US4409038A — Method of producing Al-Li alloys with improved pr…

Claim 1

Independent Claim 145 words

A method for producing a dispersion-strengthened aluminum-base alloy of improved mechanical and thermal properties comprising degassing and compacting at elevated temperature below liquation temperature a mechanically alloyed powder consisting essentially of aluminum, lithium, oxygen and carbon, and optionally one or more of the group selected from magnesium, copper and iron, the lithium level being at least about 1.7 up to about 3.5 weight %, the dispersoid comprising the carbon and oxygen, and being present in a small but effective amount for increased strength up to about 8 volume %, and the balance, apart from said optional components, essentially aluminum, and subjecting the compacted powder to a solution treatment at a temperature not exceeding the maximum degassing and/or compaction temperature, cooling the solution treated alloy, and aging the alloy at an elevated temperature for a period of time sufficient to permit age hardening of the alloy.

Claim 2

Independent Claim 145 words

A method for producing a dispersion-strengthened aluminum-base alloy of improved mechanical and thermal properties comprising degassing and compacting at elevated temperature below liquation temperature a mechanically alloyed powder consisting essentially of aluminum, lithium, oxygen and carbon, and optionally one or more of the group selected from magnesium, copper and iron, the lithium level being at least about 1.7 up to about 3.5 weight %, the dispersoid comprising the carbon and oxygen, and being present in a small but effective amount for increased strength up to about 8 volume %, and the balance, apart from said optional components, essentially aluminum, and subjecting the compacted powder to a solution treatment at a temperature not exceeding the maximum degassing and/or compaction temperature, cooling the solution treated alloy, and aging the alloy at an elevated temperature for a period of time sufficient to permit age hardening of the alloy.

Claim 3

Dependent Claim 21 words

A method according to claim 1, wherein solution treatment is carried out at substantially the same temperature as the compaction temperature.

Claim 4

Dependent Claim 52 words

A method according to claim 1, wherein degassing and/or compaction is carried out at a temperature from about 400° C. to about 510° C. and solution treatment is at a temperature from about 400° C. to 510° C. for sufficient time to bring the alloys to temperature up to about 4 hours.

Claim 5

Dependent Claim 17 words

A method according to claim 1, wherein cooling from the solution treatment temperature is by water quenching.

Claim 6

Dependent Claim 31 words

A method according to claim 1, wherein aging is effected at a temperature in the range of about 95° C. to about 260° C. for about 1 to about 48 hours.

Claim 7

Dependent Claim 31 words

A method according to claim 1, wherein aging is effected at a temperature in the range of about 120° C. to about 230° C. for about 1 to about 24 hours.

Claim 8

Dependent Claim 37 words

A method according to claim 1, wherein compaction is carried out at 510° C., solution treatment at about 510° C. for about 0.5 hours, and aging at about 177° C. for about 1 to about 4 hours.

Claim 9

Dependent Claim 52 words

A method according to claim 1, wherein the mechanical alloyed dispersion strengthened powder has on compaction a composition consisting essentially of, by weight, from about 1.7 up to about 3.5% lithium, from about 0.4% up to about 1.5% oxygen, from about 0.2% up to about 1.2% carbon, and the balance essentially aluminum.

Claim 10

Dependent Claim 13 words

A method according to claim 8, wherein the lithium level is about 2.6%.

Claim 11

Dependent Claim 70 words

A dispersion strengthened mechanically alloyed aluminum-lithium alloy consisting essentially of, by weight, from about 1.7% up to about 3.5% lithium, from about 0.4% up to about 1.5% oxygen, from about 0.2% up to about 1.2% carbon, and the balance essentially aluminum, said dispersoid being present in a small but effective amount for increased strength up to about 8 volume%, and said alloy being in the solution treated, age hardened condition.

Claim 12

Dependent Claim 70 words

A dispersion strengthened mechanically alloyed aluminum-lithium alloy consisting essentially of, by weight, from about 1.7% up to about 3.5% lithium, from about 0.4% up to about 1.5% oxygen, from about 0.2% up to about 1.2% carbon, and the balance essentially aluminum, said dispersoid being present in a small but effective amount for increased strength up to about 8 volume%, and said alloy being in the solution treated, age hardened condition.

Claim 13

Dependent Claim 23 words

A dispersion strengthened mechanically alloyed aluminum-lithium alloy according to claim 10, wherein the dispersoid level is about 3 to about 5 volume %.

Claim 14

Dependent Claim 14 words

A heat treated dispersion strengthened aluminum-lithium alloy produced by the method of claim 1.

Claim 15

Dependent Claim 82 words

A dispersion strengthened mechanically alloyed aluminum-lithium alloy consisting essentially of, by weight, from about 1.7% up to about 3.5% lithium, from about 0.4% up to about 1.5% oxygen, from about 0.2% up to about 1.2% carbon, and the balance essentially aluminum, said dispersoid being present in a small but effective amount for increased strength up to about 8 volume %, and said alloy being in the solution treated, age hardened condition and having a grain size of the order of 0.1 μm.

Claim 16

Dependent Claim 82 words

A dispersion strengthened mechanically alloyed aluminum-lithium alloy consisting essentially of, by weight, from about 1.7% up to about 3.5% lithium, from about 0.4% up to about 1.5% oxygen, from about 0.2% up to about 1.2% carbon, and the balance essentially aluminum, said dispersoid being present in a small but effective amount for increased strength up to about 8 volume %, and said alloy being in the solution treated, age hardened condition and having a grain size of the order of 0.1 μm.

Claim 17

Dependent Claim 106 words

A dispersion strengthened mechanically alloyed aluminum-lithium alloy consisting essentially of, by weight, from about 1.7% up to about 3.5% lithium, from about 0.4% up to about 1.5% oxygen, from about 0.2% up to about 1.2% carbon, and the balance essentially aluminum, with the proviso that the oxygen content is sufficient to provide enough dispersoid for the desired level of strength without being so high as to reduce the lithium content in solution below the solubility limit, said dispersoid being present in a small but effective amount for increased strength up to about 8 volume %, and said alloy being in the solution treated, age hardened condition.

Claim 18

Dependent Claim 106 words

A dispersion strengthened mechanically alloyed aluminum-lithium alloy consisting essentially of, by weight, from about 1.7% up to about 3.5% lithium, from about 0.4% up to about 1.5% oxygen, from about 0.2% up to about 1.2% carbon, and the balance essentially aluminum, with the proviso that the oxygen content is sufficient to provide enough dispersoid for the desired level of strength without being so high as to reduce the lithium content in solution below the solubility limit, said dispersoid being present in a small but effective amount for increased strength up to about 8 volume %, and said alloy being in the solution treated, age hardened condition.

Annuity Stage	Window Opens	Payment Deadline	Surcharge Period Until	Estimated Fee	Status
3.5 Years (Year 4)	1986-10-10	1987-04-11	1987-10-11	$2000.00	Window Closed / Lapsed
7.5 Years (Year 8)	1990-10-10	1991-04-11	1991-10-11	$3760.00	Window Closed / Lapsed
11.5 Years (Year 12)	1994-10-10	1995-04-11	1995-10-11	$7700.00	Window Closed / Lapsed

Method of producing Al-Li alloys with improved properties and product

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