Patent US4722754A successfully refreshed from Google Patents.
US4722754A
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Superplastically formable aluminum alloy and composite material
Assignee: Boeing North American Inc
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Filing: 1986-09-10
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Granted: 1988-02-02
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Expires: 2006-09-10
Abstract
Abstract Superplastically formable aluminum alloys and composite materials are prepared from rapidly solidified, coarse aluminum powder of a precipitation hardenable alloy, processed to have a low oxide and contaminant content. The powder is mixed, together with reinforcement in the case of the composite material, and then consolidated and extruded at a high extrusion ratio to promote microstructural uniformity and to break up the surface oxide present on the particles. The extrusion is then thermomechanically processed to impart a recrystallized fine-grain aluminum microstructure which is suitable for use in superplastic forming. The unreinforced powder alloy exhibits uniform elongations of over 800 percent at a strain rate of 2x10-4 per second, and a composite having 0.10 volume fraction silicon carbide reinforcement exhibits uniform elongations of over 450 percent at the same strain rate.
Inventors
- 👤 Amit K. Ghosh
- 👤 Murray W. Mahoney
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-31 11:24
CPC Classifications
C; C22; C22C; C22C1/00; C22C1/04; C22C1/05; C22C1/059; C22F; C22F1/00; C22F1/04; C22F1/053; Y; Y10; Y10S; Y10S420/00; Y10S420/902
Claims Analysis
Total Claims: 14
Claim 1
Independent Claim
211 words
A process for preparing a reinforced superplastically formable aluminum composite material, comprising the steps of: furnishing an aluminum powder of a precipitation-hardenable aluminum alloy having a reduced oxygen and oxide content, the powder including coarse powder particles which are of a size that is retained on a 325 mesh standard powder sieve but passes through a 100 mesh standard powder sieve; mixing with the aluminum powder a finely divided reinforcement in an amount less than about 0.20 volume fraction of the total mixture; consolidating the mixture of aluminum powder and reinforcement to form a consolidated billet in a manner minimizing the incorporation of oxygen and oxides into the consolidated billet; extruding the consolidated billet at an extrusion ratio of at least about 12 to 1 to break up the oxide coating on the aluminum powder particles; and thermomechanically processing the reduced billet to yield a microstructure of reinforcement distributed throughout a recrystallized aluminum alloy grain structure having coarse precipitates therein, said step of thermomechanically processing including the substeps of solution treating and quenching the extruded material. overaging the solution treated and quenched material; reducing the thickness of the overaged material by at least about 80 percent by warm rolling and warm cross rolling to form sheet material, and recrystallizing the sheet.
Claim 2
Dependent Claim
211 words
A process for preparing a reinforced superplastically formable aluminum composite material, comprising the steps of: furnishing an aluminum powder of a precipitation-hardenable aluminum alloy having a reduced oxygen and oxide content, the powder including coarse powder particles which are of a size that is retained on a 325 mesh standard powder sieve but passes through a 100 mesh standard powder sieve; mixing with the aluminum powder a finely divided reinforcement in an amount less than about 0.20 volume fraction of the total mixture; consolidating the mixture of aluminum powder and reinforcement to form a consolidated billet in a manner minimizing the incorporation of oxygen and oxides into the consolidated billet; extruding the consolidated billet at an extrusion ratio of at least about 12 to 1 to break up the oxide coating on the aluminum powder particles; and thermomechanically processing the reduced billet to yield a microstructure of reinforcement distributed throughout a recrystallized aluminum alloy grain structure having coarse precipitates therein, said step of thermomechanically processing including the substeps of solution treating and quenching the extruded material. overaging the solution treated and quenched material; reducing the thickness of the overaged material by at least about 80 percent by warm rolling and warm cross rolling to form sheet material, and recrystallizing the sheet.
Claim 3
Dependent Claim
39 words
The process of claim 1, wherein the aluminum alloy consists essentially of about 7 weight percent zinc, 2.3 weight percent magnesium, 2 weight percent copper, 0.12 weight percent chromium. 0.2 weight percent cobalt, 0.23 weight percent zirconium, balance aluminum.
Claim 4
Dependent Claim
11 words
The process of claim 1, wherein the reinforcement is silicon carbide.
Claim 5
Dependent Claim
18 words
The process of claim 3, wherein the silicon carbide reinforcement passes through a 1000 mesh standard powder sieve.
Claim 6
Dependent Claim
16 words
The process of claim 1, wherein the extrusion ratio is at least about 18 to 1.
Claim 7
Dependent Claim
20 words
The process of claim 1, wherein the consolidated billet is contained within an evacuated container during said step of extruding.
Claim 8
Dependent Claim
47 words
The process of claim 1, wherein said step of reducing the thickness is accomplished by warm rolling the overaged material parallel to the extrusion direction to reduce its thickness by about 50 percent, and then warm cross rolling to a reduction of at least about 80 percent.
Claim 9
Dependent Claim
14 words
The process of claim 7, wherein the warm rolling temperature is about 300° C.
Claim 10
Dependent Claim
10 words
A composite material prepared by the process of claim 1.
Claim 11
Dependent Claim
131 words
A process for preparing a reinforced superplastically formable aluminum composite material, comprising the steps of: mixing together a -100 to +325 mesh powder of a precipitation hardenable aluminum alloy, the powder particles having as low an oxygen and oxide content as possible, with up to about 0.20 volume fraction of finely divided silicon carbide reinforcement; consolidating the mixture at elevated temperature and in a vacuum to form a consolidated billet; extruding the consolidated billet at an extrusion ratio of at least about 12 to 1; solution treating the extruded material above its solves temperature and quenching the solution treated material; reducing the thickness of the solution treated and quenched material by at least about 80 percent to form sheet by warm rolling and warm cross rolling; and recrystallizing the rolled sheet.
Claim 12
Dependent Claim
131 words
A process for preparing a reinforced superplastically formable aluminum composite material, comprising the steps of: mixing together a -100 to +325 mesh powder of a precipitation hardenable aluminum alloy, the powder particles having as low an oxygen and oxide content as possible, with up to about 0.20 volume fraction of finely divided silicon carbide reinforcement; consolidating the mixture at elevated temperature and in a vacuum to form a consolidated billet; extruding the consolidated billet at an extrusion ratio of at least about 12 to 1; solution treating the extruded material above its solves temperature and quenching the solution treated material; reducing the thickness of the solution treated and quenched material by at least about 80 percent to form sheet by warm rolling and warm cross rolling; and recrystallizing the rolled sheet.
Claim 13
Dependent Claim
39 words
The process of claim 10, wherein the aluminum alloy consists essentially of about 7 weight percent zinc, 2.3 weight percent magnesium, 2 weight percent copper, 0.1 weight percent chromium, 0.2 weight percent cobalt, 0.23 weight percent zirconium, balance aluminum.
Claim 14
Dependent Claim
10 words
A composite material prepared by the process of claim 10.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1991-02-01 | 1991-08-03 | 1992-02-02 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1995-02-01 | 1995-08-03 | 1996-02-02 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1999-02-01 | 1999-08-03 | 2000-02-02 | $7700.00 | Window Closed / Lapsed |