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Process for the production of benzenesulfonamides

Assignee: HILTON-DAVIS COMPANY A CORP OF DE
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Filing: 1987-04-29
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Granted: 1989-10-17
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Expires: 2007-04-29
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Abstract

Abstract Process comprises the combination of two steps of interacting a R-benzene, sulfuric acid and phosphorus oxychloride to obtain 4-R-benzenesulfonyl chloride and amidating said sulfonyl chloride to produce 4-R-benzenesulfonamide.

Inventors

  • 👤 Ramamurthi Kannan

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-07 22:14
CPC Classifications
C; C07; C07C; C07C303/00; C07C303/36; C07C303/38; C09; C09D; C09D11/00; C09D11/30; C09D11/34

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 76 words
A process for the production of a 4-R-benzenesulfonamide of the formula ##STR4## wherein R represents a non-tertiary C 1 to C 16 alkyl or a non-tertiary C 1 to C 16 alkoxy, which consists of in the first step reacting a R-benzene with sulfuric acid and phosphorus oxychloride to produce a 4-R-benzenesulfonyl chloride of the formula ##STR5## and in a second step amidating said 4-R-benzenesulfonyl chloride with ammonia in an aqueous medium to obtain said 4-R-benzenesulfonamide.
Claim 2
Dependent Claim 76 words
A process for the production of a 4-R-benzenesulfonamide of the formula ##STR4## wherein R represents a non-tertiary C 1 to C 16 alkyl or a non-tertiary C 1 to C 16 alkoxy, which consists of in the first step reacting a R-benzene with sulfuric acid and phosphorus oxychloride to produce a 4-R-benzenesulfonyl chloride of the formula ##STR5## and in a second step amidating said 4-R-benzenesulfonyl chloride with ammonia in an aqueous medium to obtain said 4-R-benzenesulfonamide.
Claim 3
Dependent Claim 21 words
A process according to claim 1 for preparing a 4-R-benzenesulfonamide wherein R represents a non-tertiary C 1 to C 16 alkoxy.
Claim 4
Dependent Claim 9 words
A process according to claim 2 for preparing 4-methoxybenzenesulfonamide.
Claim 5
Dependent Claim 21 words
A process according to claim 1 for preparing a 4-R-benzensulfonamide wherein R represents a non-tertiary C 1 to C 16 alkyl.
Claim 6
Dependent Claim 9 words
A process according to claim 4 for preparing 4-ethylbenzenesulfonamide.
Claim 7
Dependent Claim 9 words
A process according to claim 4 for preparing 4-butylbenzenesulfonamide.
Claim 8
Dependent Claim 9 words
A process according to claim 4 for preparing 4-nonylbenzenesulfonamide.

References Cited (Backward Citations)

No citation records indexed.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1992-10-16 1993-04-17 1993-10-17 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1996-10-16 1997-04-17 1997-10-17 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2000-10-16 2001-04-17 2001-10-17 $7700.00 Window Closed / Lapsed

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