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US4898755A
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Inorganic-organic composite compositions exhibiting nonlinear optical response
Assignee: Corning Inc
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Filing: 1988-10-24
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Granted: 1990-02-06
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Expires: 2008-10-24
Abstract
Abstract This invention provides an optical medium which consists of an inorganic glass monolith with a microporous structure containing an organic component which exhibits nonlinear optical response. In one embodiment this invention provides a sol-gel process for producing a composite of a transparent homogeneous microporous inorganic oxide glass monolith and an organic compound which exhibits nonlinear optical response.
Inventors
- 👤 Tessie M. Che
- 👤 Dagobert E. Stuetz
- 👤 Alan Buckley
- 👤 Donald R. Ulrich
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-06 15:32
CPC Classifications
C; C03; C03C; C03C1/00; C03C1/006; C03C14/00; C03C14/008; C03C23/00; C03C23/0095; G; G02; G02F; G02F1/00; G02F1/35; G02F1/355; G02F1/3555; G02F1/361; C03C2214/00; C03C2214/17; C03C2214/32; C09; C09K; C09K2323/00; C09K2323/05; C09K2323/051
Claims Analysis
Total Claims: 8
Claim 1
Independent Claim
80 words
A process for producing a composite composition comprising a homogeneous inorganic oxide glass monolith with a microporous structure containing an organic component which exhibits nonlinear optical response, which comprises hydrolyzing tetraalkoxysilane under acidic or basic pH conditions in a sol-gel reaction medium comprising water, a water-miscible organic solvent and an organic component which exhibits nonlinear optical response, until gellation of the reaction medium is completed, and removing the solvent medium to provide a porous glass monolith with incorporated organic component.
Claim 2
Dependent Claim
80 words
A process for producing a composite composition comprising a homogeneous inorganic oxide glass monolith with a microporous structure containing an organic component which exhibits nonlinear optical response, which comprises hydrolyzing tetraalkoxysilane under acidic or basic pH conditions in a sol-gel reaction medium comprising water, a water-miscible organic solvent and an organic component which exhibits nonlinear optical response, until gellation of the reaction medium is completed, and removing the solvent medium to provide a porous glass monolith with incorporated organic component.
Claim 3
Dependent Claim
27 words
A process in accordance with claim 1 wherein substantially all of the pores in the microporous structure have diameters within about a 100 angstrom diameter variation range.
Claim 4
Dependent Claim
13 words
A composite composition produced in accordance with the sol-gel process of claim 1.
Claim 5
Dependent Claim
85 words
A process for producing a composite composition comprising an inorganic oxide glass monolith with a microporous structure containing an organic component which exhibits nonlinear optical response, which comprises (1) hydrolyzing tetraalkoxysilane under acidic or basic pH conditions in a sol-gel reaction medium comprising water and a water-miscible organic solvent component until gellation of the reaction medium is completed; (2) removing the solvent medium to provide a porous glass monolith; and (3) impregnating the porous glass monolith with an organic component which exhibits nonlinear optical response.
Claim 6
Dependent Claim
85 words
A process for producing a composite composition comprising an inorganic oxide glass monolith with a microporous structure containing an organic component which exhibits nonlinear optical response, which comprises (1) hydrolyzing tetraalkoxysilane under acidic or basic pH conditions in a sol-gel reaction medium comprising water and a water-miscible organic solvent component until gellation of the reaction medium is completed; (2) removing the solvent medium to provide a porous glass monolith; and (3) impregnating the porous glass monolith with an organic component which exhibits nonlinear optical response.
Claim 7
Dependent Claim
27 words
A process in accordance with claim 4 wherein substantially all of the pores in the microporous structure have diameters within about a 100 angstrom diameter variation range.
Claim 8
Dependent Claim
12 words
A composite composition produced in accordance with the process of claim 4.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
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| 3.5 Years (Year 4) | 1993-02-05 | 1993-08-07 | 1994-02-06 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1997-02-05 | 1997-08-07 | 1998-02-06 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2001-02-05 | 2001-08-07 | 2002-02-06 | $7700.00 | Window Closed / Lapsed |