US4723966A
Expired / Lapsed
US
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Gas separation by pressure swing adsorption
Assignee: Katalistiks International Inc
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Filing: 1986-12-11
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Granted: 1988-02-09
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Expires: 2006-12-11
Abstract
Abstract A pressure swing adsorption process is disclosed wherein binary gas purification is effected from a single adsorbent bed. An adsorbent bed is charged under pressure with a gas mixture having some components that are more adsorbable than others. The process causes the bed to be polarized with one end of the bed containing the more adsorbable components and the other end containing the less adsorbable components. Once charged, the bed is depressurized simultaneously from both ends, thus removing the separated components from their respective ends.
Inventors
- 👤 Andrija Fuderer
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-26 02:20
CPC Classifications
B; B01; B01D; B01D53/00; B01D53/02; B01D53/04; B01D53/047; B01D2253/00; B01D2253/10; B01D2253/102; B01D2253/104; B01D2253/106; B01D2253/108; B01D2253/30; B01D2253/302; B01D2253/304; B01D2256/00; B01D2256/10; B01D2256/16; B01D2256/22; B01D2257/00; B01D2257/10; B01D2257/104; B01D2257/50; B01D2257/502; B01D2257/504; B01D2257/70; B01D2257/702; B01D2257/7022; B01D2257/7025; B01D2259/00; B01D2259/40; B01D2259/40011; B01D2259/40028; B01D2259/4003; B01D2259/40032; B01D2259/40035; B01D2259/40041; B01D2259/40043; B01D2259/4005; B01D2259/40052; B01D2259/40058; B01D2259/40066; B01D2259/40067; B01D2259/40071; B01D2259/40073; B01D2259/404; B01D2259/406; B01D2259/4062; B01D2259/4066; B01D2259/414; B01D2259/4141; B01D2259/4145; B01D2259/4146; B01D53/0476; Y; Y02; Y02C; Y02C20/00; Y02C20/20; Y02C20/40
Claims Analysis
Total Claims: 38
Claim 1
Independent Claim
135 words
A method for gas separation of adsorbable components from less adsorbable components on fixed adsorbent beds, comprising the steps of: (a) flowing a feed gas mixture under adsorption pressure to an adsorbent bed to selectively adsorb components from said feed gas onto the adsorbent bed, said bed having a feed end and a product end; and (b) displacing said feed gas with a gas having a higher concentration of adsorbable components, whereby less adsorbable components are displaced from a portion of the bed; and (c) depressurizing the bed by taking out gas simultaneously from at least two different locations of the bed to recover essentially pure less adsorbable components at the product end of the bed and to recover the adsorbable components from at least one of the different locations; and (d) pressurizing the bed.
Claim 2
Independent Claim
135 words
A method for gas separation of adsorbable components from less adsorbable components on fixed adsorbent beds, comprising the steps of: (a) flowing a feed gas mixture under adsorption pressure to an adsorbent bed to selectively adsorb components from said feed gas onto the adsorbent bed, said bed having a feed end and a product end; and (b) displacing said feed gas with a gas having a higher concentration of adsorbable components, whereby less adsorbable components are displaced from a portion of the bed; and (c) depressurizing the bed by taking out gas simultaneously from at least two different locations of the bed to recover essentially pure less adsorbable components at the product end of the bed and to recover the adsorbable components from at least one of the different locations; and (d) pressurizing the bed.
Claim 3
Dependent Claim
26 words
The method of claim 1 wherein the step of depressurizing is simultaneously taking out gas from the feed end and the product end of the bed.
Claim 4
Dependent Claim
30 words
The method of claim 1 wherein the step of depressurizing is simultaneously taking out gas at a side takeout of the bed and at the product end of the bed.
Claim 5
Dependent Claim
40 words
The method of claim 1 where the step of depressurizing further comprises the steps of simultaneously taking out gas from the product end and the side takeout, and simultaneously taking out gas from the feed end and the product end.
Claim 6
Dependent Claim
25 words
The method of claim 1 wherein the step of depressurizing is taking out gas simultaneously from the feed end, product end and a side take-out.
Claim 7
Dependent Claim
24 words
The method of claim 1 further comprising the step of purging the bed with the less adsorbable components prior to the step of repressurizing.
Claim 8
Dependent Claim
27 words
The method of claim 6 wherein said step of purging is carried out with a purge gas obtained from the product end during said step of depressurizing.
Claim 9
Dependent Claim
20 words
The method of claim 1 wherein said steps of flowing and displacing are carried out at essentially the same pressure.
Claim 10
Dependent Claim
30 words
The method of claim 1 further comprising the step of depressurizing the bed from a side takeout prior to said step of depressurizing the bed by taking out gas simultaneously.
Claim 11
Dependent Claim
28 words
The method of claim 1 further comprising the step of depressurizing said bed in a cocurrent direction, said cocurrent depressurization occurring prior to said step of simultaneously depressurizing.
Claim 12
Dependent Claim
17 words
The method of claim 10 wherein said cocurrent depressurization step is performed before said step of displacing.
Claim 13
Dependent Claim
27 words
The method of claim 11 where the step of cocurrent depressurizing further comprises the step of repressurizing other beds with a gas obtained from the product end.
Claim 14
Dependent Claim
19 words
The method of claim 10 wherein said step of cocurrent depressurization is performed simultaneously with said step of displacing.
Claim 15
Dependent Claim
18 words
The method of claim 10 wherein said step of cocurrent depressurization is performed after said step of displacing.
Claim 16
Dependent Claim
24 words
The method of claim 10 where the step of cocurrent depressurizing further comprises repressurizing other beds with a gas obtained from the product end.
Claim 17
Dependent Claim
37 words
The method of claim 10 wherein the step of cocurrent depressurization is continued to a sufficiently low pressure to position a mass transfer front within said bed for maximum separating efficiency in said step of simultaneously depressurizing.
Claim 18
Dependent Claim
27 words
The method of claim 10 wherein the step of displacing further comprises the step of flowing said first component recovered from the feed end onto said bed.
Claim 19
Dependent Claim
25 words
The method of claim 17 wherein said first component comprises carbon monoxide, carbon dioxide, or methane and wherein said second component comprises hydrogen or nitrogen.
Claim 20
Dependent Claim
34 words
The method of claim 18 wherein said adsorbent bed is a material that contains a member selected from the group consisting of zeolitic molecular sieves, activated carbon, silica gel, activated alumina, and mixtures thereof.
Claim 21
Dependent Claim
16 words
The method of claim 1 wherein said step of displacing is performed using fixed position valves.
Claim 22
Dependent Claim
15 words
The method of claim 1 wherein said step of displacing is performed using volumetric compressors.
Claim 23
Dependent Claim
15 words
The method of claim 1 wherein the number of adsorbent beds is at least four.
Claim 24
Dependent Claim
13 words
The method of claim 1 wherein the number of adsorbent beds is five.
Claim 25
Dependent Claim
13 words
The method of claim 1 wherein the number of adsorbent beds is six.
Claim 26
Dependent Claim
22 words
The method of claim 24 wherein the step of selectively adsorbing components occurs in at least one bed at any given time.
Claim 27
Independent Claim
137 words
A method for gas purification, comprising the steps of: (a) flowing a feed gas mixture current under pressure through a fixed adsorbent bed, said mixture flowing firstly through a feed end, secondly through said bed, and thirdly out through a product end, said mixture comprising at least two components wherein a first component is more adsorbable than a second component, said first component being selectively adsorbed onto said bed; and (b) displacing said mixture with a gas having a higher concentration of said first component, whereby said second component is displaced from said feed end; and (c) depressurizing both of said ends simultaneously by lowering said pressure, whereby said first component is recovered from said feed end in a substantially pure state and said second component is recovered from said product end in a substantially pure state.
Claim 28
Independent Claim
137 words
A method for gas purification, comprising the steps of: (a) flowing a feed gas mixture current under pressure through a fixed adsorbent bed, said mixture flowing firstly through a feed end, secondly through said bed, and thirdly out through a product end, said mixture comprising at least two components wherein a first component is more adsorbable than a second component, said first component being selectively adsorbed onto said bed; and (b) displacing said mixture with a gas having a higher concentration of said first component, whereby said second component is displaced from said feed end; and (c) depressurizing both of said ends simultaneously by lowering said pressure, whereby said first component is recovered from said feed end in a substantially pure state and said second component is recovered from said product end in a substantially pure state.
Claim 29
Dependent Claim
34 words
The method of claim 26 further comprising the step of cocurrently depressurizing said bed to position a mass transfer front within said bed, said cocurrent depressurization step occuring prior to said simultaneous depressurizing step.
Claim 30
Dependent Claim
17 words
The method of claim 27 wherein said cocurrent depressurization step is prior to said step of displacing.
Claim 31
Dependent Claim
18 words
The method of claim 27 wherein said cocurrent depressurization step is performed subsequent to said step of displacing.
Claim 32
Dependent Claim
23 words
The method of claim 27 where said step of cocurrent depressurization further comprises the step of lowering said pressure at said product end.
Claim 33
Dependent Claim
27 words
The method of claim 27 where said step of cocurrent depressurization further comprises the step of lowering said pressure at a side take-out located on said bed.
Claim 34
Dependent Claim
27 words
The method of claim 31 where said step of displacing further comprises the step of flowing said first component recovered from said feed end into said bed.
Claim 35
Dependent Claim
20 words
The method of claim 32 further comprising the step of pressurizing said bed subsequent to the step of simultaneous depressurization.
Claim 36
Dependent Claim
24 words
The method of claim 33 wherein said first component comprises carbon monoxide, oxygen, or methane and wherein said second component comprises hydrogen or nitrogen.
Claim 37
Dependent Claim
34 words
The method of claim 34 wherein said adsorbent bed is a material that contains a member selected from the group consisting of zeolitic molecular sieves, activated carbon, silica gel, activated alumina, and mixtures thereof.
Claim 38
Dependent Claim
18 words
The method of claim 26 wherein said cocurrent depressurization step is performed simultaneously with said step of displacing.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1991-02-08 | 1991-08-10 | 1992-02-09 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1995-02-08 | 1995-08-10 | 1996-02-09 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1999-02-08 | 1999-08-10 | 2000-02-09 | $7700.00 | Window Closed / Lapsed |