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US4425949A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for removing undesirable substances from electrical devices

Assignee: Diamond Shamrock Chemicals Co
•
Filing: 1982-02-01
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Granted: 1984-01-17
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Expires: 2002-02-01
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Abstract

Abstract The removal of undesirable substances such as water, PCB's and air from the internal components of electrical devices such as transformers and power capacitors is efficiently and effectively achieved by contacting, in the absence of air, the internal components of these various electrical devices with a heat-stable fluid material. The heat-stable fluid materials are preferably halogenated aliphatic hydrocarbons and most preferably perchloroethylene or FREON 113.

Inventors

  • 👤 Edward A. Rowe, Jr.

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-26 07:26
CPC Classifications
C; C10; C10G; C10G21/00; C10G21/006; H; H01; H01F; H01F27/00; H01F27/08; H01F27/10; H01F27/12; H01F27/14

Claims Analysis

Total Claims: 13
Claim 1
Independent Claim 92 words
A method for retrofilling a transformer which contains polychlorinated biphenyls and other undesirable substances comprising: (A) evacuating said transformer to about one millimeter Hg; (B) introducing a halogenated aliphatic hydrocarbon vapor into said transformer removing that vapor which is not adsorbed or condensed by the transformer, such that PCBs are removed along with said vapor until the outlet vapor temperature equals the inlet vapor temperature; (C) discontinuing introduction of said halogenated aliphatic hydrocarbon; (D) evacuating said transformer to about 20 millimeters Hg; and (E) filling said evacuated transformer with a dielectric material.
Claim 2
Independent Claim 92 words
A method for retrofilling a transformer which contains polychlorinated biphenyls and other undesirable substances comprising: (A) evacuating said transformer to about one millimeter Hg; (B) introducing a halogenated aliphatic hydrocarbon vapor into said transformer removing that vapor which is not adsorbed or condensed by the transformer, such that PCBs are removed along with said vapor until the outlet vapor temperature equals the inlet vapor temperature; (C) discontinuing introduction of said halogenated aliphatic hydrocarbon; (D) evacuating said transformer to about 20 millimeters Hg; and (E) filling said evacuated transformer with a dielectric material.
Claim 3
Dependent Claim 65 words
The method according to claim 1 wherein a transformer core is contacted with a halogenated aliphatic hydrocarbon vapor under reduced pressure and said contacting is continued until said transformer is saturated with said aliphatic hydrocarbon vapor at which point said contacting is discontinued and the halogenated aliphatic hydrocarbon vapor containing water and air and other undesirable substances is removed from said transformer under reduced pressure.
Claim 4
Dependent Claim 16 words
The method according to claim 1 wherein said halogenated aliphatic hydrocarbon is a chlorinated aliphatic hydrocarbon.
Claim 5
Dependent Claim 13 words
The method according to claim 3 wherein said chlorinated aliphatic hydrocarbon is perchloroethylene.
Claim 6
Dependent Claim 12 words
The method according to claim 1 wherein said dielectric material is perchloroethylene.
Claim 7
Dependent Claim 13 words
The method according to claim 1 wherein said halogenated aliphatic hydrocarbon is 1,1,2-trichloro-1,2,2-trifluoroethane.
Claim 8
Dependent Claim 17 words
The method according to claim 1 wherein steps (A)-(C) are repeated for at least one additional cycle.
Claim 9
Dependent Claim 35 words
The method according to claim 1 wherein water, air and other undesirable substances are separated from the halogenated aliphatic hydrocarbon vapor removed from said transformer and the separated halogenated aliphatic hydrocarbon is recycled for reuse.
Claim 10
Dependent Claim 26 words
The method according to claim 1 wherein the halogenated aliphatic hydrocarbon vapor contacting procedure is followed by at least one hot halogenated aliphatic hydrocarbon liquid flush.
Claim 11
Dependent Claim 23 words
The method according to claim 1 wherein the polychlorinated biphenyls concentration level within the transformer core is reduced to less than 50 ppm.
Claim 12
Dependent Claim 23 words
The method according to claim 1 wherein the polychlorinated biphenyls concentration level within the transformer core is reduced to less than 10 ppm.
Claim 13
Dependent Claim 28 words
A transformer core of a retrofilled transformer wherein the concentration level of polychlorinated biphenyls has been reduced to less than 50 ppm by the process of claim 1.

References Cited (Backward Citations)

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US1866346A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1987-01-16 1987-07-18 1988-01-17 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1991-01-16 1991-07-18 1992-01-17 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1995-01-16 1995-07-18 1996-01-17 $7700.00 Window Closed / Lapsed

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