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Ion-beam nitriding of steels

Assignee: United States, NASA THE, Administrator of
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Filing: 1986-01-29
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Granted: 1987-11-03
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Expires: 2006-01-29
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Abstract

Abstract A surface of a steel substrate is nitrided without external heating by exposing it to a beam of nitrogen ions under a low pressure. The pressure is much lower than that employed for ion-nitriding, and an ion source is used instead of a glow discharge. Both of these features reduce the introduction of impurities into the substrate surface.

Inventors

  • 👤 Joshua Salik
  • 👤 Theodore E. Hubbell

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 03:07
CPC Classifications
C; C23; C23C; C23C8/00; C23C8/06; C23C8/36; C23C8/38

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 109 words
In a method of forming a nitrided layer without a compound layer on a surface of a steel substrate selected from the group consisting essentially of super nitralloys and stainless steels, the improvement comprising positioning said substrate in a vacuum chamber at ambient temperature, reducing the pressure in said chamber to about 3×10 -4 Torr, striking said surface with a beam of nitrogen ions having energies between about 0.5 keV and about 1.5 keV within said chamber in the absence of a discharge, and independently controlling the voltage and current of said ions to maintain said beam thereby forming said nitrided layer without external heating of said steel substrate.
Claim 2
Dependent Claim 109 words
In a method of forming a nitrided layer without a compound layer on a surface of a steel substrate selected from the group consisting essentially of super nitralloys and stainless steels, the improvement comprising positioning said substrate in a vacuum chamber at ambient temperature, reducing the pressure in said chamber to about 3×10 -4 Torr, striking said surface with a beam of nitrogen ions having energies between about 0.5 keV and about 1.5 keV within said chamber in the absence of a discharge, and independently controlling the voltage and current of said ions to maintain said beam thereby forming said nitrided layer without external heating of said steel substrate.
Claim 3
Dependent Claim 26 words
A method of nitriding as claimed in claim 1 wherein the substrate is a super nitralloy and the nitrogen ions strike the surface about 50 minutes.
Claim 4
Dependent Claim 27 words
A method of nitriding as claimed in claim 1 wherein the substrate is a stainless steel and the nitrogen ions strike the surface for about 70 minutes.

References Cited (Backward Citations)

US3341352A Cited
US3900636A Cited
US3832219A Cited
US4105443A Cited
US4250009A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1990-11-02 1991-05-04 1991-11-03 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1994-11-02 1995-05-04 1995-11-03 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1998-11-02 1999-05-04 1999-11-03 $7700.00 Window Closed / Lapsed

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