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Process for preparing microporous polyvinylidene fluoride membranes

Assignee: IONICS INCORPORATED 65 GROVE STREET WATERTOWN MASSACHUSETTS 02172
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Filing: 1988-02-22
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Granted: 1988-10-04
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Expires: 2008-02-22
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Abstract

Abstract A process for preparing assymetric polyvinylidene fluoride microporous membranes using novel pore forming agents of an ammonium salt which is a non-solvent for the polymeric casting solution; such agents for example being ammonium hydroxide, ammonium chloride and the like.

Inventors

  • 👤 Thomas J. Susa

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 19:27
CPC Classifications
C; C08; C08J; C08J9/00; C08J9/26; B; B01; B01D; B01D67/00; B01D67/0002; B01D67/0009; B01D67/0011; B01D71/00; B01D71/06; B01D71/30; B01D71/32; B01D71/34; C08J9/28; C08J2327/00; C08J2327/02; C08J2327/12; C08J2327/16

Claims Analysis

Total Claims: 3
Claim 1
Independent Claim 76 words
A casting solution adapted to be partially evaporated to form a film for subsequent conversion into a microporous membrane by leaching, said casting solution comprising about 14-21 wt. % of vinylidene fluoride polymer, 79-86 wt. % of a polar solvent capable of dissolving said polymer and between about 0.05-500 parts per million of a pore forming agent selected from the group consisting of ammonium hydroxide, ammonium acetate, ammonium bifluoride, ammonium carbonate, ammonium chloride and ammonium thiocyanate.
Claim 2
Dependent Claim 76 words
A casting solution adapted to be partially evaporated to form a film for subsequent conversion into a microporous membrane by leaching, said casting solution comprising about 14-21 wt. % of vinylidene fluoride polymer, 79-86 wt. % of a polar solvent capable of dissolving said polymer and between about 0.05-500 parts per million of a pore forming agent selected from the group consisting of ammonium hydroxide, ammonium acetate, ammonium bifluoride, ammonium carbonate, ammonium chloride and ammonium thiocyanate.
Claim 3
Dependent Claim 34 words
The casting solution of claim 1 wherein the solvent is selected from the group consisting of dimethyl acetamide, dimethyl formamide, N-methyl-2-pyrrolidone, dimethyl sulfoxide, diethyl acetamide, triethyl phosphate, hexamethly phosphoramide, propylene carbonate, tetramethylurea and acetone.

References Cited (Backward Citations)

US3620895A Cited
US3642668A Cited
US4076656A Cited
US4238571A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1991-10-04 1992-04-04 1992-10-04 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1995-10-04 1996-04-04 1996-10-04 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1999-10-04 2000-04-04 2000-10-04 $7700.00 Window Closed / Lapsed

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