Control of bed expansion in expanded bed reactor

Claim 2

In a hydrogenation process wherein a fluid is recycled from an upper portion of a reactor to a portion of the reactor below an expanded bed of catalyst by a recycle pump, the improvement comprising: automatically controlling the expansion of the expanded bed of catalyst by automatically increasing the rate of speed of the recycle pump when the expanded bed is below a first level in the reactor until the bed reaches the first level; thereafter automatically maintaining a substantially constant speed for the pump until the expanded bed of catalyst reaches a second level in the reactor which is higher than the first level; automatically decreasing the rate of speed of the recycle pump until the expanded bed falls below the second level; and thereafter maintaining a substantially constant rate of speed of the recycle pump until the expanded bed falls below the first level.

Claim 3

The process of claim 1 and further comprising automatically decreasing the rate of speed of the recycle pump when the bed reaches a third level in the reactor which is higher than the second level at a rate which is greater than the rate of reduction of speed of the recycle pump when the pump reaches the second level until the expanded catalyst bed falls below the third level.

Claim 4

The process of claim 2 wherein the expanded bed is detected at first, second and third levels by detecting the density of the interior of the reactor at the first, second and third levels.

Claim 5

The process of claim 2 wherein density is detected by detecting the change of radiation between a source of radiation in the reactor at each of the first, second and third levels, and a radiation detector at each of the first, second and third levels.

Claim 6

The process of claim 4 wherein the speed of the pump is automatically controlled by controlling the output of a variable frequency drive connected to the pump.

Claim 7

The process of claim 5 wherein the variable frequency drive output is controlled by an automatic speed controller connected to the variable frequency drive.

Claim 8

A reaction system, comprising: a reactor for an expanded catalyst bed; a recycle pump for recycling fluid from a top portion of the reactor to a portion of the reactor below a catalyst bed within the reactor for passage upwardly through a catalyst bed within the reactor; first and second bed level detection means, said second bed level detection means being positioned at a higher level in the reactor than the first bed level detection means; means for automatically controlling the speed of the recycle pump; means for providing first and second signals from the first and second bed level detection means to the means for automatically controlling the speed of the recycle pump, said means for providing the first signal and the means for automatically controlling the speed of the recycle pump incrementally increasing the speed of the recycle pump when an expanded catalyst bed is below the first bed level detection means until an expanded bed of catalyst reaches the first bed level detection means and thereafter automatically maintaining a substantially constant recycle pump speed until an expanded catalyst bed reaches the second bed level detection means and the means for providing the second signal and the means for automatically controlling the speed of the recycle pump automatically incrementally decreasing the speed of the recycle pump when an expanded catalyst bed reaches the second bed level detection means and thereafter maintaining a substantially constant recycle pump speed until an expanded catalyst bed falls below the first bed level detection means.

Claim 9

A reaction system, comprising: a reactor for an expanded catalyst bed; a recycle pump for recycling fluid from a top portion of the reactor to a portion of the reactor below a catalyst bed within the reactor for passage upwardly through a catalyst bed within the reactor; first and second bed level detection means, said second bed level detection means being positioned at a higher level in the reactor than the first bed level detection means; means for automatically controlling the speed of the recycle pump; means for providing first and second signals from the first and second bed level detection means to the means for automatically controlling the speed of the recycle pump, said means for providing the first signal and the means for automatically controlling the speed of the recycle pump incrementally increasing the speed of the recycle pump when an expanded catalyst bed is below the first bed level detection means until an expanded bed of catalyst reaches the first bed level detection means and thereafter automatically maintaining a substantially constant recycle pump speed until an expanded catalyst bed reaches the second bed level detection means and the means for providing the second signal and the means for automatically controlling the speed of the recycle pump automatically incrementally decreasing the speed of the recycle pump when an expanded catalyst bed reaches the second bed level detection means and thereafter maintaining a substantially constant recycle pump speed until an expanded catalyst bed falls below the first bed level detection means.

Claim 10

The reaction system of claim 7 and further comprising a third bed level detection means positioned at a higher level than the second bed level detection means; means for providing a third signal from the third bed level detection means to the means for automatically controlling the speed of the recycle pump, said means for providing the third signal and the means for automatically controlling the speed of the recycle pump incrementally decreasing the speed of the recycle pump when an expanded catalyst bed reaches the third bed level detection means at a rate faster than the rate of decrease of the speed of the recycle pump when an expanded catalyst bed reaches the second level detection means until an expanded catalyst bed falls below the third bed level detection means.

Claim 11

The system of claim 8 wherein the first, second and third bed level detection means are density detectors.

Claim 12

The system of claim 9 wherein the density detectors are each comprised of a radiation source within the reactor and means for detecting radiation.

Claim 13

The system of claim 10 wherein the means for automatically controlling the speed of the recycle pump comprises a variable frequency drive connected to the pump.

Claim 14

The system of claim 11 wherein the means for automatically controlling the speed of the recycle pump further comprises a speed controller for controlling the variable frequency drive.

Claim 15

The process of claim 1 wherein the rate of speed of the recycle pump is automatically incrementally increased at a rate until the bed reaches the first level, and the rate of speed of the recycle pump is automatically incrementally decreased at a predetermined rate until the bed falls below the second level.

Claim 16

The process of claim 1 and further comprising automatically decreasing the rate of speed of the recycle pump when, after a period of time, the expanded bed neither falls below the first level nor reaches the second level until the expanded bed falls below the first level.