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US4856335A
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Method of establishing standard composite material properties
Assignee: Expert System Technologies Inc
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Filing: 1987-10-21
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Granted: 1989-08-15
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Expires: 2007-10-21
Abstract
Abstract A standard reference deformation of a composite material containing a flowable phase and compressible inclusions, such as a prepreg, is measured as the deformation whereat the dominant compressive mode of composite deformation changes from that characteristic of compressible inclusion collapse to that characteristic of resin flow, termed the optimal consolidation deformation. Establishment of this point permits measurement and correlation of physically significant composite properties. For example, material properties of such composite materials are measured under a compressive loading by an ultrasonic transducer at the optimal consolidation deformation. At this point, normally determined to be the deformation at which the second derivative of compressive displacement falls to about zero, compressible inclusions such as voids are eliminated but the flowable phase has not yet begun to flow significantly so as to change the fractions of the phases. This technique is particularly valuable in ultrasonically measuring properties such as phase fractions of resin matrix prepreg materials wherein the resin has not been cured and readily flows, and wherein there are typically voids that interfere with the measurement of properties.
Inventors
- 👤 Neal E. Tornberg
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 16:02
CPC Classifications
G; G01; G01N; G01N29/00; G01N29/22; G01N29/227; G01N29/04; G01N29/07; G01N2291/00; G01N2291/02; G01N2291/023; G01N2291/0231; G01N2291/025; G01N2291/0251; G01N2291/04; G01N2291/048
Claims Analysis
Total Claims: 22
Claim 1
Independent Claim
83 words
A process for measuring a standard reference deformation for a composite material, comprising the steps of: furnishing a specimen of a multiphase material wherein at least one phase is flowable, and which initially contains compressible inclusions within the specimen; compressing the specimen; and determining the deformation at which the dominant compressive displacement behavior of the composite material changes from that characteristic of collapse of the compressible inclusions to that characteristic of flow of the flowable phase, this deformation being the standard reference deformation.
Claim 2
Dependent Claim
83 words
A process for measuring a standard reference deformation for a composite material, comprising the steps of: furnishing a specimen of a multiphase material wherein at least one phase is flowable, and which initially contains compressible inclusions within the specimen; compressing the specimen; and determining the deformation at which the dominant compressive displacement behavior of the composite material changes from that characteristic of collapse of the compressible inclusions to that characteristic of flow of the flowable phase, this deformation being the standard reference deformation.
Claim 3
Dependent Claim
17 words
The process of claim 1, including the further step of collecting data at the standard reference deformation.
Claim 4
Dependent Claim
11 words
The process of claim 1, wherein said compressible inclusions are voids.
Claim 5
Dependent Claim
112 words
A process for measuring a standard property of the phases of a multiphase material, comprising the steps of: furnishing a specimen of a multiphase material wherein at least one phase is flowable, and which initially contains compressible inclusions within the specimen; applying a compressive force to the specimen so that its deformation increases with increasing time; and measuring a property of the specimen at a standard specimen deformation at which the dominant compressive displacement behavior of the material changes from that characteristic of compressible inclusion collapse to that characteristic of flow of the flowable phase, the property measured at this point being the standard value of the property for the multiphase material.
Claim 6
Dependent Claim
112 words
A process for measuring a standard property of the phases of a multiphase material, comprising the steps of: furnishing a specimen of a multiphase material wherein at least one phase is flowable, and which initially contains compressible inclusions within the specimen; applying a compressive force to the specimen so that its deformation increases with increasing time; and measuring a property of the specimen at a standard specimen deformation at which the dominant compressive displacement behavior of the material changes from that characteristic of compressible inclusion collapse to that characteristic of flow of the flowable phase, the property measured at this point being the standard value of the property for the multiphase material.
Claim 7
Dependent Claim
28 words
The process of claim 4, wherein the standard specimen deformation is the deformation at which the second derivative of compressive displacement with time first falls to about zero.
Claim 8
Dependent Claim
32 words
The process of claim 4, wherein said steps of applying and measuring are performed by a single measurement means for measuring the property, which is forced against the surface of the specimen.
Claim 9
Dependent Claim
66 words
The process of claim 4, wherein said step of measuring is accomplished by performing a series of simultaneous measurements of the material displacement and the property being measured, and selecting from the series of data the property measured at the point whereat the dominant compressive behavior of the specimen changes from that characteristic of compressible inclusion collapse to that characteristic of flow of the flowable phase.
Claim 10
Dependent Claim
11 words
The process of claim 4, wherein the compressible inclusions are voids.
Claim 11
Dependent Claim
13 words
The process of claim 4, wherein the multiphase material is a composite prepreg.
Claim 12
Dependent Claim
26 words
The process of claim 4, wherein a property measured in said step of measuring is the time required for an ultrasonic wave to traverse the specimen.
Claim 13
Dependent Claim
117 words
A process for determining a standard property of a composite material, comprising the steps of: furnishing a specimen of a multiphase material wherein at least one phase is flowable, and which initially contains compressible inclusions within the specimen; contacting at least one surface of the specimen with an ultrasonic transducer under a compressive pressure so as to compress the composite material; and measuring the ultrasonic property of the specimen at the deformation at which the dominant compressive displacement behavior of the composite material changes from that characteristic of compressible inclusion collapse to that characteristic of flow of the flowable phase, the property measured at this point being the standard value of the property for the composite material.
Claim 14
Dependent Claim
117 words
A process for determining a standard property of a composite material, comprising the steps of: furnishing a specimen of a multiphase material wherein at least one phase is flowable, and which initially contains compressible inclusions within the specimen; contacting at least one surface of the specimen with an ultrasonic transducer under a compressive pressure so as to compress the composite material; and measuring the ultrasonic property of the specimen at the deformation at which the dominant compressive displacement behavior of the composite material changes from that characteristic of compressible inclusion collapse to that characteristic of flow of the flowable phase, the property measured at this point being the standard value of the property for the composite material.
Claim 15
Dependent Claim
13 words
The process of claim 11, wherein the property measured is the ultrasonic slowness.
Claim 16
Dependent Claim
15 words
The process of claim 11, wherein the property is measured by the transit time technique.
Claim 17
Dependent Claim
15 words
The process of claim 11, wherein the property is measured by the sing around technique.
Claim 18
Dependent Claim
15 words
The process of claim 11, wherein the pressure applied varies during said step of measuring.
Claim 19
Dependent Claim
40 words
The process of claim 11, including the further step of: comparing the standard value of the property for the specimen with standard values determined for other specimens whose phase fractions are known, to ascertain the phase fraction of the specimen.
Claim 20
Dependent Claim
121 words
A process for measuring the fractions of the phases of a composite material, comprising: furnishing a specimen of a composite material having a reinforcement phase embedded within a flowable matrix phase, and further having voids therein; contacting at least one surface of the specimen with an ultrasonic transducer under a downward compressive pressure; determining the displacement of the transducer with time; measuring the velocity of ultrasonic wave propagation of the specimen as the dominant compressive displacement behavior of the specimen changes from that characteristic of void collapse to that characteristic of flow of the flowable phase; and calculating the fractions of the phases present in the composite material from the velocity of ultrasonic wave propagation measured in said step of measuring.
Claim 21
Dependent Claim
121 words
A process for measuring the fractions of the phases of a composite material, comprising: furnishing a specimen of a composite material having a reinforcement phase embedded within a flowable matrix phase, and further having voids therein; contacting at least one surface of the specimen with an ultrasonic transducer under a downward compressive pressure; determining the displacement of the transducer with time; measuring the velocity of ultrasonic wave propagation of the specimen as the dominant compressive displacement behavior of the specimen changes from that characteristic of void collapse to that characteristic of flow of the flowable phase; and calculating the fractions of the phases present in the composite material from the velocity of ultrasonic wave propagation measured in said step of measuring.
Claim 22
Dependent Claim
28 words
The process of claim 17, wherein the specimen deformation is measured as the deformation at which the second derivative of compressive displacement with time falls to about zero.
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| 3.5 Years (Year 4) | 1992-08-14 | 1993-02-13 | 1993-08-15 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1996-08-14 | 1997-02-13 | 1997-08-15 | $3760.00 | Window Closed / Lapsed |
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