
The process of claim 7 whereby the solvent content of the mixture provided in step (d) ranges from about 65 to about 85 weight percent, based on the total weight of that mixture.
Claim 12
Dependent Claim
49 words
The process of claim 7 whereby the solvent is a liquid having an aqueous character, and sufficient solvent is separated from the mixture in step (e) to provide a mixture of tobacco extract and extracted tobacco material having a solvent content between about 10 and about 15 weight percent.
Claim 13
Dependent Claim
19 words
The process of claim 1, 2, 3 or 5 whereby the solvent is a liquid having an aqueous character.
Claim 14
Dependent Claim
19 words
The process of claim 12 whereby the liquid having an aqueous character is greater than 90 weight percent water.
Claim 15
Dependent Claim
44 words
The process of claim 1, 2, 3 or 5 whereby the amount of tobacco extractables within the mixture provided in step (c) ranges from about 10 to about 30 percent, based on the total weight of the solvent and tobacco extractables within the mixture.
Claim 16
Dependent Claim
44 words
The process of claim 1, 2, 3 or 5 whereby the amount of tobacco extractables within the mixture provided in step (c) ranges from about 15 to about 25 percent, based on the total weight of the solvent and tobacco extractables within the mixture.
Claim 17
Dependent Claim
37 words
The process of claim 1, 2, 3 or 5 whereby the solvent content of the mixture provided in step (d) ranges from about 65 to about 85 weight percent, based on the total weight of that mixture.
Claim 18
Dependent Claim
53 words
The process of claim 1, 2, 3 or 5 whereby the solvent is a liquid having an aqueous character, and sufficient solvent is separated from the mixture in step (e) to provide a mixture of tobacco extract and extracted tobacco material having a solvent content between about 10 and about 15 weight percent.
Claim 19
Dependent Claim
34 words
The process of claim 1 whereby the solvent is a liquid having an aqueous character, and the tobacco extract provided in step (b) is provided in a spray dried form prior to step (c).
Claim 20
Dependent Claim
192 words
A process for altering the character of tobacco material, the process comprising the steps of: (a) providing extracted tobacco material by extracting tobacco material using a liquid extraction solvent and separating tobacco material not extracted by the solvent from the solvent and tobacco extract extracted by the solvent; (b) providing a tobacco extract by extracting tobacco material using a liquid extraction solvent, thereby providing a tobacco extract within the extraction solvent; (c) contacting the tobacco extract provided in step (b) within liquid extraction solvent with the extracted tobacco material provided in step (a) thereby providing a mixture of solvent, tobacco extract and extracted tobacco material; the weight of solvent within the mixture being more than 3 times that of the weight of the extracted tobacco material within the mixture; (d) separating the extracted tobacco material from a portion of the solvent and tobacco extract, thereby providing a mixture of solvent, tobacco extract and extracted tobacco material; the mixture thereby having a solvent content of at least about 60 percent based on the total weight thereof; and (e) separating at least a portion of the solvent from the mixture provided in step (d).
Claim 21
Dependent Claim
192 words
A process for altering the character of tobacco material, the process comprising the steps of: (a) providing extracted tobacco material by extracting tobacco material using a liquid extraction solvent and separating tobacco material not extracted by the solvent from the solvent and tobacco extract extracted by the solvent; (b) providing a tobacco extract by extracting tobacco material using a liquid extraction solvent, thereby providing a tobacco extract within the extraction solvent; (c) contacting the tobacco extract provided in step (b) within liquid extraction solvent with the extracted tobacco material provided in step (a) thereby providing a mixture of solvent, tobacco extract and extracted tobacco material; the weight of solvent within the mixture being more than 3 times that of the weight of the extracted tobacco material within the mixture; (d) separating the extracted tobacco material from a portion of the solvent and tobacco extract, thereby providing a mixture of solvent, tobacco extract and extracted tobacco material; the mixture thereby having a solvent content of at least about 60 percent based on the total weight thereof; and (e) separating at least a portion of the solvent from the mixture provided in step (d).
Claim 22
Dependent Claim
34 words
The process of claim 19 whereby the weight of the solvent within the mixture provided in step (c) is more than about 6 times that weight of the extracted tobacco material within the mixture.
Claim 23
Dependent Claim
34 words
The process of claim 19 whereby the weight of the solvent within the mixture provided in step (c) is more than about 10 times that weight of the extracted tobacco material within the mixture.
Claim 24
Dependent Claim
18 words
The process of claim 21 further including altering the chemical composition of the extract provided in step (b).
Claim 25
Dependent Claim
19 words
The process of claim 21 whereby at least one additive is incorporated into the extract provided in step (b).
Claim 26
Dependent Claim
23 words
The process of claim 21 or 23 whereby at least one selected substance is removed from the tobacco extract provided in step (b).
Claim 27
Dependent Claim
20 words
The process of claim 21 further including altering the chemical composition of the extracted tobacco material provided in step (a).
Claim 28
Dependent Claim
15 words
The process of claim 21 whereby the solvent is a liquid having an aqueous character.
Claim 29
Dependent Claim
19 words
The process of claim 26 whereby the liquid having an aqueous character is greater than 90 weight percent water.
Claim 30
Dependent Claim
49 words
The process of claim 21 whereby the solvent is a liquid having an aqueous character, and sufficient solvent is separated from the mixture in step (e) to provide a mixture of tobacco extract and extracted tobacco material having a solvent content between about 10 and about 15 weight percent.
Claim 31
Dependent Claim
34 words
The process of claim 19 whereby the weight of the solvent within the mixture provided in step (c) is more than about 15 times that weight of the extracted tobacco material within the mixture.
Claim 32
Dependent Claim
35 words
The process of claim 21 or 29 whereby the solvent content of the mixture provided in step (d) ranges from about 60 to about 90 weight percent, based on the total weight of that mixture.
Claim 33
Dependent Claim
49 words
The process of claim 30 whereby the solvent is a liquid having an aqueous character, and sufficient solvent is separated from the mixture in step (e) to provide a mixture of tobacco extract and extracted tobacco material having a solvent content between about 10 and about 15 weight percent.
Claim 34
Dependent Claim
35 words
The process of claim 21 or 29 whereby the solvent content of the mixture provided in step (d) ranges from about 65 to about 85 weight percent, based on the total weight of that mixture.
Claim 35
Dependent Claim
34 words
The process of claim 19 whereby the solvent is a liquid having an aqueous character, and the tobacco extract provided in step (b) is provided in a spray dried form prior to step (c).
Claim 36
Dependent Claim
232 words
A process for removing at least one selected substance from tobacco material, the process comprising the steps of: (a) providing extracted tobacco material by extracting tobacco material using a liquid extraction solvent and separating tobacco material not extracted by the solvent from the solvent and tobacco extract extracted by the solvent; (b) providing a processed tobacco extract by (i) extracting tobacco material using a liquid extraction solvent, thereby providing a tobacco extract within the extraction solvent, and (ii) removing at least one selected substance from the tobacco extract; (c) contacting the processed tobacco extract within liquid extraction solvent with the extracted tobacco material provided in step (a) thereby providing a mixture of solvent, tobacco extract and extracted tobacco material; the mixture (i) including a weight of tobacco extractables greater than that weight of tobacco extract separated from the tobacco material in step (a), and (ii) including about 5 to about 40 percent tobacco extractables, based on the total weight of the solvent and tobacco extractables within the mixture; (d) separating the extracted tobacco material from a portion of the solvent and tobacco extract, thereby providing a mixture of solvent, tobacco extract and extracted tobacco material; the mixture having a solvent content of about 60 to about 90 weight percent, based on the total weight thereof; and (e) separating at least a portion of the solvent from the mixture provided in step (d).
Claim 37
Dependent Claim
232 words
A process for removing at least one selected substance from tobacco material, the process comprising the steps of: (a) providing extracted tobacco material by extracting tobacco material using a liquid extraction solvent and separating tobacco material not extracted by the solvent from the solvent and tobacco extract extracted by the solvent; (b) providing a processed tobacco extract by (i) extracting tobacco material using a liquid extraction solvent, thereby providing a tobacco extract within the extraction solvent, and (ii) removing at least one selected substance from the tobacco extract; (c) contacting the processed tobacco extract within liquid extraction solvent with the extracted tobacco material provided in step (a) thereby providing a mixture of solvent, tobacco extract and extracted tobacco material; the mixture (i) including a weight of tobacco extractables greater than that weight of tobacco extract separated from the tobacco material in step (a), and (ii) including about 5 to about 40 percent tobacco extractables, based on the total weight of the solvent and tobacco extractables within the mixture; (d) separating the extracted tobacco material from a portion of the solvent and tobacco extract, thereby providing a mixture of solvent, tobacco extract and extracted tobacco material; the mixture having a solvent content of about 60 to about 90 weight percent, based on the total weight thereof; and (e) separating at least a portion of the solvent from the mixture provided in step (d).
Claim 38
Dependent Claim
33 words
The process of claim 34 whereby the amount of processed tobacco extract within extraction solvent ranges from about 10 to about 30 percent, based on the total weight of the extract and solvent.
Claim 39
Dependent Claim
33 words
The process of claim 34 whereby the amount of processed tobacco extract within extraction solvent ranges from about 15 to about 25 percent, based on the total weight of the extract and solvent.
Claim 40
Dependent Claim
41 words
The process of claim 34 whereby the solvent content of the mixture provided in step (d) ranges from about 65 to about 85 percent, based on the total weight of the solvent, tobacco extract and tobacco material insoluble in the solvent.
Claim 41
Dependent Claim
16 words
The process of claim 34 whereby the extraction solvent is a liquid having an aqueous character.
Claim 42
Dependent Claim
11 words
The process of claim 34 whereby the selected substance includes nicotine.
Claim 43
Dependent Claim
52 words
The process of claim 34 whereby the solvent is a solvent having an aqueous character, and sufficient solvent is separated from the mixture in step (e) to provide a mixture of tobacco extract and tobacco material insoluble in the solvent having a moisture level between about 10 and about 15 weight percent.
Claim 44
Dependent Claim
34 words
The process of claim 34 whereby the solvent is a liquid having an aqueous character, and the processed tobacco extract provided in step (b) is provided in spray dried form prior to step (c).
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| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
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| 3.5 Years (Year 4) | 1994-11-18 | 1995-05-20 | 1995-11-19 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1998-11-18 | 1999-05-20 | 1999-11-19 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2002-11-18 | 2003-05-20 | 2003-11-19 | $7700.00 | Window Closed / Lapsed |