Patent US4725449A successfully refreshed from Google Patents.
US4725449A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Method of making radio frequency ion source antenna
Assignee: United States Department of Energy
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Filing: 1987-02-27
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Granted: 1988-02-16
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Expires: 2007-02-27
Abstract
Abstract In the method, the radio frequency (RF) antenna is made by providing a clean coil made of copper tubing or other metal conductor, which is coated with a tacky organic binder, and then with a powdered glass frit, as by sprinkling the frit uniformly over the binder. The coil is then heated internally in an inert gas atmosphere, preferably by passing an electrical heating current along the coil. Initially, the coil is internally heated to about 200° C. to boil off the water from the binder, and then to about 750° C.-850° C. to melt the glass frit, while also burning off the organic binder. The melted frit forms a molten glass coating on the metal coil, which is then cooled to solidify the glass, so that the metal coil is covered with a thin continuous homogeneous impervious glass coating of substantially uniform thickness. The glass coating affords complete electrical insulation and complete dielectric protection for the metal coil of the RF antenna, to withstand voltage breakdown and to prevent sputtering, while also doubling the plasma generating efficiency of the RF antenna, when energized with RF power in the vacuum chamber of an ion source for a particle accelerator or the like. The glass frit preferably contains apprxoimately 45% lead oxide.
Inventors
- 👤 Kenneth W. Ehlers
- 👤 Ka-Ngo Leung
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-07 07:57
CPC Classifications
C; C23; C23D; C23D5/00; C23D5/02; H; H01; H01Q; H01Q1/00; H01Q1/36
Claims Analysis
Total Claims: 16
Claim 1
Independent Claim
133 words
A method of making a radio frequency ion source antenna, comprising the steps of providing a clean electrically conductive metal antenna coil having power lead-ins, coating the coil with a tacky organic binder, coating the binder with a fine powdered glass frit having a melting temperature lower than the melting temperature of the metal of the antenna coil, heating the coil internally to a temperature between the melting temperature of the glass frit and the metal melting temperature to melt the glass frit and to cause the melted glass frit to flow as a coating of melted glass of substantially uniform thickness over the surface of the antenna coil while burning off the organic binder, and cooling the coil to solidify the melted glass as an adherent glass coating on the antenna coil.
Claim 2
Independent Claim
133 words
A method of making a radio frequency ion source antenna, comprising the steps of providing a clean electrically conductive metal antenna coil having power lead-ins, coating the coil with a tacky organic binder, coating the binder with a fine powdered glass frit having a melting temperature lower than the melting temperature of the metal of the antenna coil, heating the coil internally to a temperature between the melting temperature of the glass frit and the metal melting temperature to melt the glass frit and to cause the melted glass frit to flow as a coating of melted glass of substantially uniform thickness over the surface of the antenna coil while burning off the organic binder, and cooling the coil to solidify the melted glass as an adherent glass coating on the antenna coil.
Claim 3
Dependent Claim
26 words
A method according to claim 1, in which the coil is heated internally by passing an electric current along the coil to heat the coil resistively.
Claim 4
Dependent Claim
22 words
A method according to claim 1, in which the heating and cooling of the coil are done in an inert gas atmosphere.
Claim 5
Dependent Claim
52 words
A method according to claim 1, in which the organic binder includes water, and in which the internal heating of the antenna coil is initially done to a temperature above 100° C. until the water is evaporated, following which the coil is heated to a higher temperature to melt the glass frit.
Claim 6
Dependent Claim
67 words
A method according to claim 1, in which the organic binder includes water, the coil being heated internally by passing an electric current along the coil, such electric current being initially regulated to heat the coil to a temperature above 100° C. until the water is evaporated, following which the electric current is increased to heat the coil to a higher temperature for melting the glass frit.
Claim 7
Dependent Claim
22 words
A method according to claim 5, in which the heating and cooling of the coil are done in an inert gas atmosphere.
Claim 8
Dependent Claim
20 words
A method according to claim 1, in which the powdered glass frit is of the order of 80 mesh size.
Claim 9
Dependent Claim
25 words
A method according to claim 1, in which the glass frit is a lead glass frit containing lead oxide in an approximate concentration of 45%.
Claim 10
Dependent Claim
61 words
A method according to claim 1, in which the organic binder contains water, the internal heating of the antenna coil being done by initially heating the coil to a temperature of the order of 200° C. to drive off the water, after which the coil is heated to a temperature of the order of 750°-850° C. to melt the glass frit.
Claim 11
Independent Claim
179 words
A method of making a radio frequency ion source antenna, comprising the steps of providing a clean electrically conductive metal antenna coil having power lead-ins, coating the coil with a tacky organic binder, coating the binder with a fine powdered glass frit containing lead oxide in an approximate concentration of 45% and having a melting temperature lower than the melting temperature of the metal of the antenna coil, heating the coil internally to a temperature between the melting temperature of the glass frit and the melting temperature of the metal to melt the glass frit and to cause the glass frit to flow as a thin melted glass coating of substantially uniform thickness over the surface of the antenna coil while burning off the organic binder, such heating being done by passing sufficient electric current along the coil to heat the coil resistively, and cooling the coil for solidifying the melted glass to form an adherent glass coating on the coil, the heating and cooling of the coil being done while maintaining the coil in an inert gas atmosphere.
Claim 12
Independent Claim
179 words
A method of making a radio frequency ion source antenna, comprising the steps of providing a clean electrically conductive metal antenna coil having power lead-ins, coating the coil with a tacky organic binder, coating the binder with a fine powdered glass frit containing lead oxide in an approximate concentration of 45% and having a melting temperature lower than the melting temperature of the metal of the antenna coil, heating the coil internally to a temperature between the melting temperature of the glass frit and the melting temperature of the metal to melt the glass frit and to cause the glass frit to flow as a thin melted glass coating of substantially uniform thickness over the surface of the antenna coil while burning off the organic binder, such heating being done by passing sufficient electric current along the coil to heat the coil resistively, and cooling the coil for solidifying the melted glass to form an adherent glass coating on the coil, the heating and cooling of the coil being done while maintaining the coil in an inert gas atmosphere.
Claim 13
Dependent Claim
65 words
A method according to claim 10, in which the organic binder contains water, the heating of the coil being done by initially heating the coil to a temperature on the order of 200° C. until the water is boiled off, and then heating the coil to a temperature on the order of 750°-850° C. to melt the glass frit and to burn off the binder.
Claim 14
Dependent Claim
32 words
A method according to claim 10, in which the coil is heated to a temperature on the order of 750°-850° C. to melt the glass frit and to burn off the binder.
Claim 15
Dependent Claim
16 words
A method according to claim 10, in which the antenna coil is made of copper tubing.
Claim 16
Dependent Claim
73 words
A method according to claim 10, in which the antenna coil is made of copper tubing, the organic binder containing water, the heating of the coil being done by initially heating the coil to a temperature on the order of 200° C. to boil off the water, following which the coil is heated to a temperature on the order of 750°-850° C. to melt the glass frit and to burn off the binder.
References Cited (Backward Citations)
No citation records indexed.
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1991-02-15 | 1991-08-17 | 1992-02-16 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1995-02-15 | 1995-08-17 | 1996-02-16 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1999-02-15 | 1999-08-17 | 2000-02-16 | $7700.00 | Window Closed / Lapsed |