Patent US4900565A successfully refreshed from Google Patents.
US4900565A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Water-soluble extract with bread-like flavor
Assignee: Nestec SA
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Filing: 1987-09-21
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Granted: 1990-02-13
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Expires: 2007-09-21
Abstract
Abstract An extract having a bread-like flavor is prepared by baking bread, size reducing the baked bread, mixing water with the size reduced bread for preparing a mash, treating the mash with at least one enzyme capable of liquifying bread for liquifying the bread of the mash, subjecting the aqueous liquified bread to slurry extraction, and then the aqueous slurry extracted liquified bread is subjected to steam distillation. A combined residue and extract and a distillate result from the steam distillation. The residue and extract are separated for obtaining a clarified extract which is then concentrated by evaporation. The distillate is mixed with the concentrated extract, and the mixture is dried. A water-soluble light colored powder with a bread-like flavor is obtained. To improve the yield, the separated residue also may be mixed with water and processed by slurry extraction and each of the subsequent steps of the process for obtaining further product.
Inventors
- 👤 Gerhard Spies
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 20:19
CPC Classifications
A; A23; A23L; A23L27/00; A21; A21D; A21D8/00; A21D8/02; A21D8/04; A21D8/042; A23L27/10; A23L27/11; A23L27/20; A23L27/24
Claims Analysis
Total Claims: 18
Claim 1
Independent Claim
159 words
A process for preparing a product having a bread-like flavor comprising: baking bread; size reducing the baked bread; mixing water with the size-reduced baked bread for preparing an aqueous mash; adding to the aqueous mash at least one enzyme selected from the group consisting of alpha-amylase and beta-glucanase and enzymatically treating the aqueous mash for up to 30 minutes, said at least one enzyme being present in an amount effective to liquefy the bread of the aqueous mash; subjecting the enzymatically-treated aqueous liquefied bread to slurry extraction for inactivating the enzymes and for transferring water-soluble aromatic and flavoring substances of the bread to the aqueous phase of the slurry-extracted liquefied bread; steam distilling the aqueous slurry-extracted liquefied bread to obtain a distillate and a steam-distilled extract containing undissolved solids residue; separating the steam-distilled extract from the residue; concentrating the separated steam-distilled extract by evaporation; mixing the distillate with the concentrated extract; and drying the mixture to obtain the product.
Claim 2
Dependent Claim
159 words
A process for preparing a product having a bread-like flavor comprising: baking bread; size reducing the baked bread; mixing water with the size-reduced baked bread for preparing an aqueous mash; adding to the aqueous mash at least one enzyme selected from the group consisting of alpha-amylase and beta-glucanase and enzymatically treating the aqueous mash for up to 30 minutes, said at least one enzyme being present in an amount effective to liquefy the bread of the aqueous mash; subjecting the enzymatically-treated aqueous liquefied bread to slurry extraction for inactivating the enzymes and for transferring water-soluble aromatic and flavoring substances of the bread to the aqueous phase of the slurry-extracted liquefied bread; steam distilling the aqueous slurry-extracted liquefied bread to obtain a distillate and a steam-distilled extract containing undissolved solids residue; separating the steam-distilled extract from the residue; concentrating the separated steam-distilled extract by evaporation; mixing the distillate with the concentrated extract; and drying the mixture to obtain the product.
Claim 3
Dependent Claim
22 words
A process according to claim 1 wherein the at least one enzyme is added in an amount of from 0.05% to 1%.
Claim 4
Dependent Claim
20 words
A process according to claim 1 wherein the enzyme treatment is carried out for from 10 minutes to 30 minutes.
Claim 5
Dependent Claim
50 words
A process according to claim 1 wherein the baked bread has a dry substance content of from 80% to 99%, a starch content of from 70% to 75% based upon the dry substance content and a reducing sugar content of from 3.5% to 5.5% based upon the dry substance content.
Claim 6
Dependent Claim
24 words
A process according to claim 1 wherein the ratio by weight of the size reduced baked bread to water is from 1:1 to 1:10.
Claim 7
Dependent Claim
96 words
A process according to claim 1 or 4 wherein the slurry extraction is carried out at a temperature of from 90° C. to 150° C. for from 15 minutes to 30 minutes, wherein the aqueous slurry extracted liquefied bread is steam-distilled at from about 95° C. to 98° C. in a distillation column countercurrent to steam and wherein the quantity of steam used for steam distillation is adjusted for obtaining a quantity of distillate in an amount of about 25% of the amount of dry substance of the aqueous slurry extracted liquefied bread to be distilled.
Claim 8
Dependent Claim
37 words
A process according to claim 1 wherein the extract separated from the residue is concentrated under a vacuum at a temperature of about 55° C. to 70° C. for obtaining a dry substance content of about 45%.
Claim 9
Dependent Claim
40 words
A process according to claim 1 further comprising mixing the residue with water and subjecting the mixture to the slurry extraction, steam distillation, separation, concentration and drying steps for obtaining further extract and distillate for drying for obtaining the product.
Claim 10
Dependent Claim
43 words
A process according to claim 8 further comprising subjected vapor condensated obtained from each concentration step to a reverse osmosis treatment for obtaining a condensate and mixing the condensate with the extract and distillate mixture and drying the mixture for obtaining the product.
Claim 11
Dependent Claim
45 words
A process according to claim 1 further comprising subjecting vapor condensate obtained from the concentration of the extract to a reverse osmosis treatment for obtaining a condensate and mixing the condensate with the extract and distillate mixture and drying the mixture for obtaining the product.
Claim 12
Dependent Claim
42 words
A process according to claim 10 further comprising mixing the residue with water and subjecting the mixture to the slurry extraction, steam distillation, separation, concentration and reverse osmosis steps for obtaining further extract, distillate and condensate for drying for obtaining the product.
Claim 13
Dependent Claim
126 words
A process for preparing a product having a bread-like flavor comprising: baking bread; size reducing the baked bread; mixing water with the size-reduced baked bread for preparing an aqueous mash; adding to the aqueous mash at least one enzyme selected from the group consisting of alpha-amylose and beta-glucanase and enzymatically treating the aqueous mash for up to 30 minutes, said at least one enzyme being present in an amount effective to liquefy the bread of the aqueous mash; steam distilling the enzymatically-treated aqueous liquefied bread to obtain a distillate and a steam-distilled extract containing undissolved solids residue; separating the steam-distilled extract from the residue; concentrating the separated steam-distilled extract by evaporation; mixing the distillate with the concentrated extract; and drying the mixture to obtain the product.
Claim 14
Dependent Claim
126 words
A process for preparing a product having a bread-like flavor comprising: baking bread; size reducing the baked bread; mixing water with the size-reduced baked bread for preparing an aqueous mash; adding to the aqueous mash at least one enzyme selected from the group consisting of alpha-amylose and beta-glucanase and enzymatically treating the aqueous mash for up to 30 minutes, said at least one enzyme being present in an amount effective to liquefy the bread of the aqueous mash; steam distilling the enzymatically-treated aqueous liquefied bread to obtain a distillate and a steam-distilled extract containing undissolved solids residue; separating the steam-distilled extract from the residue; concentrating the separated steam-distilled extract by evaporation; mixing the distillate with the concentrated extract; and drying the mixture to obtain the product.
Claim 15
Dependent Claim
159 words
A process for preparing a product having a bread-like flavor comprising: baking bread; size reducing the baked bread; mixing water with the size-reduced baked bread for preparing an aqueous mash; adding at least one enzyme selected from the group consisting of alpha-amylase and beta-glucanase and enzymatically treating the aqueous mash for up to 30 minutes, said at least one enzyme being present in an amount effective to liquefy the bread of the aqueous mash; subjecting the enzymatically-treated aqueous liquefied bread to slurry extraction for inactivating the enzymes and for transferring water soluble aromatic and flavoring substances of the bread to the aqueous phase of the slurry-extracted liquefied bread; separating undissolved solids from the aqueous phase of the slurry-extracted bread to obtain an extract; steam distilling the separated extract for obtaining a distillate and a remaining steam-distilled extract; concentrating the remaining steam-distilled extract by evaporation; mixing the distillate with the concentrated extract; and drying the mixture to obtain the product.
Claim 16
Dependent Claim
159 words
A process for preparing a product having a bread-like flavor comprising: baking bread; size reducing the baked bread; mixing water with the size-reduced baked bread for preparing an aqueous mash; adding at least one enzyme selected from the group consisting of alpha-amylase and beta-glucanase and enzymatically treating the aqueous mash for up to 30 minutes, said at least one enzyme being present in an amount effective to liquefy the bread of the aqueous mash; subjecting the enzymatically-treated aqueous liquefied bread to slurry extraction for inactivating the enzymes and for transferring water soluble aromatic and flavoring substances of the bread to the aqueous phase of the slurry-extracted liquefied bread; separating undissolved solids from the aqueous phase of the slurry-extracted bread to obtain an extract; steam distilling the separated extract for obtaining a distillate and a remaining steam-distilled extract; concentrating the remaining steam-distilled extract by evaporation; mixing the distillate with the concentrated extract; and drying the mixture to obtain the product.
Claim 17
Dependent Claim
152 words
A process for preparing a product having a bread-like flavor comprising: mixing water with size-reduced baked bread for preparing an aqueous mash; adding to the aqueous mash at least one enzyme selected from the group consisting of alpha-amylase and beta-glucanase and enzymatically treating the aqueous mash for up to 30 minutes, said at least one enzyme being present in an amount effective to liquefy the bread of the aqueous mash; subjecting the enzymatically-treated aqueous liquefied bread to slurry extraction for inactivating the enzymes and for transferring water-soluble aromatic and flavoring substances of the bread to the aqueous phase of the slurry-extracted liquefied bread; steam distilling the aqueous slurry-extracted liquefied bread to obtain a distillate and a steam distilled extract containing undissolved solids residue; separating the steam-distilled extract from the residue; concentrating the separated steam-distilled extract by evaporation; mixing the distillate with the concentrated extract; and drying the mixture to obtain the product.
Claim 18
Dependent Claim
152 words
A process for preparing a product having a bread-like flavor comprising: mixing water with size-reduced baked bread for preparing an aqueous mash; adding to the aqueous mash at least one enzyme selected from the group consisting of alpha-amylase and beta-glucanase and enzymatically treating the aqueous mash for up to 30 minutes, said at least one enzyme being present in an amount effective to liquefy the bread of the aqueous mash; subjecting the enzymatically-treated aqueous liquefied bread to slurry extraction for inactivating the enzymes and for transferring water-soluble aromatic and flavoring substances of the bread to the aqueous phase of the slurry-extracted liquefied bread; steam distilling the aqueous slurry-extracted liquefied bread to obtain a distillate and a steam distilled extract containing undissolved solids residue; separating the steam-distilled extract from the residue; concentrating the separated steam-distilled extract by evaporation; mixing the distillate with the concentrated extract; and drying the mixture to obtain the product.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1993-02-12 | 1993-08-14 | 1994-02-13 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1997-02-12 | 1997-08-14 | 1998-02-13 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2001-02-12 | 2001-08-14 | 2002-02-13 | $7700.00 | Window Closed / Lapsed |