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US4711784A Expired / Lapsed US ⏱️ 0.0 years remaining

Encapsulation composition for use with chewing gum and edible products

Assignee: Intercontinental Great Brands LLC
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Filing: 1986-01-07
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Granted: 1987-12-08
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Expires: 2006-01-07
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Abstract

Abstract The present invention is method and composition for protecting an active ingredient and providing controlled release therefor, especially in a chewing gum composition, which includes a high molecular weight polyvinyl acetate blended with a hydrophobic plasticizer which forms a film with the high molecular weight polyvinyl acetate in the absence of an added solvent therefor. The active ingredient, such as the artificial sweetener aspartame, is blended into the encapsulating composition as, for example, by melt blend which can then be cooled to a solid and ground into particulate. The encapsulated active ingredient can then be used in a composition for ingestion by a human in the form of, for example, a chewing gum with extended shelf life and highly controlled release of the active ingredient.

Inventors

  • 👤 Robert K. Yang

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 22:12
CPC Classifications
A; A23; A23G; A23G4/00; A23G4/06; A23G4/02; A23G4/18; A23G4/20; A23V; A23V2002/00

Claims Analysis

Total Claims: 22
Claim 1
Independent Claim 69 words
A chewing gum composition containing a sweetener encapculated in a solvent-free encapsulation composition, wherein the encapsulation composition comprises a blend of high molecular weight polyvinyl acetate having a molecular weight of about 20,000 to about 100,000 MWU and a hydrophobic plasticizer, said polyvinyl acetate and hydrophobic plasticizer being present in a ratio of about 5:1 to about 1:5, and wherein said blend is capable of forming an encapsulating film.
Claim 2
Dependent Claim 69 words
A chewing gum composition containing a sweetener encapculated in a solvent-free encapsulation composition, wherein the encapsulation composition comprises a blend of high molecular weight polyvinyl acetate having a molecular weight of about 20,000 to about 100,000 MWU and a hydrophobic plasticizer, said polyvinyl acetate and hydrophobic plasticizer being present in a ratio of about 5:1 to about 1:5, and wherein said blend is capable of forming an encapsulating film.
Claim 3
Dependent Claim 22 words
The composition of claim 1, wherein said polyvinyl acetate has a molecular weight of from about 30,000 MWU to about 60,000 MWU.
Claim 4
Dependent Claim 35 words
The composition of claim 1 wherein said hydrophobic plasticizer comprises a mono-, di- or triglyceride or ester derivatives thereof, said plasticizer having a fatty acid chain of from about 16 to about 22 carbon atoms.
Claim 5
Dependent Claim 32 words
The composition of claim 1 wherein said polyvinyl acetate has a molecular weight of about 40,000 and said hydrophobic plasticizer has a fatty acid chain of from 18 to 20 carbon atoms.
Claim 6
Dependent Claim 15 words
The composition of claim 1 wherein said ratio is from about 2:1 to about 1:2.
Claim 7
Dependent Claim 21 words
The composition of claim 1 wherein said ratio of encapsulating composition to active ingredient is from about 1:1 to about 10:1.
Claim 8
Dependent Claim 15 words
The composition of claim 1 wherein said ratio is from about 3:1 to about 5:1.
Claim 9
Dependent Claim 34 words
The composition of claim 1 wherein said sweeteners are selected from the group consisting of amino acid-based sweeteners, dipeptide sweeteners, glycyrrhizin, saccharin and its salts, acesulfame salts, cyclamates, steviosides, talin, dihydrochalcone, and mixtures thereof.
Claim 10
Dependent Claim 85 words
A chewing gum oomposition containing an encapsulated sweetener wherein the encapsulant comprises a blend of polyvinyl acetate and a hydrophobic plasticizer, said polyvinyl acetate having a molecular weight of from about 20,000 MWU to about 100,000 MWU and said hydrophobic plasticizer selected from the group consisting of mono-, di- and triglycerides having a fatty acid chain length of from about 16 to about 22 carbon atoms wherein said polyvinyl acetate and hydrophobic plasticizer are present in in a ratio of about 5:1 to about 1:5.
Claim 11
Dependent Claim 85 words
A chewing gum oomposition containing an encapsulated sweetener wherein the encapsulant comprises a blend of polyvinyl acetate and a hydrophobic plasticizer, said polyvinyl acetate having a molecular weight of from about 20,000 MWU to about 100,000 MWU and said hydrophobic plasticizer selected from the group consisting of mono-, di- and triglycerides having a fatty acid chain length of from about 16 to about 22 carbon atoms wherein said polyvinyl acetate and hydrophobic plasticizer are present in in a ratio of about 5:1 to about 1:5.
Claim 12
Dependent Claim 18 words
The chewing gum composition of claim 9 wherein there is additionally included other non-encapsulated sweeteners for sequential release.
Claim 13
Dependent Claim 36 words
The product of claim 9 wherein said sweetener is selected from the group consisting of amino acid based sweeteners, dipeptides sweeteners, glycyrrhizin, saccharin and its salts, acesulfame salts, cyclamates, steviosides, talin, dihydrochalcone compounds and mixtures thereof.
Claim 14
Dependent Claim 178 words
A process for preparing a chewing gum composition containing a sweetener encapsulated in a solvent free encapsulation composition for protection of said sweetener from deterioration due to moisture comprising: providing a blend of high molecular weight polyvinyl acetate and a hydrophobic plasticizer, wherein said high molecular weight polyvinyl acetate and hydrophobic plasticizer form a film in combination in the absence of an added solvent, encapsulating said sweetener with said blend in the absence of an added solvent therefor, and incorporating said encapsulated sweetener into one of a gum base used in said chewing gum composition or directly into said overall composition during preparation thereof, and in both said base and said composition wherein said high molecular weight polyvinyl acetate is from about 30,000 MWU to about 60,000 MWU and said plasticizer is a mono-, di- or triglyceride having a fatty acid chain weight length of from about 16 to about 22 carbon atoms, said polyvinyl acetate and said hydrophobic plasticizer melt blended in a ratio of polyvinyl acetate to hydrophobic plastizer of from about 5:1 to about 1:5.
Claim 15
Dependent Claim 178 words
A process for preparing a chewing gum composition containing a sweetener encapsulated in a solvent free encapsulation composition for protection of said sweetener from deterioration due to moisture comprising: providing a blend of high molecular weight polyvinyl acetate and a hydrophobic plasticizer, wherein said high molecular weight polyvinyl acetate and hydrophobic plasticizer form a film in combination in the absence of an added solvent, encapsulating said sweetener with said blend in the absence of an added solvent therefor, and incorporating said encapsulated sweetener into one of a gum base used in said chewing gum composition or directly into said overall composition during preparation thereof, and in both said base and said composition wherein said high molecular weight polyvinyl acetate is from about 30,000 MWU to about 60,000 MWU and said plasticizer is a mono-, di- or triglyceride having a fatty acid chain weight length of from about 16 to about 22 carbon atoms, said polyvinyl acetate and said hydrophobic plasticizer melt blended in a ratio of polyvinyl acetate to hydrophobic plastizer of from about 5:1 to about 1:5.
Claim 16
Dependent Claim 39 words
The process of claim 12 wherein said high molecular weight polyvinyl acetate is about 40,000 MWU and said plasticizer is gylcerol monostearate blended in a ratio of from about 2:1 to about 1:2 of polyvinyl acetate to glyceryl mono-stearate.
Claim 17
Dependent Claim 18 words
The process of claim 12 wherein said sweetener is encapsulated by one of melt blending and spray congealing.
Claim 18
Dependent Claim 26 words
The process of claim 14 wherein said polyvinyl acetate and said plasticizer are melt blended at a temperature of from about 70° to about 90° C.
Claim 19
Dependent Claim 32 words
The process of claim 15 wherein said sweetener is encapsulated by blending in a molten mass resulting from said melt blending, followed by cooling to a solid and grinding to a particulate.
Claim 20
Dependent Claim 13 words
The process of claim 16 wherein said particulate is about 30 mesh size.
Claim 21
Dependent Claim 14 words
The process of claim 17 wherein said sweetener is one of aspartame and saccharin.
Claim 22
Dependent Claim 26 words
The process of claim 12 wherein said encapsulated sweetener is incorporated during gum composition manufacture at a temperature of from about 45° C. to 55° C.

References Cited (Backward Citations)

US4384004A Cited
US4384004B1 Cited
US4386106A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1990-12-07 1991-06-08 1991-12-08 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1994-12-07 1995-06-08 1995-12-08 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1998-12-07 1999-06-08 1999-12-08 $7700.00 Window Closed / Lapsed

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