US4915747A
Expired / Lapsed
US
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Aluminum-lithium alloys and process therefor
Assignee: Alcoa Corp
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Filing: 1988-07-01
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Granted: 1990-04-10
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Expires: 2008-07-01
Abstract
Abstract Disclosed is a method of producing an unrecrystallized, thin gauge cold rolled aluminum-lithium sheet product having improved levels of strength and fracture toughness. The method comprises the steps of providing a body of a lithium containing aluminum base alloy, heating the body to a hot rolling temperature, and hot rolling the body to a first intermediate sheet product. After cold rolling to a second intermediate thickness, the sheet product is reheated and hot rolled to produce a final sheet product while avoiding substantial recrystallization there, the hot rolling adapted to relieve stored energy capable of initiating recrystallization during a subsequent heat treating step. Thereafter, the sheet product is solution heat treated, quenched and aged to provide a substantially unrecrystallized product having improved levels of strength and fracture toughness.
Inventors
- 👤 Chul W. Cho
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-30 02:33
CPC Classifications
C; C22; C22F; C22F1/00; C22F1/04; C22F1/047; C22F1/053; C22F1/057
Claims Analysis
Total Claims: 18
Claim 1
Independent Claim
116 words
A method of producing an unrecrystallized wrought aluminum-lithium product having improved levels of strength and fracture toughness, the method comprising the steps of: (a) providing a body of a lithium containing aluminum base alloy; (b) heating the body to a hot working temperature; (c) hot working the body to a first product; (d) cold working said first product to a second wrought product; (e) reheating said second wrought product while avoiding substantially recrystallization thereof, the reheating adapted to relieve stored energy capable of causing recrystallization during a subsequent heat treating step; and (f) solution heat treating, quenching and aging said reheated product to provide a substantially unrecrystallized product having improved levels of strength and fracture toughness.
Claim 2
Independent Claim
116 words
A method of producing an unrecrystallized wrought aluminum-lithium product having improved levels of strength and fracture toughness, the method comprising the steps of: (a) providing a body of a lithium containing aluminum base alloy; (b) heating the body to a hot working temperature; (c) hot working the body to a first product; (d) cold working said first product to a second wrought product; (e) reheating said second wrought product while avoiding substantially recrystallization thereof, the reheating adapted to relieve stored energy capable of causing recrystallization during a subsequent heat treating step; and (f) solution heat treating, quenching and aging said reheated product to provide a substantially unrecrystallized product having improved levels of strength and fracture toughness.
Claim 3
Dependent Claim
25 words
The method in accordance with claim 1 wherein reheating at a temperature is performed at a temperature in the range of 750° to 920° F.
Claim 4
Dependent Claim
33 words
The method in accordance with claim 2 wherein the reheating treatment is started at a temperature of not lower than 750° F. and finished at a temperature of not greater than 920° F.
Claim 5
Dependent Claim
41 words
The method in accordance with claim 3 wherein the reheating treatment is started at a temperature not lower than 750° F. and finished at a temperature at least 50° to 150° higher than the temperature at which said treatment is started.
Claim 6
Dependent Claim
22 words
The method in accordance with claim 4 wherein the temperature is increased at a rate of 3° to 25° F. per hour.
Claim 7
Dependent Claim
22 words
The method in accordance with claim 4 wherein the temperature is increased at a rate of 5° to 15° F. per hour.
Claim 8
Dependent Claim
28 words
The method in accordance with claim 4 wherein said reheating includes soaking said product for at least one-half hour at the temperature at which said treatment is finished.
Claim 9
Independent Claim
168 words
A method of producing an unrecrystallized wrought aluminum-lithium product having improved levels of strength and fracture toughness, the method comprising the steps of: (a) providing a body of a lithium containing aluminum base alloy; (b) heating the body to a hot working temperature; (c) hot working the body to a first product; (d) cold working said first product to a second wrought product; (e) subjecting said second wrought product to a reheating treatment starting at a temperature of not lower than 750° F. and finishing at a temperature of at least 50° to 150° F. higher than the starting temperature, the increase in temperature being at the rate of 3° to 25° F. per hour, said reheating treatment being performed while avoiding substantial recrystallization thereof, the reheating treatment adapted to relieve stored energy capable of causing recrystallization during a subsequent heat treating step; and (f) solution heat treating, quenching and aging said reheated product to provide a substantially unrecrystallized product having improved levels of strength and fracture toughness.
Claim 10
Independent Claim
168 words
A method of producing an unrecrystallized wrought aluminum-lithium product having improved levels of strength and fracture toughness, the method comprising the steps of: (a) providing a body of a lithium containing aluminum base alloy; (b) heating the body to a hot working temperature; (c) hot working the body to a first product; (d) cold working said first product to a second wrought product; (e) subjecting said second wrought product to a reheating treatment starting at a temperature of not lower than 750° F. and finishing at a temperature of at least 50° to 150° F. higher than the starting temperature, the increase in temperature being at the rate of 3° to 25° F. per hour, said reheating treatment being performed while avoiding substantial recrystallization thereof, the reheating treatment adapted to relieve stored energy capable of causing recrystallization during a subsequent heat treating step; and (f) solution heat treating, quenching and aging said reheated product to provide a substantially unrecrystallized product having improved levels of strength and fracture toughness.
Claim 11
Dependent Claim
26 words
The method in accordance with claim 8 wherein after the reheating treatment to said higher temperature, said second product is soaked for at least one-half hour.
Claim 12
Dependent Claim
124 words
An aluminum base alloy wrought product having improved levels of strength and fracture toughness in response to a reheating treatment, the product comprised of 0.5 to 4.0 wt. % Li, 0 to 5.0 wt. % Mg, up to 5.0 wt. % Cu, 0 to 2.0 wt. % Mn, 0 to 7.0 wt. % Zn, 0.5 wt. % max. Fe, 0.5 wt. % max. Si, and 0 to 1 wt. % Zr the balance substantially aluminum, incidental elements and impurities, the product having improved levels of strength and fracture toughness resulting from reheating said product to a temperature below recrystallization prior to solution heat treating, the reheating for a time and temperature effective in relieving stored energy capable of causing recrystallization during solution heat treating.
Claim 13
Dependent Claim
124 words
An aluminum base alloy wrought product having improved levels of strength and fracture toughness in response to a reheating treatment, the product comprised of 0.5 to 4.0 wt. % Li, 0 to 5.0 wt. % Mg, up to 5.0 wt. % Cu, 0 to 2.0 wt. % Mn, 0 to 7.0 wt. % Zn, 0.5 wt. % max. Fe, 0.5 wt. % max. Si, and 0 to 1 wt. % Zr the balance substantially aluminum, incidental elements and impurities, the product having improved levels of strength and fracture toughness resulting from reheating said product to a temperature below recrystallization prior to solution heat treating, the reheating for a time and temperature effective in relieving stored energy capable of causing recrystallization during solution heat treating.
Claim 14
Dependent Claim
33 words
The product in accordance with claim 10 wherein said reheating treatment is started at a temperature of not lower than 750° F. and finishes at a temperature of not greater than 920° F.
Claim 15
Dependent Claim
41 words
The product in accordance with claim 10 wherein the reheating treatment is started at a temperature not lower than 750° F. and finished at a temperature at least 50° to 150° higher than the temperature at which said treatment is started.
Claim 16
Dependent Claim
22 words
The product in accordance with claim 12 wherein the temperature is increased at a rate of 3° to 25° F. per hour.
Claim 17
Dependent Claim
22 words
The product in accordance with claim 12 wherein the temperature is increased at a rate of 5° to 15° F. per hour.
Claim 18
Dependent Claim
23 words
The product in accordance with claim 12 wherein said reheating includes soaking said product for at least one-half hour at the finishing temperature.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1993-04-09 | 1993-10-09 | 1994-04-10 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1997-04-09 | 1997-10-09 | 1998-04-10 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2001-04-09 | 2001-10-09 | 2002-04-10 | $7700.00 | Window Closed / Lapsed |