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US4726983A Expired / Lapsed US ⏱️ 0.0 years remaining

Homogeneous fine grained metal film on substrate and manufacturing method thereof

Assignee: Mitsubishi Electric Corp
•
Filing: 1985-12-20
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Granted: 1988-02-23
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Expires: 2005-12-20
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Abstract

Abstract A homogeneous fine grained metal film (6') on a substrate in accordance with the present invention comprises multiple metal layers and intervening layers (14) between the respective metal layers, the intervening layers being formed of a compound of the metal and a reactive gas and serving to suppress growth of grains (12') in the respective metal layers and to suppress electromigration of grain boundaries (13'). In a method for manufacturing a metal film (6') having homogeneous and fine grains on a substrate in accordance with the present invention, one or more intervening layers (14) are formed by introducing a gas reactive with the metal film one or more times during deposition of the metal film, whereby intervening layers of a metal compound are interposed between the successively deposited metal layers. Thus, a metal film of a multilayered structure including multiple metal layers separated by the intervening layers is formed.

Inventors

  • 👤 Hiroshi Harada
  • 👤 Yoshihiro Hirata
  • 👤 Masanobu Tosa

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-31 10:58
CPC Classifications
C; C23; C23C; C23C14/00; C23C14/22; C23C14/34; C23C16/00; C23C16/06; C23C16/08; C23C16/12; C23C14/0021; C23C14/0036; C23C14/0073; C23C14/02; C23C14/024; C23C16/02; C23C16/0272; H; H10; H10W; H10W20/00; H10W20/01; H10W20/031; H10W20/064; H10W20/40; H10W20/41; H10W20/44; H10W20/4403; H10W20/4405; Y; Y10; Y10T; Y10T428/00; Y10T428/24; Y10T428/24942; Y10T428/2495; Y10T428/24967

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 101 words
A metal film arrangement (6') on a substrate, comprising: multiple layers of metal, and intervening layers (14) interposed between said respective metal layers, said intervening layers serving to suppress growth of grains (12') in said metal layers and to suppress electromigration of grain boundaries (13), wherein each metal layer of said multiple layers consists essentially of homogeneous fine grains of said metal and the thickness of each metal layer separated by the intervening layers corresponds to the grain size of metal in said metal layers, wherein said intervening layers are formed of a compound of said metal and a reactive gas.
Claim 2
Dependent Claim 101 words
A metal film arrangement (6') on a substrate, comprising: multiple layers of metal, and intervening layers (14) interposed between said respective metal layers, said intervening layers serving to suppress growth of grains (12') in said metal layers and to suppress electromigration of grain boundaries (13), wherein each metal layer of said multiple layers consists essentially of homogeneous fine grains of said metal and the thickness of each metal layer separated by the intervening layers corresponds to the grain size of metal in said metal layers, wherein said intervening layers are formed of a compound of said metal and a reactive gas.
Claim 3
Dependent Claim 19 words
A metal film in accordance with claim 1, wherein said metal is one of aluminum or an aluminum alloy.
Claim 4
Dependent Claim 14 words
A metal film in accordance with claim 2, wherein said reactive gas includes oxygen.
Claim 5
Dependent Claim 14 words
A metal film in accordance with claim 2, wherein said reactive gas includes nitrogen.

References Cited (Backward Citations)

DE2125643A1 Cited
DE3033513A1 Cited
US4364995A Cited
US4613549A Cited
US4590130A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1991-02-22 1991-08-24 1992-02-23 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1995-02-22 1995-08-24 1996-02-23 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1999-02-22 1999-08-24 2000-02-23 $7700.00 Window Closed / Lapsed

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