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US4670250A Expired / Lapsed US ⏱️ 0.0 years remaining

Durable controlled release microcapsules

Assignee: Bend Research Inc
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Filing: 1983-10-21
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Granted: 1987-06-02
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Expires: 2003-10-21
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Abstract

Abstract Impact-resistant microcapsules for the sustained and controlled release of biologically active ingredients through a surrounding permeable polymeric wall are disclosed wherein the ratio by weight of active ingredient to polymer is from about 4:1 to about 1:4, the polymeric walls having high tensile yield and tensile impact strengths and low nitrogen permeabilities.

Inventors

  • 👤 Richard W. Baker

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 16:07
CPC Classifications
A; A01; A01N; A01N25/00; A01N25/26; A01N25/28; A61; A61K; A61K9/00; A61K9/48; A61K9/50; A61K9/5005; A61K9/5021; A61K9/5031; B; B01; B01J; B01J13/00; B01J13/02; B01J13/06; B01J13/12; B01J13/125

Claims Analysis

Total Claims: 13
Claim 1
Independent Claim 88 words
A controlled release microcapsule comprising a core of active ingredient and a permeable polymer surrounding said core, (a) the active ingredient being biologically active, (b) the permeable polymer being thermoplastic and soluble in a common organic solvent, having a tensile yield strength of more than 9,000 lb/in 2 , a tensile impact strength of more than 70 ft-lb/in 2 , and a nitrogen permeability of less than 10 -10 cm 3 -cm/cm 2 -sec-cmHg, and (c) having a core-to-polymer ratio from about 4:1 to about 1:4 by weight.
Claim 2
Dependent Claim 88 words
A controlled release microcapsule comprising a core of active ingredient and a permeable polymer surrounding said core, (a) the active ingredient being biologically active, (b) the permeable polymer being thermoplastic and soluble in a common organic solvent, having a tensile yield strength of more than 9,000 lb/in 2 , a tensile impact strength of more than 70 ft-lb/in 2 , and a nitrogen permeability of less than 10 -10 cm 3 -cm/cm 2 -sec-cmHg, and (c) having a core-to-polymer ratio from about 4:1 to about 1:4 by weight.
Claim 3
Dependent Claim 48 words
The microcapsule of claim 1 wherein the polymer is selected from polysulfones, polyether sulfones, polyaryl sulfones, polycarbonates, polymethylmethacrylates, poly(styrene-acrylonitriles), polystyrenes, acrylonitrilebutadiene-styrene polymers, polyacrylonitriles, polyvinyl fluorides, polyvinylidene fluorides, polyvinyl chlorides, polyvinylidene chlorides, polyethyleneterephthalates, polybutyleneterephthalates, polyamides, polyamideimides, polyimides, polyacetals, cellulose esters, polyurethanes, polyarylates, polyaryl ethers, and derivatives or copolymers thereof.
Claim 4
Dependent Claim 17 words
The microcapsule of claim 1 wherein the polymer is selected from polysulfones, polyether sulfones and polyaryl sulfones.
Claim 5
Dependent Claim 11 words
The microcapsule of claim 1 wherein the polymer is a polycarbonate.
Claim 6
Dependent Claim 11 words
The microcapsule of claim 1 wherein the polymer is a polymethylmethacrylate.
Claim 7
Dependent Claim 11 words
The microcapsule of claim 1 wherein the polymer is a poly(styrene-acrylonitrile).
Claim 8
Dependent Claim 14 words
The microcapsule of claim 1 wherein the polymer is selected from polyamides and polyamide-imides.
Claim 9
Dependent Claim 21 words
The microcapsule of claim 1 wherein the active ingredient is selected from pheromones, insecticides, herbicides, fertilizers, pharmaceuticals, deodorants, fragrances, and flavors.
Claim 10
Dependent Claim 12 words
The microcapsule of claim 1 wherein the active ingredient is a pheromone.
Claim 11
Dependent Claim 22 words
The microcapsule of claim 9 wherein the pheromone is selected from disparlure, gossyplure, virelure, muscalure, grandlure, japonilure, trimedlure, codlure and periplanone B.
Claim 12
Dependent Claim 12 words
The microcapsule of claim 1 wherein the active ingredient is an insecticide.
Claim 13
Dependent Claim 24 words
The microcapsule of claim 11 wherein the insecticide is selected from naled, dimpylate, propoxur, chlorpyrifos, malathion, methyl parathion, carbaryl, methomyl, permethrin, fenvalerate and dichlorvos.

References Cited (Backward Citations)

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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1990-06-01 1990-12-01 1991-06-02 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1994-06-01 1994-12-01 1995-06-02 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1998-06-01 1998-12-01 1999-06-02 $7700.00 Window Closed / Lapsed

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