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US4933094A Expired / Lapsed US ⏱️ 0.0 years remaining

Method and apparatus for separating liquid components from a liquid mixture

Assignee: Lubrizol Specialty Products Inc
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Filing: 1988-09-30
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Granted: 1990-06-12
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Expires: 2008-09-30
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Abstract

Abstract Method and apparatus for separating oil-water mixtures in which the oil is present as droplets so as to comprise the disperse phase, the mean droplet size being greater than 56.7 micron, using a cyclone separator having a swirl coefficient, S, in the range S'≦S≦S.sup.u2, where S'=-0.46 φ+31 or S'=2, whichever is the greater, and S u2 =0.26 φ+31.6, where φ is the mean droplet size in micron. The swirl coefficient is defined as ##EQU1## where d i is the effective diameter at the inlet to the separator d 2 is the nominal separator diameter at a downstream location, and A i is the total effective inlet area.

Inventors

  • 👤 Charles M. Kalnins

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-31 05:16
CPC Classifications
B; B04; B04C; B04C5/00; B04C5/08; B04C5/081; B01; B01D; B01D17/00; B01D17/02; B01D17/0217

Claims Analysis

Total Claims: 20
Claim 1
Independent Claim 237 words
A method of separating a mixture of oil and water, in which the oil is present in droplet form as a disperse phase and the water is present as a continuous phase, by providing a cyclone separator having a single continuous taper change possibly with portions of constant diameter interposed therewithin or at either or both ends which can separate oil-water mixtures substantially as effectively as a cyclone separator including three separately defined portions, subjecting the mixture to centrifugal action in said cyclone separator of the kind having an elongate axially extending separating chamber defined as a surface of revolution about the axis thereof, the separator having at least one inlet for inlet of said mixture to be separated, with a tangential component of motion about said axis, an overflow outlet for outlet of separated oil, and an underflow outlet for outlet of separated water, the method comprising admitting the mixture to said separating chamber via said inlet to cause the mixture to undergo centrifugal action and to direct at least a substantial part of said oil to said overflow outlet and of said water to said underflow outlet, the mixture having therein said oil in the form of droplets the mean droplet size of which lies in the range 22 to 50 micron and said cyclone separator being characterised in the `S` is greater than 12.5, where S is the swirl coefficient of the cyclone separator.
Claim 2
Independent Claim 237 words
A method of separating a mixture of oil and water, in which the oil is present in droplet form as a disperse phase and the water is present as a continuous phase, by providing a cyclone separator having a single continuous taper change possibly with portions of constant diameter interposed therewithin or at either or both ends which can separate oil-water mixtures substantially as effectively as a cyclone separator including three separately defined portions, subjecting the mixture to centrifugal action in said cyclone separator of the kind having an elongate axially extending separating chamber defined as a surface of revolution about the axis thereof, the separator having at least one inlet for inlet of said mixture to be separated, with a tangential component of motion about said axis, an overflow outlet for outlet of separated oil, and an underflow outlet for outlet of separated water, the method comprising admitting the mixture to said separating chamber via said inlet to cause the mixture to undergo centrifugal action and to direct at least a substantial part of said oil to said overflow outlet and of said water to said underflow outlet, the mixture having therein said oil in the form of droplets the mean droplet size of which lies in the range 22 to 50 micron and said cyclone separator being characterised in the `S` is greater than 12.5, where S is the swirl coefficient of the cyclone separator.
Claim 3
Dependent Claim 19 words
A method as claimed in claim 1 wherein said mean droplet size lies in the range 56.7 to 70.
Claim 4
Dependent Claim 22 words
A method as claimed in claim 1 wherein said mean droplet size is in the range 56.7 to 63 micron and S'≦S<5.
Claim 5
Independent Claim 203 words
A method of separating a mixture of oil and water, in which the oil is present in droplet form as a disperse phase and the water is present as a continuous phase, by C1 subjecting the mixture to centrifugal action in said cyclone separator of the kind having an elongate axially extending separating chamber defined as a surface of revolution about the axis thereof, the separator having at least one inlet for inlet of said mixture to be separated, with a tangential component of motion about said axis, an overflow outlet for separated said oil, and an underflow outlet for outlet of separated said water, the method comprising admitting the mixture to said separating chamber via said inlet to cause the mixture to undergo centrifugal action and to direct at least a substantial part of said oil to said overflow outlet and of said water to said underflow outlet, the mixture having therein said oil in the form of droplets the means droplet size of which at least 56.7 micron and said cyclone separator being characterized in that: S"≦S≦S u2 , where S"=-0.32 φ+18.24, or S"=5, whichever is the greater, φ being the mean droplet size in micron, and S u2 =0.26 φ31.6.
Claim 6
Independent Claim 203 words
A method of separating a mixture of oil and water, in which the oil is present in droplet form as a disperse phase and the water is present as a continuous phase, by C1 subjecting the mixture to centrifugal action in said cyclone separator of the kind having an elongate axially extending separating chamber defined as a surface of revolution about the axis thereof, the separator having at least one inlet for inlet of said mixture to be separated, with a tangential component of motion about said axis, an overflow outlet for separated said oil, and an underflow outlet for outlet of separated said water, the method comprising admitting the mixture to said separating chamber via said inlet to cause the mixture to undergo centrifugal action and to direct at least a substantial part of said oil to said overflow outlet and of said water to said underflow outlet, the mixture having therein said oil in the form of droplets the means droplet size of which at least 56.7 micron and said cyclone separator being characterized in that: S"≦S≦S u2 , where S"=-0.32 φ+18.24, or S"=5, whichever is the greater, φ being the mean droplet size in micron, and S u2 =0.26 φ31.6.
Claim 7
Dependent Claim 9 words
A method as claimed in claim 4 wherein 56.7≦φ≦70.
Claim 8
Independent Claim 233 words
A method of separating a mixture of oil and water in which the oil is present in droplet form as a disperse phase and the water is present as a continuous phase, by providing a cyclone separator having a single continuous taper change possibly with portions of constant diameter interposed therewithin or at either or both ends which can separate oil-water mixtures substantially as effectively as a cyclone separator including three separately defined portions, subjecting the mixture to centrifugal action in said cyclone separator of the kind having an elongate axially extending separating chamber defined as a surface of revolution about the axis thereof, the separator having at least one inlet for inlet of said mixture to be separated, with a tangential component of motion about said axis, an overflow outlet for outlet of separated oil, and an underflow outlet for outlet of separated water, the method comprising admitting the mixture to said separating chamber via said inlet to cause the mixture to undergo centrifugal action and to direct at least a substantial part of said oil to said overflow outlet and of said water to said underflow outlet, the mixture having therein said oil in the form of droplets the means droplet size of which lies in the range 28 to 42 micron and said cyclone separator being characterized in that 8≦S≦25, where `S` is the swirl coefficient of the cyclone separator.
Claim 9
Independent Claim 233 words
A method of separating a mixture of oil and water in which the oil is present in droplet form as a disperse phase and the water is present as a continuous phase, by providing a cyclone separator having a single continuous taper change possibly with portions of constant diameter interposed therewithin or at either or both ends which can separate oil-water mixtures substantially as effectively as a cyclone separator including three separately defined portions, subjecting the mixture to centrifugal action in said cyclone separator of the kind having an elongate axially extending separating chamber defined as a surface of revolution about the axis thereof, the separator having at least one inlet for inlet of said mixture to be separated, with a tangential component of motion about said axis, an overflow outlet for outlet of separated oil, and an underflow outlet for outlet of separated water, the method comprising admitting the mixture to said separating chamber via said inlet to cause the mixture to undergo centrifugal action and to direct at least a substantial part of said oil to said overflow outlet and of said water to said underflow outlet, the mixture having therein said oil in the form of droplets the means droplet size of which lies in the range 28 to 42 micron and said cyclone separator being characterized in that 8≦S≦25, where `S` is the swirl coefficient of the cyclone separator.
Claim 10
Dependent Claim 12 words
A method as claimed in claim 4 wherein 56.7≦φ≦63 and S'=-0.46 φ+31.
Claim 11
Dependent Claim 9 words
A method as claim in claim 7, wherein S≦25.
Claim 12
Dependent Claim 9 words
A method as claimed in claim 4 wherein S≦25.
Claim 13
Independent Claim 206 words
A method of separating a mixture of oil and water, in which the oil is present in droplet form as a disperse phase and the water is present as a continuous phase, by C1 subjecting the mixture to centrifugal action in said cyclone separator of the kind having an elongate axially extending separating chamber defined as a surface of revolution about the axis thereof, the separator having at least one inlet for inlet of said mixture to be separated, with a tangential component of motion about said axis, an overflow outlet for separated said oil, and an underflow outlet for outlet of separated said water, the method comprising admitting the mixture to said separating chamber via said inlet to cause the mixture to undergo centrifugal action and to direct at least a substantial part of said oil to said overflow outlet and of said water to said underflow outlet, the mixture having therein said oil in the form of droplets the mean droplet size of which at least 56.7 micron and said cyclone separator being characterised in that: S'≦S≦S l , where S'=-0.46 φ+31, or S'=2, which ever is the greater, and where φ is the means droplet size in micron, and S ul =0.32 φ+16.8.
Claim 14
Independent Claim 206 words
A method of separating a mixture of oil and water, in which the oil is present in droplet form as a disperse phase and the water is present as a continuous phase, by C1 subjecting the mixture to centrifugal action in said cyclone separator of the kind having an elongate axially extending separating chamber defined as a surface of revolution about the axis thereof, the separator having at least one inlet for inlet of said mixture to be separated, with a tangential component of motion about said axis, an overflow outlet for separated said oil, and an underflow outlet for outlet of separated said water, the method comprising admitting the mixture to said separating chamber via said inlet to cause the mixture to undergo centrifugal action and to direct at least a substantial part of said oil to said overflow outlet and of said water to said underflow outlet, the mixture having therein said oil in the form of droplets the mean droplet size of which at least 56.7 micron and said cyclone separator being characterised in that: S'≦S≦S l , where S'=-0.46 φ+31, or S'=2, which ever is the greater, and where φ is the means droplet size in micron, and S ul =0.32 φ+16.8.
Claim 15
Dependent Claim 9 words
A method as claimed in claim 10 wherein 56.7≦φ≦70.
Claim 16
Independent Claim 233 words
A method of separating a mixture of oil and water, in which the oil is present in droplet form as a disperse phase and the water is present as a continuous phase, by providing a cyclone separator having a single continuous taper change possibly with portions of constant diameter interposed therewith or at either or both ends which can separate oil-water mixtures substantially as effectively as a cyclone separator including three separately defined portions, subjecting the mixture to centrifugal action in said cyclone separator of the kind having an elongate axially extending separating chamber defined as a surface of revolution about the axis thereof, the separator having at least one inlet for inlet of said mixture to be separated, with a tangential component of motion about said axis, an overflow outlet for outlet of separated oil, and an underflow outlet for outlet of separated water, the method comprising admitting the mixture to said separating chamber via said inlet to cause the mixture to undergo centrifugal action and to direct at least a substantial part of said oil to said overflow outlet and of said water to said underflow outlet, the mixture having therein said oil in the form of droplets the means droplet size of which lies in the range 33 to 38 micron and said cyclone separator being characterised in that 8≦S≦28, where `S` is the swirl coefficient of the cyclone separator.
Claim 17
Independent Claim 233 words
A method of separating a mixture of oil and water, in which the oil is present in droplet form as a disperse phase and the water is present as a continuous phase, by providing a cyclone separator having a single continuous taper change possibly with portions of constant diameter interposed therewith or at either or both ends which can separate oil-water mixtures substantially as effectively as a cyclone separator including three separately defined portions, subjecting the mixture to centrifugal action in said cyclone separator of the kind having an elongate axially extending separating chamber defined as a surface of revolution about the axis thereof, the separator having at least one inlet for inlet of said mixture to be separated, with a tangential component of motion about said axis, an overflow outlet for outlet of separated oil, and an underflow outlet for outlet of separated water, the method comprising admitting the mixture to said separating chamber via said inlet to cause the mixture to undergo centrifugal action and to direct at least a substantial part of said oil to said overflow outlet and of said water to said underflow outlet, the mixture having therein said oil in the form of droplets the means droplet size of which lies in the range 33 to 38 micron and said cyclone separator being characterised in that 8≦S≦28, where `S` is the swirl coefficient of the cyclone separator.
Claim 18
Dependent Claim 11 words
A method as claimed in claim 10 wherein 56.7≦φ≦63 and S'=-0.46.
Claim 19
Dependent Claim 9 words
A method as claimed in claim 13 wherein S≦19.
Claim 20
Dependent Claim 9 words
A method as claimed in claim 10 wherein S≦19.

References Cited (Backward Citations)

US4764287A Cited
US4793924A Cited
US4749490A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1993-06-11 1993-12-11 1994-06-12 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1997-06-11 1997-12-11 1998-06-12 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2001-06-11 2001-12-11 2002-06-12 $7700.00 Window Closed / Lapsed

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