Patent US4818295A successfully refreshed from Google Patents.
US4818295A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Cyclone reactor
Assignee: United States Department of Energy
•
Filing: 1986-04-04
•
Granted: 1989-04-04
•
Expires: 2006-04-04
Abstract
Abstract A system is provided to produce sugars from a liquid-solid mixture containing biomass, and an acid, wherein the mixture is heated to an appropriate temperature to achieve hydrolysis. The liquid-solid mixture is introduced as a stream into the circular-cylindrical chamber of a cyclone reaction vessel and steam is introduced to the vessel to provide the necessary heat for hydrolysis as well as to establish the liquid-solid mixture in a rotary flow field whereby the liquids and solids of the mixture move along spiral paths within the chamber. The liquid-solid mixture may be introduced at the periphery of the chamber to spiral down toward and be discharged at or near the center of the chamber. Because of differing mass, the solid particles in the mixture move radially inward at a different rate than the liquid and that rate is controlled to maximize the hydrolysis of the solids and to minimize the decomposition of sugars, thus formed.
Inventors
- 👤 Alvin O. Converse
- 👤 Hans E. Grethlein
- 👤 Joseph E. Holland
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 21:22
CPC Classifications
B; B01; B01J; B01J19/00; B01J19/24; B01J19/2405; B01J2219/00; B01J2219/00049; B01J2219/00051; B01J2219/00074; B01J2219/00105; B01J2219/00114; B01J2219/00162; B01J2219/00164; B01J2219/00166
Claims Analysis
Total Claims: 5
Claim 1
Independent Claim
235 words
A cocurrent-flow reactor system for the hydrolysis of cellulosic or lignocellulosic material to sugar comprising: a hollow cylindrical reactor vessel having an internal reaction chamber defined by a peripheral annular wall and end walls having inwardly extending central cores to define a central portion of said chamber of less height than that at said peripheral wall; first and second tangential entries coupled into said reaction chamber at the peripheral, annular wall thereof; a source of slurry connected to said first tangential entry for introducing slurry as a cyclonic flow into said reaction chamber, said slurry including cellulosic or lignocellulosic solids and aqueous solution for hydrolysis of said solids to sugar, said solids being of greater density than said solution; a steam boiler connected to said second tangential entry for introducing steam in support of said cyclonic flow and to provide heat for hydrolysis within said reaction chamber, said cylonic flow biasing slurry solids towards the outer periphery and slurry solution towards the central portion of said reaction chamber; slurry discharge means disposed at the central portion of said reaction chamber for withdrawing slurry with solution of enriched sugar content, said slurry solids being retained longer than said solution within said reaction chamber due to the biasing of solids towards said peripheral wall by said cyclonic flow; and a let-down orifice coupled to said discharge means for reducing the slurry temperature and stopping the hydrolysis process.
Claim 2
Dependent Claim
235 words
A cocurrent-flow reactor system for the hydrolysis of cellulosic or lignocellulosic material to sugar comprising: a hollow cylindrical reactor vessel having an internal reaction chamber defined by a peripheral annular wall and end walls having inwardly extending central cores to define a central portion of said chamber of less height than that at said peripheral wall; first and second tangential entries coupled into said reaction chamber at the peripheral, annular wall thereof; a source of slurry connected to said first tangential entry for introducing slurry as a cyclonic flow into said reaction chamber, said slurry including cellulosic or lignocellulosic solids and aqueous solution for hydrolysis of said solids to sugar, said solids being of greater density than said solution; a steam boiler connected to said second tangential entry for introducing steam in support of said cyclonic flow and to provide heat for hydrolysis within said reaction chamber, said cylonic flow biasing slurry solids towards the outer periphery and slurry solution towards the central portion of said reaction chamber; slurry discharge means disposed at the central portion of said reaction chamber for withdrawing slurry with solution of enriched sugar content, said slurry solids being retained longer than said solution within said reaction chamber due to the biasing of solids towards said peripheral wall by said cyclonic flow; and a let-down orifice coupled to said discharge means for reducing the slurry temperature and stopping the hydrolysis process.
Claim 3
Dependent Claim
25 words
The system of claim 1 wherein a condenser cooler is included in combination with said let-down orifice for effecting cooling and stopping the hydrolysis process.
Claim 4
Dependent Claim
228 words
A countercurrent-flow reactor system for the hydrolysis of cellulosic or lignocellulosic material to sugar comprising: a hollow, cylindrical reactor vessel having an internal reaction chamber defined by a peripheral, annular wall and end walls having inwardly extending central cores to define a central portion of said chamber of less height than that at said peripheral wall; a source of slurry connected to said reaction chamber radially inward from said peripheral, annular wall and radially outward from said central portion of said reaction chamber, said slurry including cellulosic or lignocellulosic solids and aqueous solution for hydrolysis of said solids to sugar, said solids being of greater density than said solution; a steam boiler tangentially connected to the outer periphery of said reaction chamber for introducing steam and establishing cyclonic flow of solids and solution to bias solids towards the outer periphery and solution towards the central portion of said reaction chamber; first discharge means at the outer periphery opposite to the tangential connection of said steam boiler for withdrawing solids-rich slurry from said reaction chamber; said discharge means at said central portion for withdrawing solution-rich slurry from said reaction chamber at a location inwardly from said slurry source connection whereby a countercurrent flow of solution and solids is established; and first and second let-down orifices for stopping the hydrolysis process connected to said first and second discharge means respectively.
Claim 5
Dependent Claim
228 words
A countercurrent-flow reactor system for the hydrolysis of cellulosic or lignocellulosic material to sugar comprising: a hollow, cylindrical reactor vessel having an internal reaction chamber defined by a peripheral, annular wall and end walls having inwardly extending central cores to define a central portion of said chamber of less height than that at said peripheral wall; a source of slurry connected to said reaction chamber radially inward from said peripheral, annular wall and radially outward from said central portion of said reaction chamber, said slurry including cellulosic or lignocellulosic solids and aqueous solution for hydrolysis of said solids to sugar, said solids being of greater density than said solution; a steam boiler tangentially connected to the outer periphery of said reaction chamber for introducing steam and establishing cyclonic flow of solids and solution to bias solids towards the outer periphery and solution towards the central portion of said reaction chamber; first discharge means at the outer periphery opposite to the tangential connection of said steam boiler for withdrawing solids-rich slurry from said reaction chamber; said discharge means at said central portion for withdrawing solution-rich slurry from said reaction chamber at a location inwardly from said slurry source connection whereby a countercurrent flow of solution and solids is established; and first and second let-down orifices for stopping the hydrolysis process connected to said first and second discharge means respectively.
References Cited (Backward Citations)
GB329600A
Cited
US2304679A
Cited
US2739876A
Cited
US2737414A
Cited
US3322506A
Cited
US3284055A
Cited
US3495949A
Cited
US3519397A
Cited
US3739910A
Cited
US4059419A
Cited
US3802570A
Cited
US3920423A
Cited
US4005998A
Cited
US4205965A
Cited
US4273750A
Cited
US4339206A
Cited
US4612088A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1992-04-03 | 1992-10-03 | 1993-04-04 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1996-04-03 | 1996-10-03 | 1997-04-04 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2000-04-03 | 2000-10-03 | 2001-04-04 | $7700.00 | Window Closed / Lapsed |