US4659571A
Expired / Lapsed
US
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Compressed powder formulation containing organophilic clay and a process for making the formulation
Assignee: Elementis Specialties Inc
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Filing: 1985-03-20
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Granted: 1987-04-21
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Expires: 2005-03-20
Abstract
Abstract A compressed powder formulation which consists essentially of an organophilic clay and at least one topical agent. The formulation maintains its physical integrity upon handling thereby permitting the preparation of the formulation in the form of self-supporting sticks and exhibits an acceptable level of payout. Additionally, the formulation retains an acceptable level of payout even when contacted with water. A process of making the formulation by compressing a powderous mixture is also set forth.
Inventors
- 👤 Dennis Laba
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-04 09:36
CPC Classifications
A; A61; A61K; A61K8/00; A61K8/18; A61K8/30; A61K8/40; A61K8/41; A61K8/416; A61K8/02; A61K8/19; A61K8/26; A61Q; A61Q1/00; A61Q1/12; Y; Y10; Y10S; Y10S424/00; Y10S424/05
Claims Analysis
Total Claims: 30
Claim 1
Independent Claim
84 words
A dry, compressed powder formulation consisting essentially of: (a) from about 10 to about 99.95% by weight of an organophilic clay; and (b) from about 0.05% to about 90% by weight of at least one topical agent, wherein the compressed powder formulation is in solid form, maintains its physical integrity upon handling, has a payout which is substantially uniform and which is from about 10 to about 100 milligrams and retains at least about 90% of its original payout after being contacted with water.
Claim 2
Dependent Claim
84 words
A dry, compressed powder formulation consisting essentially of: (a) from about 10 to about 99.95% by weight of an organophilic clay; and (b) from about 0.05% to about 90% by weight of at least one topical agent, wherein the compressed powder formulation is in solid form, maintains its physical integrity upon handling, has a payout which is substantially uniform and which is from about 10 to about 100 milligrams and retains at least about 90% of its original payout after being contacted with water.
Claim 3
Dependent Claim
30 words
The compressed powder formulation of claim 1 wherein the topical agent is selected from the group consisting of antiperspirant agents, deodorant agents, pigments, antifungal agents, insect repellants and mixtures thereof.
Claim 4
Dependent Claim
22 words
The compressed powder formulation of claim 2 wherein the formulation contains from about 10 to about 30% by weight of antiperspirant agent.
Claim 5
Dependent Claim
35 words
The compressed powder formulation of claim 3 wherein the antiperspirant agent is selected from the group consisting of aluminum chlorohydrate, aluminum chlorohydrex, aluminum zirconium chlorohydrate, aluminum zirconium chlorohydrex, aluminum zirconium glycine complexes and mixtures thereof.
Claim 6
Dependent Claim
14 words
The compressed powder formulation of claim 4 wherein the antiperspirant agent is aluminum chlorohydrate.
Claim 7
Dependent Claim
21 words
The compressed powder formulation of claim 5 wherein the formulation is in the form of a stick adapted for human use.
Claim 8
Dependent Claim
23 words
The compressed powder formulation of claim 4 wherein the formulation contains from about 15 to about 25% by weight of the antiperspirant agent.
Claim 9
Dependent Claim
22 words
The compressed powder formulation of claim 1 wherein the formulation contains from about 0.05 to about 10% by weight of deodorant agent.
Claim 10
Dependent Claim
37 words
The compressed powder formulation of claim 8 wherein the deodorant agent is selected from the group consisting of triclosan, benzethonium chloride, aluminum chlorohydrate, aluminum zirconium chlorohydrate, fragrance, sodium aluminum chlorohydroxy lactate, cetyl pyridinium chloride, and mixtures thereof.
Claim 11
Dependent Claim
28 words
The compressed powder formulation of claim 9 wherein the deodorant agent is triclosan or benzethonium chloride in an amount ranging from about 0.1 to about 1% by weight.
Claim 12
Dependent Claim
73 words
The compressed powder formulation of claim 1 wherein the organophilic clay is the reaction product of a smectite-type clay having a cation exchange capacity of at least 75 milliequivalents per 100 grams of clay and at least one organic cation having the formula ##STR2## wherein R 1 is an alkyl group containing from 12 to 22 carbon atoms, R 2 is a benzyl group and R 3 and R 4 are methyl groups.
Claim 13
Dependent Claim
15 words
The compressed powder formulation of claim 11 wherein the smectite-type clay is bentonite or hectorite.
Claim 14
Dependent Claim
13 words
The compressed powder formulation of claim 12 wherein the smectite-type clay is hectorite.
Claim 15
Dependent Claim
28 words
The compressed powder formulation of claim 11 wherein from about 90 to about 150 milliequivalents of the cation are reacted with each 100 grams of the smectite-type clay.
Claim 16
Dependent Claim
45 words
The compressed powder formulation of claim 11 wherein from about 5 to about 100 milliequivalents of an organic anion derived from an organic compound having a pK A less than about 11.0 is reacted the organic cation and each 100 grams of the smectite-type clay.
Claim 17
Dependent Claim
18 words
The compressed powder formulation of claim 15 wherein the organic anion is a mixture of different organic anions.
Claim 18
Dependent Claim
28 words
The compressed powder formulation of claim 15 wherein the amount of organic anion ranges from about 10 to about 50 milliequivalents per 100 grams of the smectite-type clay.
Claim 19
Dependent Claim
22 words
The compressed powder formulation of claim 1 wherein the payout is in the range of from about 40 to about 80 milligrams.
Claim 20
Dependent Claim
23 words
The compressed powder formulation of claim 18 wherein the formulation retains a payout of at least about 95% after being contacted with water.
Claim 21
Dependent Claim
22 words
The compressed powder formulation of claim 1 wherein the formulation further comprises at least one of a filler and a lubricating agent.
Claim 22
Dependent Claim
106 words
A process for making a dry, compressed powder formulation comprising: (a) mixing from about 10 to about 99.95% by weight of an organophilic clay and from about 0.05 to about 90% of at least one topical agent to obtain a substantially uniform powderous mixture; and (b) compressing the powderous mixture at a pressure in the range of from about 200 to about 1600 pounds per square inch to obtain a compressed powder formulation which maintains its physical integrity upon handling, has a payout of from about 10 to about 100 milligrams and retains at least about 90% of its original payout after being contacted with water.
Claim 23
Dependent Claim
106 words
A process for making a dry, compressed powder formulation comprising: (a) mixing from about 10 to about 99.95% by weight of an organophilic clay and from about 0.05 to about 90% of at least one topical agent to obtain a substantially uniform powderous mixture; and (b) compressing the powderous mixture at a pressure in the range of from about 200 to about 1600 pounds per square inch to obtain a compressed powder formulation which maintains its physical integrity upon handling, has a payout of from about 10 to about 100 milligrams and retains at least about 90% of its original payout after being contacted with water.
Claim 24
Dependent Claim
20 words
The process of claim 21 wherein the formulation is compressed into the form of a stick adapted for human use.
Claim 25
Dependent Claim
27 words
The process of claim 21 wherein the formulation is compressed at a pressure in the range of from about 250 to about 650 pounds per square inch.
Claim 26
Dependent Claim
17 words
The process of claim 21 wherein the formulation is prepared in the substantial absence of free water.
Claim 27
Dependent Claim
28 words
The process of claim 21 wherein the topical agent is selected from the group consisting of antiperspirant agents, deodorant agents, pigments, antifungal agents, insect repellants and mixtures thereof.
Claim 28
Dependent Claim
21 words
The process of claim 25 wherein the formulation contains from about 10 to about 30% by weight of an antiperspirant agent.
Claim 29
Dependent Claim
12 words
The process of claim 26 wherein the antiperspirant agent is aluminim chlorohydrate.
Claim 30
Dependent Claim
19 words
The process of claim 27 wherein the formulation has a payout of from about 40 to about 80 milligrams.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1990-04-20 | 1990-10-20 | 1991-04-21 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1994-04-20 | 1994-10-20 | 1995-04-21 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1998-04-20 | 1998-10-20 | 1999-04-21 | $7700.00 | Window Closed / Lapsed |