US4801411A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Method and apparatus for producing monosize ceramic particles
Assignee: Southwest Research Institute
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Filing: 1986-06-05
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Granted: 1989-01-31
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Expires: 2006-06-05
Abstract
Abstract A method and apparatus for producing uniform, monosize ceramic particles forming the microsize particles by vapor condensation or ultrasonic cavitation. Organometallic liquids are directed to an aerosol generator where a droplet stream is projected in free flight within a reaction chamber and a particle sorter. Through the process of sorting the droplets according to their velocity in flight, monosize droplets are collected. The particles may be reacted prior to or after sorting and collection to form the monosize ceramic particle of interest. Sintering aids are introduced into the process to produce ceramic particles capable of improved green body formation.
Inventors
- 👤 Stephen T. Wellinghoff
- 👤 Thomas E. Owen
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-25 09:04
CPC Classifications
B; B05; B05B; B05B17/00; B05B17/04; B05B17/06; B05B17/0607; B05B17/0615; B01; B01J; B01J13/00; B01J13/0095; C; C01; C01B; C01B13/00; C01B13/14; C01B13/32; C01G; C01G25/00; C01G25/02; C01P; C01P2002/00; C01P2002/20; C01P2002/22; C01P2004/00; C01P2004/51; C01P2004/52
Claims Analysis
Total Claims: 2
Claim 1
Independent Claim
125 words
A method for producing two-layer ceramic particles comprising the steps of: a. directing an immiscible combination of an organometallic liquid and surface coating liquid to an aerosol particle generator; b. separating at said generator said organometallic liquid to a top layer and said surface coating liquid to a bottom layer; c. mechanically exciting said layers whereby said organometallic liquid mixes with said surface coating liquid said mechanical excitation generating and releasing simultaneously into a space from a single discharge opening a multiplicity of two-layered microparticles thereby forming a stream of said two-layered microparticles in said space; d. electrostatically charging said two-layered microparticles to induce particle repulsion; e. separating from said charged microparticles, microparticles having substantially equal size; and f. oxidizing said substantially equal size microparticles.
Claim 2
Independent Claim
125 words
A method for producing two-layer ceramic particles comprising the steps of: a. directing an immiscible combination of an organometallic liquid and surface coating liquid to an aerosol particle generator; b. separating at said generator said organometallic liquid to a top layer and said surface coating liquid to a bottom layer; c. mechanically exciting said layers whereby said organometallic liquid mixes with said surface coating liquid said mechanical excitation generating and releasing simultaneously into a space from a single discharge opening a multiplicity of two-layered microparticles thereby forming a stream of said two-layered microparticles in said space; d. electrostatically charging said two-layered microparticles to induce particle repulsion; e. separating from said charged microparticles, microparticles having substantially equal size; and f. oxidizing said substantially equal size microparticles.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1992-01-31 | 1992-08-01 | 1993-01-31 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1996-01-31 | 1996-08-01 | 1997-01-31 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2000-01-31 | 2000-08-01 | 2001-01-31 | $7700.00 | Window Closed / Lapsed |