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US4810415A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for manufacturing ultra pure silica and resulting encapsulated products

Assignee: Indresco Inc
•
Filing: 1986-09-10
•
Granted: 1989-03-07
•
Expires: 2006-09-10
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Abstract

Abstract High purity silica powder formed from a sol-gel process is made from a quantity of an industrial grade hydrolizable silicon organometallic substance mixed with a quantity of an industrial grade organic solvent miscible in said organometallic substance and with a quantity of an acidified water having a pH less than 2 to form a solution. The solution is heated, then dried to form a gel, milled, and calcined to form the pure silica powder and the pure powder used to form encapsulated micro-miniature circuits.

Inventors

  • 👤 Howard M. Winkelbauer
  • 👤 Glenn A. Moore

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-06 00:37
CPC Classifications
C; C01; C01B; C01B33/00; C01B33/113; C01B33/12; C01B33/16; C01B33/163

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 96 words
A composition for forming a pure silica powder consisting essentially of: a quantity of an industrial grade hydrolyzable silicon organometallic substance; a quantity of an industrial grade organic solvent miscible in said substance, the ratio by volume of said solvent to said organometallic substance being from about 0.1 to about 1:1; a quantity of acidified distilled water having a pH less than 2; and micronized fumed silica; the quantity of said water being from about 520 to about 720% of the stoichiometric amount and the micronized silica being present in an amount up to 16 wt%.
Claim 2
Dependent Claim 96 words
A composition for forming a pure silica powder consisting essentially of: a quantity of an industrial grade hydrolyzable silicon organometallic substance; a quantity of an industrial grade organic solvent miscible in said substance, the ratio by volume of said solvent to said organometallic substance being from about 0.1 to about 1:1; a quantity of acidified distilled water having a pH less than 2; and micronized fumed silica; the quantity of said water being from about 520 to about 720% of the stoichiometric amount and the micronized silica being present in an amount up to 16 wt%.
Claim 3
Dependent Claim 13 words
A composition in accordance with claim 1 wherein the organometallic substance is tetraethylorthosilicate.
Claim 4
Dependent Claim 13 words
A composition in accordance with claim 2 wherein the organic solvent is ethanol.
Claim 5
Dependent Claim 13 words
A composition in accordance with claim 1 wherein the organic solvent is ethanol.

References Cited (Backward Citations)

US3672833A Cited
US4053565A Cited
US4006175A Cited
US4243422A Cited
US4070286A Cited
US4228261A Cited
US4249903A Cited
US4327065A Cited
US4619908A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1992-03-06 1992-09-05 1993-03-07 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1996-03-06 1996-09-05 1997-03-07 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2000-03-06 2000-09-05 2001-03-07 $7700.00 Window Closed / Lapsed

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