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US4826538A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for removing an insulating fluid (PCB) from an electrical insulating part

Assignee: BBC BROWN
•
Filing: 1987-11-30
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Granted: 1989-05-02
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Expires: 2007-11-30
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Abstract

Abstract A method for removing an insulating fluid containing polychlorinated biphenyl (PCB) which was used as an insulating medium, from the pores of a porous solid electrical insulating part which had been immersed in PCB-containing insulating fluid of an electrical apparatus from the group consisting of electrical transformers, chokes and capacitors includes the steps of removing the insulating part from the electrical apparatus and subsequently immersing the insulating part in a bath containing at least one fluid solvent for PCB selected from the group consisting of aliphatic, aromatic, chlorinated and fluorinated hydrocarbons. The insulating part is moved within the bath for a period of from 8-60 minutes at a speed of from 0.02 to 0.5 meters per second, and the solvent of the bath is heated during the movement of the insulating part from the ambient temperature to a final temperature of from 5° to 25° C. below the boiling temperature of the solvent at the pressure prevailing in the bath. The solvent is subjected to ultrasonic waves having a frequency of from 15 to 40 kHz.

Inventors

  • 👤 Gerhard Sanders
  • 👤 Erwin Wessling

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 06:41
CPC Classifications
B; B08; B08B; B08B3/00; B08B3/04; B08B3/10; B08B3/12; C; C10; C10G; C10G21/00; C10G21/006

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 341 words
The method for removing an insulating fluid containing polychlorinated biphenyl (PCB), which had been used as an insulating dielectric medium, from the pores of a porous solid electrical insulating part which had been immersed in the PCB-containing insulating fluid of an electrical apparatus from the group consisting of electrical transformers, chokes and capacitors, which comprises the steps of: (a) removing the insulating part from the electrical apparatus; (b) immersing the insulating part in a bath containing at least one fluid solvant for PCB selected from the group consisting of aliphatic, aromatic, chlorinated and fluorinated hydrocarbons; (c) moving the insulating part within the bath for a period of from 8 to 60 minutes at a speed of from 0.02 to 0.5 meters per second; (d) heating the solvent of the bath during said part immersion period from the ambient temperature to a final temperature of from 5° to 25° C. below the boilding temperature of the solvent at the pressure prevailing in the bath; (e) subjecting the solvent bath and the immersed insulating part to ultrasonic waves having a frequency of from 15 to 40 KKz. (f) measuring and monitoring the PCB-content of the solvent in the solvent bath and exchanging the solvent when a predetermined threshold value of PCB is exceeded; (g) said heating step comprising three operating stages-- (i) a first operating stage wherein said solvent bath is maintained at ambient temperature until the initial PCB threshold value of 5000 ppm of PCB is reached and "such" solvent is excanged for PCB-free solvent; (ii) a second operating stage wherein the solvent bath is heated to a temperature about midway between the ambient temperature and said final temperature and maintained thereat until a second PCB threshold value of 500 Ppm of PCB is reached and such solvent is exchanged for PCB-free solvent; and (iii) a third operating stage wherein the solvent bath is heated to said final temperature and maintained thereat until the predetermined threshold value of 30 ppm PCB is reached and then such solvent is exchanged for PCB-free solvent.
Claim 2
Independent Claim 341 words
The method for removing an insulating fluid containing polychlorinated biphenyl (PCB), which had been used as an insulating dielectric medium, from the pores of a porous solid electrical insulating part which had been immersed in the PCB-containing insulating fluid of an electrical apparatus from the group consisting of electrical transformers, chokes and capacitors, which comprises the steps of: (a) removing the insulating part from the electrical apparatus; (b) immersing the insulating part in a bath containing at least one fluid solvant for PCB selected from the group consisting of aliphatic, aromatic, chlorinated and fluorinated hydrocarbons; (c) moving the insulating part within the bath for a period of from 8 to 60 minutes at a speed of from 0.02 to 0.5 meters per second; (d) heating the solvent of the bath during said part immersion period from the ambient temperature to a final temperature of from 5° to 25° C. below the boilding temperature of the solvent at the pressure prevailing in the bath; (e) subjecting the solvent bath and the immersed insulating part to ultrasonic waves having a frequency of from 15 to 40 KKz. (f) measuring and monitoring the PCB-content of the solvent in the solvent bath and exchanging the solvent when a predetermined threshold value of PCB is exceeded; (g) said heating step comprising three operating stages-- (i) a first operating stage wherein said solvent bath is maintained at ambient temperature until the initial PCB threshold value of 5000 ppm of PCB is reached and "such" solvent is excanged for PCB-free solvent; (ii) a second operating stage wherein the solvent bath is heated to a temperature about midway between the ambient temperature and said final temperature and maintained thereat until a second PCB threshold value of 500 Ppm of PCB is reached and such solvent is exchanged for PCB-free solvent; and (iii) a third operating stage wherein the solvent bath is heated to said final temperature and maintained thereat until the predetermined threshold value of 30 ppm PCB is reached and then such solvent is exchanged for PCB-free solvent.
Claim 3
Dependent Claim 104 words
Method according to claim 1, which comprises carrying out the step of moving the insulating part within the bath for a period of from 10-30 minutes at a speed of from 0.05 to 0.15 meters per second, carrying out the step of heating the solvent of the bath during the movement of the insulating part from the ambient temperature to a final temperature of from 10° to 20° C. below the boiling temperature of the solvent at the pressure prevailing in the bath, and carrying out the step of subjecting the solvent to ultrasonic waves having a frequency of from 20 to 30 kHz.
Claim 4
Dependent Claim 56 words
Method according to claim 1, which comprises using approximately 10 to 30% of the duration of the heating during the first operating stage, using approximately 20 to 35% of the duration of the heating during the second operating stage, and using approximately 70 to 35% of the duration of the heating during the third operating stage.
Claim 5
Dependent Claim 20 words
Method according to claim 1, which comprises carrying out the step of detecting the PCB content of the solvent continuously.
Claim 6
Dependent Claim 77 words
The method according to claim 1 which comprises circulating the solvent through the bath and at least one heat exchanger, introducing the circulating solvent into the bath below the fluid level as a fluid stream through at least one nozzle, and directing the fluid stream at the insulating part, wherein said directing nozzles are located on the side walls and/or bottom of the bath and at least one of said nozzles are disposed between the ultrasonic transducers.
Claim 7
Dependent Claim 24 words
Method according to claim 5, which comprises introducing the solvent into the bath at a speed of from 0.2 to 1 meter per second.
Claim 8
Dependent Claim 24 words
Method according to claim 5, which comprises introducing the solvent into the bath at a speed of from 0.2 to 0.4 meters per second.
Claim 9
Dependent Claim 25 words
The method according to claim 1 wherein the insulating part immersed in said solvent bath is moved therethrough in a combined reciprocating and rotational movement.
Claim 10
Dependent Claim 26 words
Method according to claim 1, which comprises introducing the insulating part into the bath along with the electrical component that is provided with the insulating part.
Claim 11
Dependent Claim 52 words
Method according to claim 1, which comprises selecting the solvent, in the liquid state, from the group consisting of n-hexane CH 3 --(CH 2 ) 4 --CH 3 ; xylene C 6 H 4 (CH 3 ) 2 ; tetrachloroethylene Cl 2 C═CCl 2 ; and trichlorotrifluoroethane Cl 2 FC--CClF 2 .

References Cited (Backward Citations)

US2860646A Cited
DE1091076B Cited
US3001532A Cited
SU517200A1 Cited
US4055507A Cited
SU584912A1 Cited
SU608572A1 Cited
SU912311A1 Cited
US4425949A Cited
GB2104104A Cited
US4483717A Cited
US4685972A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1992-05-01 1992-10-31 1993-05-02 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1996-05-01 1996-10-31 1997-05-02 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2000-05-01 2000-10-31 2001-05-02 $7700.00 Window Closed / Lapsed

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