Process for forming flavor compounds in tobacco

Claim 3

The method of claim 1, said tobacco having a moisture content of at least 10% by weight when introduced into said containing zone.

Claim 4

The method of claim 1, and reordering said treated tobacco to a moisture content of 12% to 15% by weight.

Claim 5

The method of claim 1, said tobacco having a moisture content in the range of approximately 10%-60% by weight when introduced into said containing zone.

Claim 6

The method of claim 1, said tobacco having a moisture content advantageously in the range of approximately 14%-21% by weight when introduced into said containing zone.

Claim 7

The method of claim 1, said tobacco being subjected to at least fifteen inches of mercury vacuum when in said containing zone prior to introduction of an ammonia source into said zone.

Claim 8

The method of claim 1, said ammonia source introduced into said containing zone as an ammonia gas.

Claim 9

The method of claim 1, said ammonia source being introduced into said containing zone by pretreating the tobacco with ammonium hydroxide.

Claim 10

The method of claim 1, said heating of said containing zone being accomplished by injecting superheated steam into said containing zone when substantially closed.

Claim 11

The method of claim 1, said temperature range of said tobacco in said containing zone being maintained preferably in the range of approximately 280° to 320° F. when substantially closed.

Claim 12

The method of claim 1, said tobacco temperature in said containing zone being maintained advantageously at approximately 308° F.

Claim 13

The method of claim 1, said temperature range of approximately 250° F. to 350° F. being maintained for a time period in the range of approximately 5 minutes to 24 hours.

Claim 14

The method of claim 1, said heating of said containing zone being accomplished by an injection of steam for approximately twenty minutes at a temperature of approximately 308° F. when said zone is substantially closed.

Claim 15

The method of claim 1, comprising heating said containing zone with steam for ninety minutes at a temperature of approximately 308° F. when said zone is closed.

Claim 16

The method of claim 1, said tobacco being cooled in said containing zone by releasing the gas pressure in said containing zone.

Claim 17

The method of claim 1, said tobacco being cooled in said containing zone by subjecting the containing zone to conductive cooling.

Claim 18

The method of claim 1, said tobacco being cooled in said containing zone by allowing the heat in said tobacco to be reduced to ambient by natural convection.

Claim 19

The method of claim 1, said ammonia source and said heat being introduced to the said containing zone simultaneously.

Claim 20

The method of claim 1, said ammonia source and said heat being introduced to the said containing zone sequentially.

Claim 21

The method of claim 1, said tobacco being a mixture of stem and leaf tobacco in preselected proportions.

Claim 22

The method of claim 1, said tobacco being reconstituted tobacco.

Claim 23

The method of claim 1, said tobacco being substantially of stem type.

Claim 24

The method of claim 1, said tobacco being substantially of leaf type.

Claim 25

The method of claim 1, said heating of said containing zone being controlled to bring the pressure in said zone when substantially closed within an approximate range of at least 30 psig to 90 psig.

Claim 26

The method of claim 1, said heating of said containing zone being controlled to bring the pressure in said zone when substantially closed to advantageously 60 psig.

Claim 27

The method of claim 1, including the step of adding reducing sugars.

Claim 28

The method of claim 1, including the step of adding reducing sugars comprising approximately 20% of the tobacco weight.

Claim 29

A process of forming favorable flavor compounds in a moisturized tobacco comprising: introducing tobacco having a moisture content in the range of approximately 14-21% by weight into a tobacco containing zone; subjecting said tobacco in said containing zone to at least fifteen inches of mercury vacuum when in said containing zone; introducing an ammonia source into said tobacco containing zone; injecting superheated steam into said containing zone when substantially closed to bring the temperature of the tobacco introduced into said zone to a temperature of approximately 308° F. and to a pressure of approximately 60 psig of a period of approximately twenty minutes to cause reaction of the ammonia source and reducing sugars in the tobacco without substantially reducing moisture content of the tobacco to improve tobacco flavor compounds; cooling said tobacco in said containing zone by allowing the heat in said tobacco to be reduced to ambient by natural convection; removing the treated tobacco from the said containing zone; and reordering said treated tobacco to a moisture content of 12% to 15% by weight.

Claim 30

A process of forming favorable flavor compounds in a moisturized tobacco comprising: introducing tobacco having a moisture content in the range of approximately 14-21% by weight into a tobacco containing zone; subjecting said tobacco in said containing zone to at least fifteen inches of mercury vacuum when in said containing zone; introducing an ammonia source into said tobacco containing zone; injecting superheated steam into said containing zone when substantially closed to bring the temperature of the tobacco introduced into said zone to a temperature of approximately 308° F. and to a pressure of approximately 60 psig of a period of approximately twenty minutes to cause reaction of the ammonia source and reducing sugars in the tobacco without substantially reducing moisture content of the tobacco to improve tobacco flavor compounds; cooling said tobacco in said containing zone by allowing the heat in said tobacco to be reduced to ambient by natural convection; removing the treated tobacco from the said containing zone; and reordering said treated tobacco to a moisture content of 12% to 15% by weight.

Claim 31

A process of forming favorable flavor compounds in a moisturized tobacco comprising: introducing tobacco having a moisture content in the range of approximately 14-21% by weight into a tobacco containing zone; introducing an ammonia source into said tobacco containing zone; indirectly heating said tobacco while in said containing zone when substantially closed to bring the temperature of the tobacco introduced into said zone to a temperature of approximately 308° F. and to a pressure of approximately 60 psig for a period of approximately ninety minutes to cause reaction of the ammonia source and reducing sugars in the tobacco without substantially reducing moisture content of the tobacco to improve tobacco flavor compounds; cooling said tobacco in said containing zone by allowing the heat in said tobacco to be reduced to ambient by natural convection; removing the treated tobacco from the said containing zone; and reordering said treated tobacco to a moisture content of 12% to 15% by weight.

Claim 32

A process of forming favorable flavor compounds in a moisturized tobacco comprising: introducing tobacco having a moisture content in the range of approximately 14-21% by weight into a tobacco containing zone; introducing an ammonia source into said tobacco containing zone; indirectly heating said tobacco while in said containing zone when substantially closed to bring the temperature of the tobacco introduced into said zone to a temperature of approximately 308° F. and to a pressure of approximately 60 psig for a period of approximately ninety minutes to cause reaction of the ammonia source and reducing sugars in the tobacco without substantially reducing moisture content of the tobacco to improve tobacco flavor compounds; cooling said tobacco in said containing zone by allowing the heat in said tobacco to be reduced to ambient by natural convection; removing the treated tobacco from the said containing zone; and reordering said treated tobacco to a moisture content of 12% to 15% by weight.