← Back to Patent Explorer
US4877814A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for producing open-cell polyethylene foam materials and the resultant product

Assignee: SERUTEKUNO A CORP OF JAPAN KK
•
Filing: 1986-09-05
•
Granted: 1989-10-31
•
Expires: 2006-09-05
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract This disclosure relates to a method for producing polyethylene open-cell foam materials, comprising a process step of pressurized heating at a temperature of 110° to 135° C. of a base compound consisting of polyethylene or a copolymer of polyethylene which has been compounded with an azodicarbonamide foaming agent and a bridging agent, in order to obtain a primary intermediate product with a cubical expansion coefficient of 1.0 to 2.0 times; a process step of heating the primary intermediate product under normal atmospheric pressure at a temperature of 150°˜190° C. and thus causing the complete decomposition of the foaming agent in order to obtain a secondary intermediate product having cell membranes capable of being easily ruptured by mechanical compression; and a process step of subjecting said secondary intermediate product to mechanical pressure in order to rupture and interconnect the closed cells; and, as needed, a foaming assist agent, or a high-melting-point resin powder, or both a high-melting-point resin powder and a foaming assist agent are added to and compounded with the base compound so that the resulting products are high-expansive or ultra-high-expansive materials with an expansion ratio of 25 times said base compound, or more, and have an open-cell ratio nof 96˜100%.

Inventors

  • 👤 Hiroo Ito

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-03 18:11
CPC Classifications
C; C08; C08J; C08J9/00; C08J9/36; C08J9/38; C08J9/0061; C08J9/04; C08J9/06; C08J9/10; C08J9/102; C08J9/103; C08J2323/00; C08J2323/02; C08J2323/04; Y; Y10; Y10S; Y10S264/00; Y10S264/05; Y10S264/16; Y10S264/18

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 213 words
A method for producing polyethylene open-cell foam materials whose characteristic feature is that it comprises: (i) a first process step of compacting a base compound into a tightly closed mold in a press at a pressure of about 3kg/cm 2 to about 10 kg/cm 2 which is heated at a temperature of approximately 110° to 135° C., said base compound comprising polyethylene or copolymer of polyethylene which has been compounded with an azodicarbonamide foaming agent and a cross-linking agent in order to obtain a primary intermediary product wherein said foaming agent and said cross-linking agent have a decomposition ratio of from about zero to about 4% to provide a cubical expansion coefficient of 1.0 to 2.0 times. (ii) a second process step of heating said primary intermediary product under normal pressure at a temperature of 150 ° to 190° C., thus causing the complete decomposition of said foaming agent and said cross-linking agent in order to obtain a secondary intermediate product having uniform cell membrane capable of being easily ruptured by mechanical compression; and (iii) a third process step of mechanically compressing said secondary intermediate product to rapture said cell membranes and thereby interconnect said cells and thus obtain open-cell foam products, said open-cell foam products having expansion ratios greater than about 25.
Claim 2
Independent Claim 213 words
A method for producing polyethylene open-cell foam materials whose characteristic feature is that it comprises: (i) a first process step of compacting a base compound into a tightly closed mold in a press at a pressure of about 3kg/cm 2 to about 10 kg/cm 2 which is heated at a temperature of approximately 110° to 135° C., said base compound comprising polyethylene or copolymer of polyethylene which has been compounded with an azodicarbonamide foaming agent and a cross-linking agent in order to obtain a primary intermediary product wherein said foaming agent and said cross-linking agent have a decomposition ratio of from about zero to about 4% to provide a cubical expansion coefficient of 1.0 to 2.0 times. (ii) a second process step of heating said primary intermediary product under normal pressure at a temperature of 150 ° to 190° C., thus causing the complete decomposition of said foaming agent and said cross-linking agent in order to obtain a secondary intermediate product having uniform cell membrane capable of being easily ruptured by mechanical compression; and (iii) a third process step of mechanically compressing said secondary intermediate product to rapture said cell membranes and thereby interconnect said cells and thus obtain open-cell foam products, said open-cell foam products having expansion ratios greater than about 25.
Claim 3
Dependent Claim 18 words
A method descried in claim 1 in which a foaming assist agent is added to said base compound.
Claim 4
Dependent Claim 40 words
A method described in claim 1 in which 5 to 30 parts by weight of a high-melting-point resin powder with a melting point of at least 140° C. is added to said base compound of polyethylene or copolymer of polyethylene.
Claim 5
Dependent Claim 18 words
A method described in claim 2 in which a foaming assist agent is added to said base compound.
Claim 6
Dependent Claim 17 words
The method described in claim 3 in which an inorganic filler is added to said base compound.
Claim 7
Dependent Claim 17 words
The method described in claim 4 in which an inorganic filler is added to said base compound.
Claim 8
Dependent Claim 14 words
A polyethylene open-cell foam material produced by the method set forth in claim 1.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1992-10-30 1993-05-01 1993-10-31 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1996-10-30 1997-05-01 1997-10-31 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2000-10-30 2001-05-01 2001-10-31 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag