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US4677188A
Expired / Lapsed
US
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Transparent slippery biaxially stretched polyester film
Assignee: Diafoil Co Ltd
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Filing: 1986-06-04
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Granted: 1987-06-30
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Expires: 2006-06-04
Abstract
Abstract There is disclosed a transparent slippery biaxially stretched polyester film characterized by satisfying the relations represented by the following formulas after being biaxially stretched and heat-set: 0.155</= DELTA P</=0.165 (1) 1.605</= &upbar& n</=1.610 (2) DELTA n</=0.02 (3) 7.0</=XI</=11.0 (4) 0.55</=[ eta ]F</=0.65 (5) <IMAGE> (6) DELTA H</=0.5 (7) wherein DELTA P, &upbar& n, DELTA n, XI, [ eta ]F and DELTA H ar respectively degree of planar orientation, average refractive index, birefringence, % ratio of the peak value of the (1 &upbar& 10) face measured by X-ray diffractometry to the peak value of the (100) face, intrinsic viscosity and surface haze of the biaxially stretched film.
Inventors
- 👤 Shigeo Utsumi
- 👤 Kichinojyo Tomitaka
- 👤 Yujiro Fukuda
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-05 09:43
CPC Classifications
C; C08; C08J; C08J5/00; C08J5/18; G; G03; G03C; G03C1/00; G03C1/76; G03C1/795; G03C1/7954; C08J2367/00; C08J2367/02; Y; Y10; Y10T; Y10T428/00; Y10T428/31504; Y10T428/31786
Claims Analysis
Total Claims: 5
Claim 1
Independent Claim
90 words
Transparent slippery biaxially stretched polyester film characterized by satisfying the relations represented by the following formulas after being biaxially stretched and heat-set: 0.155≦ΔP≦0.165 (1) 1.605≦n≦1.610 (2) Δn≦0.02 (3) 7.0≦X.sub.I ≦11.0 (4) 0.55≦[η].sub.F ≦0.65 (5) ##EQU6## ΔH≦0.5 (7) wherein ΔP, n, Δn, X I , [η] F and ΔH are respectively degree of planar orientation, average refractive index, birefringence, % ratio of the peak value of the (1l0) face measured by X-ray diffractometry to the peak value of the (100) face, intrinsic viscosity and surface haze of the biaxially stretched film.
Claim 2
Dependent Claim
90 words
Transparent slippery biaxially stretched polyester film characterized by satisfying the relations represented by the following formulas after being biaxially stretched and heat-set: 0.155≦ΔP≦0.165 (1) 1.605≦n≦1.610 (2) Δn≦0.02 (3) 7.0≦X.sub.I ≦11.0 (4) 0.55≦[η].sub.F ≦0.65 (5) ##EQU6## ΔH≦0.5 (7) wherein ΔP, n, Δn, X I , [η] F and ΔH are respectively degree of planar orientation, average refractive index, birefringence, % ratio of the peak value of the (1l0) face measured by X-ray diffractometry to the peak value of the (100) face, intrinsic viscosity and surface haze of the biaxially stretched film.
Claim 3
Dependent Claim
38 words
The polyester film as recited in claim 1, which is characterized by containing not less than 0.003% by weight and not more than 0.015% by weight of amorphous silica having an average particle diameter of 0.8μ to 1.5μ.
Claim 4
Dependent Claim
180 words
A process for transparent slippery polyester film which satisfies the relations represented by the following formulas: 0.155≦ΔP≦0.165 (1) 1.605≦n≦1.610 (2) Δn≦0.02 (3) 7.0≦X.sub.I ≦11.0 (4) 0.55≦[η].sub.F ≦0.65 (5) ##EQU7## ΔH≦0.5 (7) wherein ΔP, n, Δn, X I , [η] F and ΔH are respectively degree of surface orientation, average refractive index, birefringence, % ratio of the peak value of the (110) face measured by X-ray diffractometry to the peak value of the (100) face, intrinsic viscosity and surface haze of the biaxially stretched film, said process comprising longitudinally stretching an unstretched polyester film containing minute particles of amorphous silica and other substances at a temperature of 75° C. to 130° C. in one step so that the birefringence after the longitudinal stretching exceeds 0.080, and transversally stretching the film by a factor of not less than 3.5 and not more than 5.0, and thereafter heat-setting the film at a temperature of 200° C. to 250° C. for 1 second to 10 minutes, wherein the film is transversally relaxed by 1 to 15% at a temperature not lower than 200° C.
Claim 5
Dependent Claim
180 words
A process for transparent slippery polyester film which satisfies the relations represented by the following formulas: 0.155≦ΔP≦0.165 (1) 1.605≦n≦1.610 (2) Δn≦0.02 (3) 7.0≦X.sub.I ≦11.0 (4) 0.55≦[η].sub.F ≦0.65 (5) ##EQU7## ΔH≦0.5 (7) wherein ΔP, n, Δn, X I , [η] F and ΔH are respectively degree of surface orientation, average refractive index, birefringence, % ratio of the peak value of the (110) face measured by X-ray diffractometry to the peak value of the (100) face, intrinsic viscosity and surface haze of the biaxially stretched film, said process comprising longitudinally stretching an unstretched polyester film containing minute particles of amorphous silica and other substances at a temperature of 75° C. to 130° C. in one step so that the birefringence after the longitudinal stretching exceeds 0.080, and transversally stretching the film by a factor of not less than 3.5 and not more than 5.0, and thereafter heat-setting the film at a temperature of 200° C. to 250° C. for 1 second to 10 minutes, wherein the film is transversally relaxed by 1 to 15% at a temperature not lower than 200° C.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1990-06-29 | 1990-12-29 | 1991-06-30 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1994-06-29 | 1994-12-29 | 1995-06-30 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1998-06-29 | 1998-12-29 | 1999-06-30 | $7700.00 | Window Closed / Lapsed |