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US4728465A
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US
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Nickelboride-polymer catalyst used in hydrogenation of fatty compounds
Assignee: Unilever Patent Holdings BV
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Filing: 1986-01-24
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Granted: 1988-03-01
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Expires: 2006-01-24
Abstract
Abstract The invention provides a novel, active hydrogenation catalyst comprising nickelboride stabilized with a vinylpyrrolidone group containing polymer, said catalyst satisfies a certain activity test in the hydrogenation of soybean oil. The invention further provides a method for the preparation of said catalyst involving the use of a nickel salt contaiing less than 6, preferably less than 5 molecules of crystal water.
Inventors
- 👤 Rudolph O. DeJongh
- 👤 Cornelis VanDijk
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 11:38
CPC Classifications
B; B01; B01J; B01J23/00; B01J23/70; B01J23/74; B01J31/00; B01J31/02; B01J31/06; B01J23/755; B01J31/26; B01J31/28; C; C11; C11C; C11C3/00; C11C3/12; C11C3/123; B01J2231/00; B01J2231/60; B01J2231/64; B01J2231/641; B01J2231/645
Claims Analysis
Total Claims: 8
Claim 1
Independent Claim
78 words
In a process for the catalytic hydrogenation of an unsaturated fatty compound, the improvement which comprises using, as the catalyst, a finely dispersed nickel boride stabilised with a linear organic polymer, said catalyst being prepared by a process in which an at least partly dissolved nickel salt containing less than 6 molecules of crystal water in the presence of an at least partly dissolved polar linear polymer of vinylpyrrolidone is reduced with the aid of an alkali borohydride.
Claim 2
Dependent Claim
78 words
In a process for the catalytic hydrogenation of an unsaturated fatty compound, the improvement which comprises using, as the catalyst, a finely dispersed nickel boride stabilised with a linear organic polymer, said catalyst being prepared by a process in which an at least partly dissolved nickel salt containing less than 6 molecules of crystal water in the presence of an at least partly dissolved polar linear polymer of vinylpyrrolidone is reduced with the aid of an alkali borohydride.
Claim 3
Dependent Claim
20 words
The process of claim 1 wherein the amount of catalyst used, calculated as nickel, is between 5 and 500 ppm.
Claim 4
Dependent Claim
19 words
A process as claimed in claim 2 wherein the amount of nickelboride catalyst is between 5 and 200 ppm.
Claim 5
Dependent Claim
15 words
A process as claimed in claim 3 wherein the cataylst is dispersed in a triglyceride.
Claim 6
Dependent Claim
17 words
A process as claimed in claim 4 wherein the unsaturated hydrocarbon which is hydrogenated is a triglyceride.
Claim 7
Dependent Claim
24 words
The process of claim 5 wherein the hydrogen pressure is between 100 and 500 kPa and the temperature is between 20° and 180° C.
Claim 8
Dependent Claim
10 words
The process of claim 6 wherein the polymer is polyvinylpyrrolidone.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1991-03-01 | 1991-08-31 | 1992-03-01 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1995-03-01 | 1995-08-31 | 1996-03-01 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1999-03-01 | 1999-08-31 | 2000-03-01 | $7700.00 | Window Closed / Lapsed |